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Information card for entry 7044347
Preview
| Coordinates | 7044347.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C108.5 H65 B2 F47 N4 P |
|---|---|
| Calculated formula | C108.495 H65.04 B2 F46.99 N4 P |
| Title of publication | Synthesis and Oxidation of Phosphine Cations† |
| Authors of publication | Mehta, Meera; Johnstone, Tim; Lam, Jolie; Bidraha, Bid; Hermannsdorfer, Andre; Driess, Matthias; Stephan, Douglas W. |
| Journal of publication | Dalton Trans. |
| Year of publication | 2017 |
| a | 15.5736 ± 0.0004 Å |
| b | 17.498 ± 0.0005 Å |
| c | 18.9275 ± 0.0004 Å |
| α | 83.61 ± 0.002° |
| β | 89.0867 ± 0.0019° |
| γ | 73.915 ± 0.003° |
| Cell volume | 4924.6 ± 0.2 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0815 |
| Residual factor for significantly intense reflections | 0.0699 |
| Weighted residual factors for significantly intense reflections | 0.1983 |
| Weighted residual factors for all reflections included in the refinement | 0.2143 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 201395 (current) | 2017-09-28 | cif/ Adding structures of 7044346, 7044347, 7044348, 7044349 via cif-deposit CGI script. |
7044347.cif |
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Users of the data should acknowledge the original authors of the
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