Crystallography Open Database

Information card for entry 7052543

Preview

Coordinates	7052543.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H31 Cl3 N2 Ni O
Calculated formula	C23 H31 Cl3 N2 Ni O
Title of publication	Synthesis, characterisation and ethylene oligomerization behaviour of N-(2-substituted-5,6,7-trihydroquinolin-8-ylidene)arylaminonickel dichlorides
Authors of publication	Yu, Jiangang; Hu, Xinquan; Zeng, Yanning; Zhang, Liping; Ni, Caihua; Hao, Xiang; Sun, Wen-Hua
Journal of publication	New Journal of Chemistry
Year of publication	2011
Journal volume	35
Journal issue	1
Pages of publication	178
a	11.597 ± 0.002 Å
b	17.402 ± 0.004 Å
c	12.326 ± 0.003 Å
α	90°
β	99.83 ± 0.03°
γ	90°
Cell volume	2451 ± 0.9 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.1587
Weighted residual factors for significantly intense reflections	0.3174
Weighted residual factors for all reflections included in the refinement	0.333
Goodness-of-fit parameter for all reflections included in the refinement	1.412
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180079 (current)	2016-03-26	cif/7/05/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/05/25.	7052543.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7052543.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7052543.cif
14948	2011-03-12	../uploads/cif-deposit/cod/cif Adding structures of 7052542, 7052543, 7052544, 7052545 via cif-deposit CGI script.	7052543.cif