Crystallography Open Database

Information card for entry 7046906

Preview

Coordinates	7046906.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H62 Cl4 P4 Rh2
Calculated formula	C74 H62 Cl4 P4 Rh2
Title of publication	Simple generation of a dirhodium μ-carbido complex via thiocarbonyl reduction.
Authors of publication	Barnett, Harrison J.; Burt, Liam K.; Hill, Anthony F.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	29
Pages of publication	9570 - 9574
a	12.5983 ± 0.0002 Å
b	13.8742 ± 0.0003 Å
c	20.565 ± 0.0004 Å
α	85.461 ± 0.002°
β	84.238 ± 0.001°
γ	75.285 ± 0.001°
Cell volume	3453.74 ± 0.12 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0345
Residual factor for significantly intense reflections	0.0319
Weighted residual factors for significantly intense reflections	0.0875
Weighted residual factors for all reflections included in the refinement	0.0901
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229165 (current)	2019-11-17	cif/ Updating files of 7046906, 7046907, 7046908, 7046909, 7046910 Original log message: Adding full bibliography for 7046906--7046910.cif.	7046906.cif
208731	2018-06-29	cif/ Adding structures of 7046906, 7046907, 7046908, 7046909, 7046910 via cif-deposit CGI script.	7046906.cif