Crystallography Open Database

Information card for entry 7047984

Preview

Coordinates	7047984.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H38 N2 P2
Calculated formula	C20 H38 N2 P2
Title of publication	Symmetrical and unsymmetrical diphosphanes with diversified alkyl, aryl, and amino substituents.
Authors of publication	Szynkiewicz, Natalia; Ponikiewski, Łukasz; Grubba, Rafał
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	47
Pages of publication	16885 - 16894
a	9.902 ± 0.0005 Å
b	18.9837 ± 0.0007 Å
c	11.9159 ± 0.0006 Å
α	90°
β	95.506 ± 0.004°
γ	90°
Cell volume	2229.58 ± 0.18 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1617
Residual factor for significantly intense reflections	0.0656
Weighted residual factors for significantly intense reflections	0.149
Weighted residual factors for all reflections included in the refinement	0.1872
Goodness-of-fit parameter for all reflections included in the refinement	1.002
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229678 (current)	2019-11-17	cif/ Updating files of 7047971, 7047972, 7047973, 7047974, 7047975, 7047976, 7047977, 7047978, 7047979, 7047980, 7047981, 7047982, 7047983, 7047984 Original log message: Adding full bibliography for 7047971--7047984.cif.	7047984.cif
211817	2018-11-07	cif/ Adding structures of 7047971, 7047972, 7047973, 7047974, 7047975, 7047976, 7047977, 7047978, 7047979, 7047980, 7047981, 7047982, 7047983, 7047984 via cif-deposit CGI script.	7047984.cif