Crystallography Open Database

Information card for entry 7047762

Preview

Coordinates	7047762.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Ce(CzTiPr)2[N(SiMe3)2]
Chemical name	Bis(1,8-Bis(2?-H-tetrazo-5?-yl)-3,6-di-tert-butylcarbazolyl)(bis(trimethylsilyl)amido) cerium(III)
Formula	C79.5 H110 Ce N19 Si2
Calculated formula	C79.5 H110 Ce N19 Si2
Title of publication	Variable coordination of carbazolyl-bis(tetrazole) ligands in lanthanide chemistry.
Authors of publication	Gajecki, Leah; Berg, David J.; Hoenisch, Josh; Oliver, Allen G.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	43
Pages of publication	15487 - 15496
a	40.053 ± 0.007 Å
b	18.203 ± 0.003 Å
c	28.621 ± 0.005 Å
α	90°
β	128.185 ± 0.004°
γ	90°
Cell volume	16402 ± 5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	119.9 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0541
Residual factor for significantly intense reflections	0.0406
Weighted residual factors for significantly intense reflections	0.0937
Weighted residual factors for all reflections included in the refinement	0.1013
Goodness-of-fit parameter for all reflections included in the refinement	1.082
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229440 (current)	2019-11-17	cif/ Updating files of 7047755, 7047756, 7047757, 7047758, 7047759, 7047760, 7047761, 7047762 Original log message: Adding full bibliography for 7047755--7047762.cif.	7047762.cif
211437	2018-10-13	cif/ Adding structures of 7047755, 7047756, 7047757, 7047758, 7047759, 7047760, 7047761, 7047762 via cif-deposit CGI script.	7047762.cif