Crystallography Open Database

Information card for entry 7049009

Preview

Coordinates	7049009.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H61 Ni P3 Si4
Calculated formula	C32 H61 Ni P3 Si4
Title of publication	Isolation of two bis(silyl)nickel complexes with Si-Si bond formation in a single-crystal-to-single-crystal fashion.
Authors of publication	Zhang, Sen-Yu; Li, Jie; Zhao, Sheng-Ze; Wang, Shi; Lu, Min-Ming; Li, Yong-Hua; Huang, Wei
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	10
Pages of publication	3433 - 3439
a	11.352 ± 0.002 Å
b	21.355 ± 0.004 Å
c	15.654 ± 0.003 Å
α	90°
β	100.59 ± 0.03°
γ	90°
Cell volume	3730.2 ± 1.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0556
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.1083
Weighted residual factors for all reflections included in the refinement	0.1118
Goodness-of-fit parameter for all reflections included in the refinement	0.955
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
223812 (current)	2019-11-07	cif/ Updating files of 7049008, 7049009 Original log message: Adding full bibliography for 7049008--7049009.cif.	7049009.cif
213631	2019-02-14	cif/ Adding structures of 7049008, 7049009 via cif-deposit CGI script.	7049009.cif