Crystallography Open Database

Information card for entry 7055036

Preview

Coordinates	7055036.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H24 Cl Cu N3 O6
Calculated formula	C19 H24 Cl Cu N3 O6
SMILES	[Cu]1234Oc5ccccc5C=[N]2CCCC[N]4(CC[OH]1)Cc1[n]3cccc1.Cl(=O)(=O)(=O)[O-]
Title of publication	Probing the effect of arm length and inter- and intramolecular interactions in the formation of Cu(ii) complexes of Schiff base ligands derived from some unsymmetrical tripodal amines
Authors of publication	Keypour, Hassan; Shayesteh, Maryam; Salehzadeh, Sadegh; Dhers, Sébastien; Maleki, Farahnaz; Ünver, Hüseyin; Dilek, Nefise
Journal of publication	New J. Chem.
Year of publication	2015
Journal volume	39
Journal issue	9
Pages of publication	7429
a	11.5021 ± 0.0003 Å
b	18.7307 ± 0.0005 Å
c	20.7277 ± 0.0007 Å
α	90°
β	95.504 ± 0.001°
γ	90°
Cell volume	4445 ± 0.2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0504
Residual factor for significantly intense reflections	0.0456
Weighted residual factors for significantly intense reflections	0.1319
Weighted residual factors for all reflections included in the refinement	0.1359
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
155214 (current)	2015-09-08	cif/ Updating files of 7055035, 7055036, 7055037, 7055038, 7055039 Original log message: Adding full bibliography for 7055035--7055039.cif.	7055036.cif
152659	2015-07-31	cif/ Adding structures of 7055035, 7055036, 7055037, 7055038, 7055039 via cif-deposit CGI script.	7055036.cif