Crystallography Open Database

Information card for entry 7048003

Preview

Coordinates	7048003.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H49 N2 Ni O P
Calculated formula	C35 H49 N2 Ni O P
Title of publication	A comparative analysis of hydrosilative amide reduction catalyzed by first-row transition metal (Mn, Fe, Co, and Ni) N-phosphinoamidinate complexes.
Authors of publication	Macaulay, Casper M.; Ogawa, Takahiko; McDonald, Robert; Sydora, Orson L.; Stradiotto, Mark; Turculet, Laura
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	26
Pages of publication	9581 - 9587
a	8.6286 ± 0.0003 Å
b	11.7724 ± 0.0004 Å
c	17.2358 ± 0.0006 Å
α	86.1898 ± 0.0004°
β	79.796 ± 0.0004°
γ	72.2523 ± 0.0004°
Cell volume	1640.96 ± 0.1 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0395
Residual factor for significantly intense reflections	0.0345
Weighted residual factors for significantly intense reflections	0.0908
Weighted residual factors for all reflections included in the refinement	0.0944
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224061 (current)	2019-11-07	cif/ Updating files of 7048002, 7048003 Original log message: Adding full bibliography for 7048002--7048003.cif.	7048003.cif
211839	2018-11-08	cif/ Adding structures of 7048002, 7048003 via cif-deposit CGI script.	7048003.cif