Crystallography Open Database

Information card for entry 7039024

Preview

Coordinates	7039024.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H75 Cl2 P Sn
Calculated formula	C60 H75 Cl2 P Sn
SMILES	[Sn](Cl)(Cl)(c1c(cccc1c1c(cc(C(C)C)cc1C(C)C)C(C)C)c1c(cc(cc1C(C)C)C(C)C)C(C)C)c1c(P(c2ccccc2)c2ccccc2)cccc1.C=CCCCC
Title of publication	Reaction of stannylene phosphorus Lewis pairs with dichlorides of germanium, tin and lead - the formation of base stabilized stannyl stannylenes/germylenes and redox reaction with PbCl2.
Authors of publication	Krebs, K. M.; Maudrich, J.-J.; Wesemann, L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	19
Pages of publication	8081 - 8088
a	14.7617 ± 0.0003 Å
b	24.9093 ± 0.0005 Å
c	29.069 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	10688.8 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.052
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.0782
Weighted residual factors for all reflections included in the refinement	0.0858
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
185533 (current)	2016-08-07	cif/ Updating files of 7039020, 7039021, 7039022, 7039023, 7039024 Original log message: Adding full bibliography for 7039020--7039024.cif.	7039024.cif
182134	2016-04-15	cif/ Adding structures of 7039020, 7039021, 7039022, 7039023, 7039024 via cif-deposit CGI script.	7039024.cif