Crystallography Open Database

Information card for entry 7049791

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Structure parameters

Formula	C72 H70 Ag B F24 N4
Calculated formula	C72 H70 Ag B F24 N4
Title of publication	A d<sup>10</sup> Ag(i) amine-borane σ-complex and comparison with a d<sup>8</sup> Rh(i) analogue: structures on the η<sup>1</sup> to η<sup>2</sup>:η<sup>2</sup> continuum.
Authors of publication	Johnson, Alice; Martínez-Martínez, Antonio J; Macgregor, Stuart A.; Weller, Andrew S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	26
Pages of publication	9776 - 9781
a	17.4613 ± 0.0002 Å
b	17.6877 ± 0.0001 Å
c	24.9895 ± 0.0002 Å
α	90°
β	107.062 ± 0.001°
γ	90°
Cell volume	7378.33 ± 0.12 Å³
Cell temperature	150.01 ± 0.12 K
Ambient diffraction temperature	150.01 ± 0.12 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0526
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.126
Weighted residual factors for all reflections included in the refinement	0.1323
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301850 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 7/04/ Each referenced PubChem compound corresponds to the full crystal structure.	7049791.cif
224059	2019-11-07	cif/ Updating files of 7049789, 7049790, 7049791, 7049792, 7049793, 7049794 Original log message: Adding full bibliography for 7049789--7049794.cif.	7049791.cif
214729	2019-04-24	cif/ Adding structures of 7049789, 7049790, 7049791, 7049792, 7049793, 7049794 via cif-deposit CGI script.	7049791.cif