Crystallography Open Database

Information card for entry 7038713

Preview

Coordinates	7038713.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H64 P2 Pt Si2
Calculated formula	C34 H64 P2 Pt Si2
SMILES	[Pt]1([P](CC[P]1(C1CCCCC1)C1CCCCC1)(C1CCCCC1)C1CCCCC1)([SiH2]C)[SiH2]C.c1ccccc1
Title of publication	Hydrodealkoxylation reactions of silyl ligands at platinum: reactivity of SiH3 and SiH2Me complexes.
Authors of publication	Mitzenheim, Cathérine; Braun, Thomas; Laubenstein, Reik; Braun, Beatrice; Herrmann, Roy
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	15
Pages of publication	6394 - 6404
a	11.214 ± 0.0004 Å
b	14.028 ± 0.0005 Å
c	23.0967 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	3633.3 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0257
Residual factor for significantly intense reflections	0.0229
Weighted residual factors for significantly intense reflections	0.0456
Weighted residual factors for all reflections included in the refinement	0.0463
Goodness-of-fit parameter for all reflections included in the refinement	0.998
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
182696 (current)	2016-05-06	cif/ Updating files of 7038713, 7038714, 7038715 Original log message: Adding full bibliography for 7038713--7038715.cif.	7038713.cif
178012	2016-03-08	cif/ Adding structures of 7038713, 7038714, 7038715 via cif-deposit CGI script.	7038713.cif