Crystallography Open Database

Information card for entry 7055817

Preview

Coordinates	7055817.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43.5 H104.1 N14.5 O77.8 P2 Pb3 W18
Calculated formula	C43.5 H72.5 N14.5 O77.8 P2 Pb3 W18
Title of publication	Complexes of non-lacunary Keggin- and Dawson-type polyoxometalates with Pb(ii): formation of 1D coordination polymers with different bonding modes
Authors of publication	Udalova, Liubov I.; Adonin, Sergey A.; Abramov, Pavel A.; Korolkov, Ilya V.; Yunoshev, Alexander S.; Plyusnin, Pavel E.; Sokolov, Maxim N.
Journal of publication	New J. Chem.
Year of publication	2016
Journal volume	40
Journal issue	12
Pages of publication	9981
a	27.4927 ± 0.0006 Å
b	17.8801 ± 0.0006 Å
c	25.0895 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	12333.3 ± 0.6 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	7
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.068
Residual factor for significantly intense reflections	0.0475
Weighted residual factors for significantly intense reflections	0.0999
Weighted residual factors for all reflections included in the refinement	0.1102
Goodness-of-fit parameter for all reflections included in the refinement	1.102
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
190240 (current)	2017-01-09	cif/ Updating files of 7055816, 7055817 Original log message: Adding full bibliography for 7055816--7055817.cif.	7055817.cif
187253	2016-10-11	cif/ Adding structures of 7055816, 7055817 via cif-deposit CGI script.	7055817.cif