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Information card for entry 7049525
Preview
| Coordinates | 7049525.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H41 N Ni O3 P2 S |
|---|---|
| Calculated formula | C37 H41 N Ni O3 P2 S |
| Title of publication | Phosphine-promoted ring-opening of benzisothiazolinate ligands at a nickel(ii) centre: a convenient synthesis of Ni(ii)-thiolate complexes. |
| Authors of publication | Al-Jibori, Subhi A; Ali, Samer Hussein; Al-Janabi, Ahmed S; Wagner, Christoph; Hogarth, Graeme |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2019 |
| Journal volume | 48 |
| Journal issue | 17 |
| Pages of publication | 5520 - 5522 |
| a | 15.7991 ± 0.0006 Å |
| b | 14.1552 ± 0.0005 Å |
| c | 16.1484 ± 0.0006 Å |
| α | 90° |
| β | 106.068 ± 0.003° |
| γ | 90° |
| Cell volume | 3470.3 ± 0.2 Å3 |
| Cell temperature | 213 K |
| Ambient diffraction temperature | 213 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.052 |
| Residual factor for significantly intense reflections | 0.0329 |
| Weighted residual factors for significantly intense reflections | 0.0695 |
| Weighted residual factors for all reflections included in the refinement | 0.0759 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 224091 (current) | 2019-11-07 | cif/ Updating files of 7049523, 7049524, 7049525 Original log message: Adding full bibliography for 7049523--7049525.cif. |
7049525.cif |
| 214409 | 2019-03-29 | cif/ Adding structures of 7049523, 7049524, 7049525 via cif-deposit CGI script. |
7049525.cif |
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Users of the data should acknowledge the original authors of the
structural data.