Crystallography Open Database

Information card for entry 7049106

Preview

Coordinates	7049106.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H36 Ni P
Calculated formula	C22 H36 Ni P
Title of publication	Simplified and versatile access to low valent Ni complexes by metal-free reduction of Ni<sup>II</sup> precursors.
Authors of publication	Moser, Emile; Jeanneau, Erwann; Mézailles, Nicolas; Olivier-Bourbigou, Hélène; Breuil, Pierre-Alain R
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	13
Pages of publication	4101 - 4104
a	9.5546 ± 0.001 Å
b	17.1029 ± 0.0015 Å
c	13.375 ± 0.0015 Å
α	90°
β	100 ± 0.01°
γ	90°
Cell volume	2152.4 ± 0.4 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0769
Residual factor for significantly intense reflections	0.0594
Weighted residual factors for all reflections	0.138
Weighted residual factors for significantly intense reflections	0.1096
Weighted residual factors for all reflections included in the refinement	0.138
Goodness-of-fit parameter for all reflections included in the refinement	1.0091
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224278 (current)	2019-11-08	cif/ Updating files of 7049106, 7049107 Original log message: Adding full bibliography for 7049106--7049107.cif.	7049106.cif
213776	2019-02-22	cif/ Adding structures of 7049106, 7049107 via cif-deposit CGI script.	7049106.cif