Crystallography Open Database

Information card for entry 7038554

Preview

Coordinates	7038554.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H60 B2 F24 N P2 Rh
Calculated formula	C55 H60 B2 F24 N P2 Rh
Title of publication	Variable coordination modes and catalytic dehydrogenation of B-phenyl amine-boranes.
Authors of publication	Kumar, Amit; Priest, Isobel K.; Hooper, Thomas N.; Weller, Andrew S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	14
Pages of publication	6183 - 6195
a	25.3462 ± 0.0003 Å
b	18.3643 ± 0.0002 Å
c	25.7382 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	11980.2 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0636
Residual factor for significantly intense reflections	0.0549
Weighted residual factors for significantly intense reflections	0.1531
Weighted residual factors for all reflections included in the refinement	0.1666
Goodness-of-fit parameter for all reflections included in the refinement	0.841
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
181720 (current)	2016-04-05	cif/ Updating files of 7038549, 7038550, 7038551, 7038552, 7038553, 7038554, 7038555, 7038556 Original log message: Adding full bibliography for 7038549--7038556.cif.	7038554.cif
176906	2016-02-25	cif/ Adding structures of 7038549, 7038550, 7038551, 7038552, 7038553, 7038554, 7038555, 7038556 via cif-deposit CGI script.	7038554.cif