Crystallography Open Database

Information card for entry 7039557

Preview

Coordinates	7039557.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H35 Li N4
Calculated formula	C21.997 H35 Li N4
Title of publication	Simplifying metal-'ate' chemistry: formation and comprehensive characterisation of a homo-metallic amido lithiate complex.
Authors of publication	Greer, Jamie A.; Blair, Victoria L.; Thompson, Christopher D.; Andrews, Philip C.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	27
Pages of publication	10887 - 10890
a	9.0445 ± 0.0008 Å
b	15.2792 ± 0.0011 Å
c	15.5861 ± 0.0013 Å
α	90°
β	90°
γ	90°
Cell volume	2153.9 ± 0.3 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0434
Residual factor for significantly intense reflections	0.0355
Weighted residual factors for significantly intense reflections	0.0821
Weighted residual factors for all reflections included in the refinement	0.0866
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
185409 (current)	2016-08-07	cif/ Updating files of 7039555, 7039556, 7039557 Original log message: Adding full bibliography for 7039555--7039557.cif.	7039557.cif
183522	2016-06-16	cif/ Adding structures of 7039555, 7039556, 7039557 via cif-deposit CGI script.	7039557.cif