Crystallography Open Database

Information card for entry 7055620

Preview

Coordinates	7055620.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H26 N7 Ni O15 Tb
Calculated formula	C28 H26 N7 Ni O15 Tb
Title of publication	Nine self-assembled nickel(ii)‒lanthanide(iii) heterometallic complexes constructed from a Salamo-type bisoxime and bearing a N- or O-donor auxiliary ligand: syntheses, structures and magnetic properties
Authors of publication	Dong, Wen-Kui; Ma, Jian-Chun; Zhu, Li-Chun; Zhang, Yang
Journal of publication	New J. Chem.
Year of publication	2016
Journal volume	40
Journal issue	8
Pages of publication	6998
a	10.2398 ± 0.0004 Å
b	20.6747 ± 0.0007 Å
c	15.2449 ± 0.0005 Å
α	90°
β	92.096 ± 0.003°
γ	90°
Cell volume	3225.3 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0419
Residual factor for significantly intense reflections	0.041
Weighted residual factors for significantly intense reflections	0.1026
Weighted residual factors for all reflections included in the refinement	0.1038
Goodness-of-fit parameter for all reflections included in the refinement	1.078
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
185618 (current)	2016-08-07	cif/ Updating files of 7055617, 7055618, 7055619, 7055620, 7055621, 7055622, 7055623, 7055624, 7055625 Original log message: Adding full bibliography for 7055617--7055625.cif.	7055620.cif
183408	2016-06-11	cif/ Adding structures of 7055617, 7055618, 7055619, 7055620, 7055621, 7055622, 7055623, 7055624, 7055625 via cif-deposit CGI script.	7055620.cif