Crystallography Open Database

Information card for entry 7039451

Preview

Coordinates	7039451.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H56 N8 P4 Sb2
Calculated formula	C32 H56 N8 P4 Sb2
SMILES	CC(C)C1=PC(C(C)C)=[N]2N1[Sb]134N5[N](=C(P=C5C(C)C)C(C)C)[Sb]24(N2[N]1=C(P=C2C(C)C)C(C)C)N1C(=PC(C(C)C)=[N]31)C(C)C
Title of publication	Paddlewheel 1,2,4-diazaphospholide distibines with the shortest antimony-antimony single bonds.
Authors of publication	Zhao, Minggang; Wang, Lixia; Zhang, Xiang; Zheng, Wenjun
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	26
Pages of publication	10505 - 10509
a	10.4526 ± 0.0006 Å
b	13.8011 ± 0.0009 Å
c	15.2389 ± 0.001 Å
α	90.444 ± 0.005°
β	100.987 ± 0.005°
γ	94.207 ± 0.005°
Cell volume	2151.7 ± 0.2 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0862
Residual factor for significantly intense reflections	0.0575
Weighted residual factors for significantly intense reflections	0.1425
Weighted residual factors for all reflections included in the refinement	0.166
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
211691 (current)	2018-10-29	cif/7: Fixing Z values and formulae	7039451.cif
185340	2016-08-07	cif/ Updating files of 7039448, 7039449, 7039450, 7039451, 7039452 Original log message: Adding full bibliography for 7039448--7039452.cif.	7039451.cif
183381	2016-06-11	cif/ Adding structures of 7039448, 7039449, 7039450, 7039451, 7039452 via cif-deposit CGI script.	7039451.cif