Crystallography Open Database

Information card for entry 7047343

Preview

Coordinates	7047343.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Complex1
Formula	C44 H104 O20 P4 Sn6
Calculated formula	C44 H98 O20 P4 Sn6
Title of publication	High-nuclearity silver ethynide clusters containing polynucleating oxygen donor ligands.
Authors of publication	Jin, Jun-Ling; Xie, Yun-Peng; Lu, Xing
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	37
Pages of publication	12972 - 12978
a	10.607 ± 0.0013 Å
b	16.984 ± 0.002 Å
c	19.941 ± 0.002 Å
α	90°
β	93.564 ± 0.003°
γ	90°
Cell volume	3585.4 ± 0.7 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0621
Residual factor for significantly intense reflections	0.0522
Weighted residual factors for significantly intense reflections	0.1079
Weighted residual factors for all reflections included in the refinement	0.1156
Goodness-of-fit parameter for all reflections included in the refinement	1.179
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229300 (current)	2019-11-17	cif/ Updating files of 7047343, 7047344, 7047345, 7047346 Original log message: Adding full bibliography for 7047343--7047346.cif.	7047343.cif
210106	2018-08-24	cif/ Adding structures of 7047343, 7047344, 7047345, 7047346 via cif-deposit CGI script.	7047343.cif