Crystallography Open Database

Information card for entry 7046918

Preview

Coordinates	7046918.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H134 Ce Co O16 Si4
Calculated formula	C72 H134 Ce Co O16 Si4
Title of publication	Redox-enhanced hemilability of a tris(tert-butoxy)siloxy ligand at cerium.
Authors of publication	Friedrich, Jochen; Qiao, Yusen; Maichle-Mössmer, Cäcilia; Schelter, Eric J.; Anwander, Reiner
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	30
Pages of publication	10113 - 10123
a	20.536 ± 0.004 Å
b	16.007 ± 0.003 Å
c	25.726 ± 0.005 Å
α	90°
β	91.04 ± 0.03°
γ	90°
Cell volume	8455 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.081
Residual factor for significantly intense reflections	0.0422
Weighted residual factors for significantly intense reflections	0.0825
Weighted residual factors for all reflections included in the refinement	0.0979
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229805 (current)	2019-11-17	cif/ Updating files of 7046916, 7046917, 7046918, 7046919 Original log message: Adding full bibliography for 7046916--7046919.cif.	7046918.cif
208733	2018-06-29	cif/ Adding structures of 7046916, 7046917, 7046918, 7046919 via cif-deposit CGI script.	7046918.cif