Crystallography Open Database

Information card for entry 7041062

Preview

Coordinates	7041062.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H45 Li O3 Si
Calculated formula	C34 H45 Li O3 Si
Title of publication	Synthesis and study of an unprecedented 1-hydro-1-lithio-1-silafluorene anion.
Authors of publication	Tian, Dawei; Li, Xiaofei; Liu, YuanYuan; Cao, Yue; Li, Tianhao; Hu, Hongfan; Cui, Chunming
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2016
Journal volume	45
Journal issue	46
Pages of publication	18447 - 18449
a	8.991 ± 0.004 Å
b	16.122 ± 0.007 Å
c	22.047 ± 0.01 Å
α	90°
β	91.154 ± 0.007°
γ	90°
Cell volume	3195 ± 2 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1173
Residual factor for significantly intense reflections	0.0994
Weighted residual factors for significantly intense reflections	0.2372
Weighted residual factors for all reflections included in the refinement	0.25
Goodness-of-fit parameter for all reflections included in the refinement	1.148
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
190109 (current)	2017-01-09	cif/ Updating files of 7041062 Original log message: Adding full bibliography for 7041062.cif.	7041062.cif
187677	2016-10-29	cif/ Adding structures of 7041062 via cif-deposit CGI script.	7041062.cif