Crystallography Open Database

Information card for entry 7049351

Preview

Coordinates	7049351.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H44 Al Cl N2 O Si4
Calculated formula	C16 H44 Al Cl N2 O Si4
Title of publication	Grafting of a new bis-silylamido aluminum species on silica: insight from solid-state NMR into interactions with the surface.
Authors of publication	Vancompernolle, Tom; Merle, Nicolas; Capet, Frédéric; Del Rosal, Iker; Laurent, Maron; Delevoye, Laurent; Pourpoint, Frédérique; Gauvin, Régis M
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	16
Pages of publication	5243 - 5252
a	8.3419 ± 0.0004 Å
b	11.3931 ± 0.0005 Å
c	15.5621 ± 0.0007 Å
α	104.962 ± 0.002°
β	93.099 ± 0.002°
γ	109.088 ± 0.002°
Cell volume	1334.69 ± 0.11 Å³
Cell temperature	100.15 K
Ambient diffraction temperature	100.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.038
Residual factor for significantly intense reflections	0.0294
Weighted residual factors for significantly intense reflections	0.074
Weighted residual factors for all reflections included in the refinement	0.079
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
224197 (current)	2019-11-08	cif/ Updating files of 7049351 Original log message: Adding full bibliography for 7049351.cif.	7049351.cif
214201	2019-03-20	cif/ Adding structures of 7049351 via cif-deposit CGI script.	7049351.cif