Crystallography Open Database

Information card for entry 7046922

Preview

Coordinates	7046922.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	B28 K11 O48 Rb
Calculated formula	B28 K11 O48 Rb
Title of publication	K<sub>11</sub>RbB<sub>28</sub>O<sub>48</sub>: a new triple-layered borate with an unprecedented [B<sub>28</sub>O<sub>57</sub>] fundamental building block.
Authors of publication	Jiang, Dequan; Wang, Ying; Zhang, Bingbing; Han, Guopeng; Yang, Zhihua; Pan, Shilie
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	32
Pages of publication	10833 - 10836
a	6.6231 ± 0.0002 Å
b	11.3213 ± 0.0003 Å
c	28.701 ± 0.0009 Å
α	92.208 ± 0.002°
β	91.584 ± 0.002°
γ	90.2 ± 0.002°
Cell volume	2149.62 ± 0.11 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1361
Residual factor for significantly intense reflections	0.0719
Weighted residual factors for significantly intense reflections	0.1805
Weighted residual factors for all reflections included in the refinement	0.22
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229370 (current)	2019-11-17	cif/ Updating files of 7046922 Original log message: Adding full bibliography for 7046922.cif.	7046922.cif
208741	2018-06-30	cif/ Adding structures of 7046922 via cif-deposit CGI script.	7046922.cif