Crystallography Open Database

Information card for entry 7048345

Preview

Coordinates	7048345.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H59 B F20 Mg N2
Calculated formula	C65 H59 B F20 Mg N2
Title of publication	Bulky cationic β-diketiminate magnesium complexes.
Authors of publication	Friedrich, Alexander; Pahl, Jürgen; Elsen, Holger; Harder, Sjoerd
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	17
Pages of publication	5560 - 5568
a	17.6212 ± 0.0004 Å
b	17.7017 ± 0.0005 Å
c	19.053 ± 0.0004 Å
α	90°
β	90.265 ± 0.002°
γ	90°
Cell volume	5943 ± 0.2 Å³
Cell temperature	200 ± 0.1 K
Ambient diffraction temperature	200 ± 0.1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0605
Residual factor for significantly intense reflections	0.0479
Weighted residual factors for significantly intense reflections	0.1287
Weighted residual factors for all reflections included in the refinement	0.1426
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224119 (current)	2019-11-07	cif/ Updating files of 7048343, 7048344, 7048345 Original log message: Adding full bibliography for 7048343--7048345.cif.	7048345.cif
212539	2018-12-12	cif/ Adding structures of 7048343, 7048344, 7048345 via cif-deposit CGI script.	7048345.cif