Crystallography Open Database

Information card for entry 7038690

Preview

Coordinates	7038690.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H48 F6 P5 Re Si
Calculated formula	C19 H48 F6 P5 Re Si
Title of publication	Electronic communication in phosphine substituted bridged dirhenium complexes - clarifying ambiguities raised by the redox non-innocence of the C4H2- and C4-bridges.
Authors of publication	Li, Yan; Blacque, Olivier; Fox, Thomas; Luber, Sandra; Polit, Walther; Winter, Rainer F.; Venkatesan, Koushik; Berke, Heinz
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	13
Pages of publication	5783 - 5799
a	19.4556 ± 0.0003 Å
b	19.8765 ± 0.0002 Å
c	33.6182 ± 0.0005 Å
α	90°
β	90°
γ	90°
Cell volume	13000.5 ± 0.3 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0615
Residual factor for significantly intense reflections	0.0414
Weighted residual factors for significantly intense reflections	0.084
Weighted residual factors for all reflections included in the refinement	0.0872
Goodness-of-fit parameter for all reflections included in the refinement	0.942
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
181636 (current)	2016-04-05	cif/ Updating files of 7038690, 7038691, 7038692, 7038693, 7038694, 7038695 Original log message: Adding full bibliography for 7038690--7038695.cif.	7038690.cif
177272	2016-03-04	cif/ Adding structures of 7038690, 7038691, 7038692, 7038693, 7038694, 7038695 via cif-deposit CGI script.	7038690.cif