Crystallography Open Database

Information card for entry 7049549

Preview

Coordinates	7049549.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H48 Co2 Cu3 Mo10 N8 O50
Calculated formula	C32 H48 Co2 Cu3 Mo10 N8 O50
Title of publication	Syntheses, structures and catalytic properties of Evans-Showell-type polyoxometalate-based 3D metal-organic complexes constructed from the semi-rigid bis(pyridylformyl)piperazine ligand and transition metals.
Authors of publication	Li, Feng-Cai; Tan, Li-Kun; Li, Xi-Li; Kong, Hua-Jie; Ge, Li-Ming; Yue, Ling-Yu; Han, Li-Feng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	17
Pages of publication	5831 - 5841
a	12.1598 ± 0.0005 Å
b	14.1021 ± 0.0006 Å
c	23.8608 ± 0.0012 Å
α	78.079 ± 0.004°
β	82.282 ± 0.004°
γ	83.825 ± 0.003°
Cell volume	3953.6 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	298.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1279
Residual factor for significantly intense reflections	0.0923
Weighted residual factors for significantly intense reflections	0.2229
Weighted residual factors for all reflections included in the refinement	0.2481
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224117 (current)	2019-11-07	cif/ Updating files of 7049549, 7049550 Original log message: Adding full bibliography for 7049549--7049550.cif.	7049549.cif
214456	2019-04-03	cif/ Adding structures of 7049549, 7049550 via cif-deposit CGI script.	7049549.cif