Crystallography Open Database

Information card for entry 7052730

Preview

Coordinates	7052730.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C169 H157 Ag8 Cl27 Fe8 P4 Se8
Calculated formula	C169 H148 Ag8 Cl27 Fe8 P4 Se8
Title of publication	A ferrocenylmethylselenolate complex of Ag(i): preparation of the polyferrocenyl cluster [Ag8(SeCH2Fc)8(PPh3)4] from the new silylated reagent FcCH2SeSiMe3
Authors of publication	Ahmar, Siawash; Nitschke, Christian; Vijayaratnam, Niranjan; MacDonald, Daniel G.; Fenske, Dieter; Corrigan, John F.
Journal of publication	New Journal of Chemistry
Year of publication	2011
Journal volume	35
Journal issue	10
Pages of publication	2013
a	29.884 ± 0.0006 Å
b	44.24 ± 0.0007 Å
c	22.015 ± 0.0005 Å
α	90°
β	130.463 ± 0.001°
γ	90°
Cell volume	22144.1 ± 0.8 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1537
Residual factor for significantly intense reflections	0.0791
Weighted residual factors for significantly intense reflections	0.2319
Weighted residual factors for all reflections included in the refinement	0.2922
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180081 (current)	2016-03-26	cif/7/05/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/05/27.	7052730.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7052730.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7052730.cif
28140	2011-10-13	../uploads/cif-deposit/cod/cif Adding structures of 7052728, 7052729, 7052730 via cif-deposit CGI script.	7052730.cif