Crystallography Open Database

Information card for entry 7045012

Preview

Coordinates	7045012.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58.63 H74.13 Cl P Rh Sn
Calculated formula	C59 H75 Cl P Rh Sn
Title of publication	Coordination chemistry of stannylene-based Lewis pairs - insertion into M-Cl and M-C bonds. From base stabilized stannylenes to bidentate ligands.
Authors of publication	Krebs, K. M.; Freitag, S.; Maudrich, J.-J.; Schubert, H.; Sirsch, P.; Wesemann, L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2017
Journal volume	47
Journal issue	1
Pages of publication	83 - 95
a	13.1474 ± 0.0002 Å
b	16.9062 ± 0.0003 Å
c	24.3248 ± 0.0004 Å
α	90°
β	103.307 ± 0.001°
γ	90°
Cell volume	5261.57 ± 0.15 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.035
Residual factor for significantly intense reflections	0.0282
Weighted residual factors for significantly intense reflections	0.0632
Weighted residual factors for all reflections included in the refinement	0.0664
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229380 (current)	2019-11-17	cif/ Updating files of 7045009, 7045010, 7045011, 7045012, 7045013, 7045014, 7045015, 7045016 Original log message: Adding full bibliography for 7045009--7045016.cif.	7045012.cif
204174	2017-12-12	cif/ Adding structures of 7045009, 7045010, 7045011, 7045012, 7045013, 7045014, 7045015, 7045016 via cif-deposit CGI script.	7045012.cif