#------------------------------------------------------------------------------ #$Date: 2021-03-05 04:15:59 +0200 (Fri, 05 Mar 2021) $ #$Revision: 262678 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/06/02/7060224.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7060224 loop_ _publ_author_name 'Giorgi, Luca' 'Ambrosi, Gianluca' 'Paderni, Daniele' 'Conti, Luca' 'Amatori, Stefano' 'Romagnoli, Francesca' 'Rossi, Patrizia' 'Formica, Mauro' 'Macedi, Eleonora' 'Giorgi, Claudia' 'Paoli, Paola' 'Fanelli, Mirco' 'Fusi, Vieri' _publ_section_title ; Bis-maltol-polyamine family: structural modifications at strategic positions. Synthesis, coordination and antineoplastic activity of two new ligands ; _journal_issue 5 _journal_name_full 'New Journal of Chemistry' _journal_page_first 2659 _journal_page_last 2669 _journal_paper_doi 10.1039/D0NJ05327A _journal_volume 45 _journal_year 2021 _chemical_formula_moiety '(C18 H26 O6 N2) 2(H2O) 2(ClO4-))' _chemical_formula_sum 'C18 H30 Cl2 N2 O16' _chemical_formula_weight 601.34 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens difmap _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2020-12-19 deposited with the CCDC. 2020-12-30 downloaded from the CCDC. ; _cell_angle_alpha 104.296(9) _cell_angle_beta 104.670(8) _cell_angle_gamma 105.419(8) _cell_formula_units_Z 1 _cell_length_a 8.0335(7) _cell_length_b 8.3743(8) _cell_length_c 10.4076(10) _cell_measurement_reflns_used 3301 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.1830 _cell_measurement_theta_min 4.7600 _cell_volume 614.77(12) _computing_cell_refinement 'CrysAlisPro 1.171.38.41r (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.41r (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.41r (Rigaku OD, 2015)' _computing_molecular_graphics 'Mercury (Macrae, 2008)' _computing_publication_material 'Parst-97 (Nardelli, 1995)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SIR-2004 (Burla, 2005)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.847 _diffrn_measurement_device_type 'Xcalibur, Sapphire3' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_unetI/netI 0.0434 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.847 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_number 2905 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.847 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.532 _diffrn_reflns_theta_min 4.255 _diffrn_source 'fine-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 0.348 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.97714 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.41r (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.624 _exptl_crystal_description prism _exptl_crystal_F_000 314 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.18 _refine_diff_density_max 0.515 _refine_diff_density_min -0.418 _refine_diff_density_rms 0.087 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.188 _refine_ls_hydrogen_treatment refxyz _refine_ls_matrix_type full _refine_ls_number_parameters 218 _refine_ls_number_reflns 2905 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.188 _refine_ls_R_factor_all 0.0606 _refine_ls_R_factor_gt 0.0505 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0452P)^2^+0.8705P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1325 _refine_ls_wR_factor_ref 0.1371 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2491 _reflns_number_total 2905 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0nj05327a2.cif _cod_data_source_block Me-Malten _cod_depositor_comments 'Adding full bibliography for 7060224.cif.' _cod_original_cell_volume 614.77(11) _cod_database_code 7060224 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL nuovo1.ins shelx.res created by SHELXL-2018/3 at 12:06:48 on 19-Dec-2020 CELL 0.71073 8.0335 8.3743 10.4076 104.296 104.670 105.419 ZERR 2.00 0.0007 0.0008 0.0010 0.009 0.008 0.008 LATT 1 SFAC C H N O CL UNIT 18 30 2 16 2 MERG 2 ACTA BOND $H L.S. 300 TEMP -173.00 WGHT 0.045200 0.870500 BASF 0.18538 FVAR 1.10327 O1 4 0.924903 0.215671 0.586437 11.00000 0.01267 0.02176 = 0.01364 0.01023 0.00574 0.00993 H1O 2 1.004697 0.192126 0.609909 11.00000 -1.20000 O2 4 1.205203 0.226800 0.480701 11.00000 0.01118 0.02458 = 0.01594 0.00777 0.00709 0.01004 O3 4 0.773449 0.345203 0.286141 11.00000 0.01277 0.01447 = 0.01391 0.00754 0.00766 0.00650 N1 3 0.457576 0.136795 0.381809 11.00000 0.00747 0.01350 = 0.01195 0.00505 0.00515 0.00483 H1N 2 0.375566 0.164801 0.416634 11.00000 -1.20000 C1 1 0.908521 0.347690 0.231421 11.00000 0.01694 0.01127 = 0.01617 0.00532 0.01126 0.00563 C2 1 1.055993 0.310350 0.293211 11.00000 0.01337 0.01245 = 0.01502 0.00394 0.00942 0.00410 H2 2 1.143324 0.317355 0.257549 11.00000 -1.20000 C3 1 1.073318 0.263702 0.416388 11.00000 0.00946 0.00941 = 0.01494 0.00157 0.00505 0.00209 C4 1 0.922196 0.258786 0.469952 11.00000 0.01116 0.00991 = 0.01177 0.00410 0.00519 0.00288 C5 1 0.780478 0.299781 0.404018 11.00000 0.01165 0.00655 = 0.01235 0.00326 0.00593 0.00169 C6 1 0.620067 0.306009 0.449484 11.00000 0.01088 0.01137 = 0.01326 0.00530 0.00596 0.00489 H6A 2 0.653392 0.337842 0.546977 11.00000 -1.20000 H6B 2 0.576680 0.391934 0.423714 11.00000 -1.20000 C7 1 0.489818 -0.014075 0.423179 11.00000 0.01200 0.01039 = 0.01479 0.00470 0.00621 0.00462 H7A 2 0.381742 -0.113673 0.366040 11.00000 -1.20000 H7B 2 0.596287 -0.024757 0.406916 11.00000 -1.20000 C15 1 0.389186 0.086268 0.224055 11.00000 0.01298 0.02131 = 0.01011 0.00605 0.00227 0.00612 H15A 2 0.382076 0.191294 0.204196 11.00000 -1.50000 H15B 2 0.473669 0.041388 0.194474 11.00000 -1.50000 H15C 2 0.274497 0.004145 0.201674 11.00000 -1.50000 C16 1 0.873032 0.392723 0.100584 11.00000 0.02801 0.02434 = 0.02155 0.01545 0.01577 0.01522 H16A 2 0.949888 0.364613 0.042664 11.00000 -1.50000 H16B 2 0.750197 0.321478 0.033653 11.00000 -1.50000 H16C 2 0.889597 0.501992 0.117602 11.00000 -1.50000 O1W 4 1.545025 0.443345 0.741434 11.00000 0.02274 0.02260 = 0.02132 0.00597 0.01256 0.00387 H1WA 2 1.577141 0.495921 0.835145 11.00000 -1.50000 H1WB 2 1.452060 0.377944 0.720267 11.00000 -1.50000 CL1 5 1.237543 0.159915 0.882426 11.00000 0.01359 0.01132 = 0.01099 0.00290 0.00470 0.00443 O11 4 1.216312 0.142410 0.735849 11.00000 0.02061 0.02847 = 0.01214 0.00983 0.00648 0.01283 O12 4 1.367945 0.331662 0.969113 11.00000 0.03574 0.01457 = 0.02693 -0.00044 0.00431 -0.00060 O13 4 1.305183 0.028524 0.915837 11.00000 0.03089 0.01974 = 0.01809 0.00852 0.00754 0.01537 O14 4 1.064934 0.139970 0.901236 11.00000 0.02412 0.04565 = 0.04118 0.02042 0.02352 0.01797 HKLF 5 REM nuovo1.ins REM wR2 = 0.1371, GooF = S = 1.188, Restrained GooF = 1.188 for all data REM R1 = 0.0505 for 2491 Fo > 4sig(Fo) and 0.0606 for all 2905 data REM 218 parameters refined using 0 restraints END WGHT 0.0471 0.7528 REM Highest difference peak 0.515, deepest hole -0.418, 1-sigma level 0.087 Q1 1 1.3380 0.3235 0.8787 11.00000 0.05 0.52 Q2 1 1.1197 0.0104 0.8894 11.00000 0.05 0.49 Q3 1 0.9947 0.2623 0.4418 11.00000 0.05 0.42 Q4 1 1.0061 0.3759 0.2871 11.00000 0.05 0.41 Q5 1 1.2743 0.2891 0.9808 11.00000 0.05 0.38 Q6 1 0.8248 0.2217 0.4055 11.00000 0.05 0.38 Q7 1 1.0539 0.2879 0.3521 11.00000 0.05 0.37 Q8 1 0.7174 0.3208 0.4421 11.00000 0.05 0.34 Q9 1 1.4524 0.4603 0.8905 11.00000 0.05 0.33 Q10 1 0.1422 -0.0526 0.2515 11.00000 0.05 0.32 Q11 1 1.2386 0.0095 0.8426 11.00000 0.05 0.31 Q12 1 0.2483 -0.0835 0.2239 11.00000 0.05 0.31 Q13 1 0.9955 0.1437 0.1208 11.00000 0.05 0.31 Q14 1 1.1959 -0.0990 0.9215 11.00000 0.05 0.30 Q15 1 0.4854 0.0747 0.4188 11.00000 0.05 0.30 Q16 1 0.8786 0.4751 0.4006 11.00000 0.05 0.29 Q17 1 0.8494 0.3393 0.2606 11.00000 0.05 0.29 Q18 1 1.2968 -0.0054 1.0026 11.00000 0.05 0.29 Q19 1 1.2961 0.0453 0.8542 11.00000 0.05 0.29 Q20 1 0.5000 0.0000 0.5000 10.50000 0.05 0.28 ; _shelx_res_checksum 30598 _shelx_hkl_file ; 2 0 0 102.91 2.80 1 3 0 0 253.12 5.21 1 4 0 0 322.50 14.54 1 5 0 0 28.55 5.34 1 6 0 0 1151.83 34.08 1 7 0 0 1278.92 27.50 1 8 0 0 5.05 2.82 1 -9 0 8 62.96 10.77 -2 9 0 0 62.96 10.77 1 -9 1 0 10.96 4.59 1 -8 1 0 3.00 4.47 1 -7 1 0 12.33 5.09 1 -6 1 0 118.55 8.49 1 -5 1 0 123.08 7.14 1 -4 1 0 103.39 4.60 1 -3 1 0 206.18 4.37 1 -2 1 0 1283.46 23.76 1 1 1 0 1866.57 14.60 1 2 1 0 21.40 1.69 1 3 1 0 390.50 8.73 1 4 1 0 736.47 16.10 1 5 1 0 177.68 8.98 1 6 1 0 163.59 9.47 1 7 1 0 66.34 7.69 1 -8 -1 8 12.11 7.38 -2 8 1 0 12.11 7.38 1 9 1 0 47.75 10.45 1 -9 2 0 28.89 8.61 1 -8 2 0 148.50 8.59 1 -7 2 0 217.84 9.40 1 -6 2 0 1049.84 15.93 1 -5 2 0 277.41 5.91 1 -4 2 0 633.54 12.55 1 -3 2 1 404.59 4.22 -2 -3 2 0 404.59 4.22 1 -2 2 0 1098.51 13.72 1 -1 2 0 474.83 4.08 1 0 2 0 3361.21 50.49 1 1 2 015488.46 98.70 1 2 2 0 24.26 2.12 1 3 2 0 162.29 6.26 1 4 2 0 457.13 11.46 1 5 2 0 1205.94 24.08 1 -6 -2 7 235.00 15.77 -2 6 2 0 235.00 15.77 1 7 2 0 986.18 53.38 1 8 2 0 279.01 15.55 1 -9 3 0 136.49 11.77 1 -8 3 0 12.72 4.81 1 -7 3 0 13.16 3.54 1 -6 3 0 469.45 7.95 1 -5 3 0 226.96 30.30 1 -4 3 1 105.29 2.94 -2 -4 3 0 105.29 2.94 1 -3 3 0 641.59 5.36 1 -2 3 0 34.00 1.28 1 -1 3 0 6.48 1.08 1 0 3 0 50.09 3.07 1 1 3 0 259.60 6.32 1 2 3 0 167.90 6.37 1 3 3 0 146.60 6.49 1 4 3 0 672.46 14.90 1 -5 -3 7 102.26 7.45 -2 5 3 0 102.26 7.45 1 6 3 0 28.53 4.81 1 7 3 0 13.36 4.64 1 8 3 0 1.52 3.57 1 -9 4 0 306.27 17.29 1 -8 4 0 7.14 4.00 1 -7 4 0 178.85 7.90 1 -6 4 2 22.43 1.78 -2 -6 4 0 22.43 1.78 1 -5 4 0 862.19 8.94 1 -4 4 0 240.59 4.60 1 -3 4 0 2337.06 16.92 1 -2 4 0 2.07 1.10 1 -1 4 0 291.66 6.92 1 0 4 0 270.96 11.43 1 1 4 0 446.16 13.82 1 2 4 0 604.46 14.31 1 -3 -4 6 593.00 15.39 -2 3 4 0 593.00 15.39 1 4 4 0 527.21 21.05 1 5 4 0 6.33 3.52 1 6 4 0 267.99 15.65 1 7 4 0 107.16 10.40 1 8 4 0 286.24 24.37 1 -9 5 0 51.02 9.97 1 -8 5 0 96.81 9.36 1 -7 5 2 183.71 13.13 -2 -7 5 0 183.71 13.13 1 -6 5 0 6.13 2.03 1 -5 5 0 1369.67 11.82 1 -4 5 0 368.57 5.94 1 -3 5 0 289.24 5.94 1 -2 5 0 8.66 1.57 1 -1 5 0 81.81 4.97 1 0 5 0 3.98 2.68 1 1 5 0 190.29 16.59 1 -2 -5 6 31.51 4.89 -2 2 5 0 31.51 4.89 1 3 5 0 69.17 6.25 1 4 5 0 4.94 4.71 1 5 5 0 37.84 5.51 1 6 5 0 19.85 7.89 1 -9 6 3 38.19 8.24 -2 -9 6 0 38.19 8.24 1 -8 6 0 331.67 13.77 1 -7 6 0 66.59 6.25 1 -6 6 0 113.17 4.90 1 -5 6 0 69.58 4.58 1 -4 6 0 144.43 4.36 1 -3 6 0 154.27 4.86 1 -2 6 0 1640.13 17.43 1 -1 6 0 98.62 6.58 1 0 -6 5 740.59 16.66 -2 0 6 0 740.59 16.66 1 1 6 0 12.89 4.39 1 2 6 0 16.43 4.80 1 3 6 0 22.82 5.30 1 4 6 0 332.47 17.72 1 5 6 0 164.16 13.61 1 -9 7 0 41.96 7.40 1 -8 7 0 20.04 3.98 1 -7 7 0 73.83 5.41 1 -6 7 0 54.03 5.23 1 -5 7 0 2.87 2.00 1 -4 7 0 837.68 11.34 1 -3 7 0 134.17 5.02 1 -2 7 0 7.09 4.16 1 1 -7 5 86.79 5.00 -2 -1 7 0 86.79 5.00 1 0 7 0 255.60 11.66 1 1 7 0 146.40 8.73 1 2 7 0 15.34 4.84 1 3 7 0 7.26 6.16 1 4 7 0 40.77 7.86 1 -9 8 0 3.88 4.43 1 -8 8 0 288.03 13.69 1 -7 8 0 35.11 6.25 1 -6 8 0 2.70 2.54 1 -5 8 0 164.18 7.40 1 -4 8 0 55.83 5.05 1 -3 8 0 294.75 9.41 1 -2 8 0 239.35 10.32 1 -1 8 0 447.86 14.96 1 0 8 0 3.96 3.16 1 1 8 0 71.99 6.86 1 2 8 0 10.76 3.80 1 3 8 0 7.69 4.63 1 -8 9 0 161.94 17.99 1 -7 9 0 3.54 4.14 1 -6 9 0 64.93 7.93 1 -5 9 0 6.90 3.52 1 4 -9 4 100.24 7.38 -2 -4 9 0 100.24 7.38 1 -3 9 0 57.90 8.29 1 -2 9 0 67.47 9.64 1 -1 9 0 13.05 3.53 1 0 9 0 -0.02 3.28 1 1 9 0 187.01 11.59 1 -7 10 0 199.01 20.60 1 -6 10 0 58.14 8.32 1 5 -10 4 16.64 5.00 -2 -5 10 0 16.64 5.00 1 -4 10 0 61.38 6.39 1 -3 10 0 34.90 5.26 1 -2 10 0 26.94 5.87 1 -1 10 0 11.11 4.91 1 0 10 0 114.30 15.46 1 -4 11 0 46.20 10.69 1 -3 11 0 26.28 7.90 1 3 -11 1 8.64 6.74 1 4 -11 1 116.82 10.75 1 0 -10 1 57.33 8.21 1 1 -10 1 41.21 5.54 1 2 -10 1 23.03 4.26 1 3 -10 1 91.48 7.66 1 4 -10 1 23.89 8.38 1 5 -10 3 225.23 11.74 -2 5 -10 1 225.23 11.74 1 6 -10 1 134.09 17.62 1 -2 -9 1 57.25 12.44 1 -1 -9 1 26.15 4.80 1 0 -9 1 231.06 11.98 1 1 -9 1 32.38 4.62 1 2 -9 1 235.14 11.01 1 3 -9 1 56.55 9.40 1 4 -9 3 2.22 2.64 -2 4 -9 1 2.22 2.64 1 5 -9 1 138.60 7.49 1 6 -9 1 6.81 2.91 1 7 -9 1 110.76 10.54 1 -3 -8 1 161.25 11.00 1 -2 -8 1 10.87 3.48 1 -1 -8 1 89.77 7.63 1 0 -8 1 295.64 12.51 1 1 -8 1 198.75 10.05 1 2 -8 1 267.96 10.79 1 3 -8 1 39.45 3.86 1 4 -8 1 262.14 8.60 1 5 -8 1 57.55 4.98 1 6 -8 1 207.33 10.32 1 7 -8 1 103.68 7.45 1 8 -8 1 66.18 7.39 1 9 -8 1 69.96 12.70 1 -4 -7 1 49.00 6.98 1 -3 -7 1 254.45 12.67 1 -2 -7 1 26.51 4.66 1 -1 -7 1 87.57 11.26 1 0 -7 1 51.06 6.99 1 1 -7 4 1954.40 22.02 -2 1 -7 1 1954.40 22.02 1 2 -7 1 175.47 6.05 1 3 -7 1 277.47 6.77 1 4 -7 1 3.51 1.70 1 5 -7 1 40.55 3.63 1 6 -7 1 87.15 4.83 1 7 -7 1 321.42 10.89 1 8 -7 1 118.95 8.75 1 9 -7 1 26.52 8.44 1 -6 -6 1 126.76 16.73 1 -5 -6 1 41.93 9.51 1 -4 -6 1 24.02 5.64 1 -3 -6 1 2.24 3.54 1 -2 -6 1 204.76 9.83 1 -1 -6 1 114.63 8.65 1 0 -6 4 527.93 13.79 -2 0 -6 1 527.93 13.79 1 1 -6 1 790.88 12.37 1 2 -6 1 498.06 8.99 1 3 -6 1 63.73 3.12 1 4 -6 1 117.03 4.56 1 5 -6 1 525.99 8.80 1 6 -6 1 293.53 7.70 1 7 -6 1 252.56 11.23 1 8 -6 1 67.19 8.20 1 -9 6 4 62.27 7.90 -2 9 -6 1 62.27 7.90 1 -7 -5 1 78.32 13.16 1 -6 -5 1 18.52 6.72 1 -5 -5 1 141.20 11.04 1 -4 -5 1 5.40 10.44 1 -3 -5 1 80.05 7.47 1 -2 -5 5 378.37 14.70 -2 -2 -5 1 378.37 14.70 1 -1 -5 1 458.39 16.59 1 0 -5 1 6.98 2.47 1 1 -5 1 17.57 1.90 1 2 -5 1 1116.53 17.28 1 3 -5 1 630.57 7.07 1 4 -5 1 221.63 5.02 1 5 -5 1 42.57 2.48 1 6 -5 1 928.28 15.42 1 -7 5 3 42.94 6.33 -2 7 -5 1 42.94 6.33 1 8 -5 1 381.94 18.50 1 9 -5 1 5.25 10.53 1 -8 -4 1 86.29 13.63 1 -7 -4 1 21.01 6.77 1 -6 -4 1 -0.55 2.97 1 -5 -4 1 805.81 16.59 1 -4 -4 1 185.31 9.12 1 -3 -4 5 105.28 7.96 -2 -3 -4 1 105.28 7.96 1 -2 -4 1 963.91 30.86 1 -1 -4 1 1.36 2.27 1 0 -4 1 31.24 3.07 1 1 -4 1 963.11 8.99 1 2 -4 1 2925.34 21.93 1 3 -4 1 55.66 2.02 1 4 -4 1 21.93 1.72 1 5 -4 1 585.08 9.31 1 -6 4 3 312.66 10.39 -2 6 -4 1 312.66 10.39 1 7 -4 1 315.29 11.21 1 8 -4 1 120.20 10.44 1 9 -4 1 17.40 8.43 1 -8 -3 1 11.32 5.09 1 -7 -3 1 54.03 7.03 1 -6 -3 1 225.06 10.17 1 -5 -3 6 21.56 3.34 -2 -5 -3 1 21.56 3.34 1 -4 -3 1 395.68 10.09 1 -3 -3 1 65.60 3.94 1 -2 -3 1 467.28 12.46 1 -1 -3 1 163.04 10.22 1 0 -3 1 503.60 7.26 1 1 -3 1 1.05 0.86 1 2 -3 1 196.28 3.07 1 3 -3 1 207.22 3.35 1 -4 3 2 1347.07 11.56 -2 4 -3 1 1347.07 11.56 1 5 -3 1 237.98 11.59 1 6 -3 1 44.81 4.33 1 7 -3 1 506.60 14.40 1 8 -3 1 38.22 4.65 1 9 -3 1 63.13 8.31 1 -8 -2 1 397.98 15.71 1 -7 -2 1 64.46 5.63 1 -6 -2 6 237.95 11.08 -2 -6 -2 1 237.95 11.08 1 -5 -2 1 93.83 7.44 1 -4 -2 1 2695.07 27.42 1 -3 -2 1 28.78 2.64 1 -2 -2 1 109.30 3.74 1 -1 -2 1 262.37 4.32 1 0 -2 1 88.75 2.43 1 1 -2 1 835.78 4.78 1 2 -2 1 6074.16 37.85 1 -3 2 2 384.26 5.59 -2 3 -2 1 384.26 5.59 1 4 -2 1 213.21 5.55 1 5 -2 1 3.44 5.76 1 6 -2 1 27.22 4.10 1 7 -2 1 67.49 6.89 1 8 -2 1 117.03 9.48 1 9 -2 1 135.29 17.04 1 -9 -1 1 32.10 8.49 1 -8 -1 7 3.28 2.14 -2 -8 -1 1 3.28 2.14 1 -7 -1 1 50.28 6.13 1 -6 -1 1 371.79 18.55 1 -5 -1 1 309.71 12.40 1 -4 -1 1 368.97 9.41 1 -3 -1 1 412.32 6.72 1 -2 -1 1 2.69 1.77 1 2 -1 1 537.02 11.14 1 3 -1 1 94.82 5.24 1 4 -1 1 141.84 7.32 1 5 -1 1 345.59 12.60 1 6 -1 1 27.84 4.59 1 7 -1 1 92.31 10.98 1 8 -1 1 85.99 11.44 1 9 -1 1 26.57 8.46 1 -9 0 7 10.86 4.12 -2 -9 0 1 10.86 4.12 1 -8 0 1 451.24 17.59 1 -7 0 1 897.64 22.67 1 -6 0 1 200.71 13.79 1 -5 0 1 59.68 6.77 1 -4 0 1 2.61 1.69 1 -3 0 1 6020.93 60.59 1 -2 0 1 4626.11 33.16 1 2 0 1 13.21 2.51 1 3 0 1 622.18 13.62 1 4 0 1 1.05 2.36 1 5 0 1 0.06 3.47 1 6 0 1 134.89 8.37 1 7 0 1 9.70 3.18 1 8 0 1 16.40 7.30 1 -9 0 9 38.40 9.12 -2 9 0 1 38.40 9.12 1 -10 1 1 97.98 14.51 1 -9 1 1 55.14 7.43 1 -8 1 1 0.65 3.03 1 -7 1 1 478.31 20.92 1 -6 1 1 10.87 2.89 1 -5 1 1 1.89 1.28 1 -4 1 1 1468.03 17.69 1 -3 1 1 1564.03 9.89 1 -2 1 1 3265.61 27.63 1 1 1 1 471.97 5.65 1 2 1 1 596.87 8.37 1 3 1 1 3.34 1.76 1 4 1 1 52.01 4.43 1 5 1 1 39.67 4.44 1 6 1 1 398.10 24.07 1 7 1 1 230.98 12.02 1 -8 -1 9 31.19 8.87 -2 8 1 1 31.19 8.87 1 9 1 1 1.44 5.26 1 -9 2 1 180.90 18.52 1 -8 2 1 238.98 14.21 1 -7 2 1 1604.80 33.07 1 -6 2 1 666.24 10.19 1 -5 2 1 569.66 9.97 1 -4 2 1 49.93 1.97 1 -3 2 0 317.32 5.79 -2 -3 2 1 317.32 5.79 1 -2 2 1 647.21 21.82 1 -1 2 111537.44 42.40 1 0 2 1 8300.06 47.24 1 1 2 1 2715.89 15.75 1 2 2 1 2545.35 30.58 1 3 2 1 150.47 6.79 1 4 2 1 122.80 7.00 1 5 2 1 239.19 10.63 1 -6 -2 8 410.45 15.10 -2 6 2 1 410.45 15.10 1 7 2 1 69.60 12.02 1 8 2 1 -0.32 5.11 1 -9 3 1 26.01 14.41 1 -8 3 1 186.56 12.56 1 -7 3 1 87.11 5.42 1 -6 3 1 888.58 8.71 1 -5 3 1 11.29 1.09 1 -4 3 0 49.17 1.87 -2 -4 3 1 49.17 1.87 1 -3 3 1 677.50 5.95 1 -2 3 1 217.29 3.40 1 -1 3 1 28.24 2.07 1 0 3 1 20.33 1.95 1 1 3 1 120.54 6.29 1 2 3 1 9.09 1.92 1 3 3 1 761.89 20.41 1 4 3 1 50.39 12.21 1 -5 -3 8 244.28 12.42 -2 5 3 1 244.28 12.42 1 6 3 1 2.78 4.26 1 7 3 1 39.54 9.38 1 8 3 1 182.76 19.22 1 -9 4 1 3.85 3.89 1 -8 4 1 180.76 12.37 1 -7 4 1 1039.40 21.92 1 -6 4 1 2649.08 22.03 -2 -6 4 1 2649.08 22.03 1 -5 4 1 146.81 20.77 1 -4 4 1 501.92 6.45 1 -3 4 1 103.54 2.62 1 -2 4 1 23.91 1.58 1 -1 4 1 7.18 2.36 1 0 4 1 5267.91 63.75 1 1 4 1 2730.88 34.86 1 2 4 1 3.14 3.05 1 -3 -4 7 205.56 17.43 -2 3 4 1 205.56 17.43 1 4 4 1 53.31 7.65 1 5 4 1 13.50 6.67 1 6 4 1 181.91 13.47 1 7 4 1 595.62 35.21 1 -9 5 1 6.44 4.58 1 -8 5 1 11.01 4.84 1 -7 5 1 698.38 18.30 -2 -7 5 1 698.38 18.30 1 -6 5 1 181.85 8.86 1 -5 5 1 286.66 5.19 1 -4 5 1 1.63 0.73 1 -3 5 1 76.57 2.86 1 -2 5 1 42.58 2.83 1 -1 5 1 592.53 19.58 1 0 5 1 34.41 4.52 1 1 5 1 103.27 6.44 1 -2 -5 7 111.58 7.39 -2 2 5 1 111.58 7.39 1 3 5 1 69.13 6.29 1 4 5 1 31.44 5.26 1 5 5 1 8.17 4.35 1 6 5 1 89.96 14.08 1 -9 6 2 107.41 13.19 -2 -9 6 1 107.41 13.19 1 -8 6 1 14.95 3.78 1 -7 6 1 119.64 6.27 1 -6 6 1 1155.01 25.45 1 -5 6 1 215.60 6.29 1 -4 6 1 227.79 5.40 1 -3 6 1 815.17 12.11 1 -2 6 1 121.88 5.63 1 -1 6 1 410.49 14.80 1 0 -6 6 314.17 33.61 -2 0 6 1 314.17 33.61 1 1 6 1 1093.56 27.32 1 2 6 1 4.07 7.43 1 3 6 1 14.28 4.71 1 4 6 1 70.96 9.16 1 5 6 1 34.54 9.64 1 -9 7 1 148.94 15.30 1 -8 7 1 29.49 5.01 1 -7 7 1 10.34 6.13 1 -6 7 1 309.68 11.28 1 -5 7 1 5.56 1.66 1 -4 7 1 45.91 3.39 1 -3 7 1 3.39 1.65 1 -2 7 1 419.17 10.37 1 1 -7 6 186.58 8.90 -2 -1 7 1 186.58 8.90 1 0 7 1 135.77 20.09 1 1 7 1 26.44 6.12 1 2 7 1 59.26 7.90 1 3 7 1 29.26 6.13 1 -9 8 1 34.84 9.42 1 -8 8 1 11.96 9.06 1 -7 8 1 63.81 7.68 1 -6 8 1 13.68 9.60 1 -5 8 1 227.91 8.58 1 -4 8 1 3.12 2.14 1 -3 8 1 499.15 16.51 1 -2 8 1 545.30 15.65 1 -1 8 1 117.71 7.86 1 0 8 1 63.10 6.31 1 1 8 1 45.37 6.22 1 2 8 1 165.87 13.63 1 -8 9 1 19.65 5.68 1 -7 9 1 -0.22 3.53 1 -6 9 1 4.37 4.16 1 -5 9 1 143.83 11.36 1 4 -9 5 27.24 3.99 -2 -4 9 1 27.24 3.99 1 -3 9 1 14.11 4.19 1 -2 9 1 24.07 4.13 1 -1 9 1 21.27 4.31 1 0 9 1 3.57 4.75 1 1 9 1 61.95 8.60 1 -7 10 1 19.79 8.75 1 -6 10 1 142.06 12.38 1 5 -10 5 70.25 8.80 -2 -5 10 1 70.25 8.80 1 -4 10 1 -1.68 3.57 1 -3 10 1 20.64 4.59 1 -2 10 1 137.96 11.96 1 -1 10 1 68.57 8.78 1 1 -11 2 10.82 7.50 1 3 -11 2 144.40 17.71 1 4 -11 2 113.02 11.03 1 5 -11 2 73.43 12.24 1 0 -10 2 50.92 9.39 1 1 -10 2 14.65 5.24 1 2 -10 2 31.37 4.85 1 3 -10 2 5.22 2.94 1 4 -10 2 110.16 10.03 1 5 -10 2 98.98 8.12 -2 5 -10 2 98.98 8.12 1 6 -10 2 159.02 12.84 1 -2 -9 2 17.57 4.65 1 -1 -9 2 2.01 3.66 1 0 -9 2 140.15 9.54 1 1 -9 2 56.76 5.92 1 2 -9 2 30.99 5.31 1 3 -9 2 287.43 12.95 1 4 -9 2 18.58 3.76 -2 4 -9 2 18.58 3.76 1 5 -9 2 14.71 5.60 1 6 -9 2 210.96 13.80 1 7 -9 2 14.16 5.28 1 -3 -8 2 71.09 7.40 1 -2 -8 2 378.99 15.41 1 -1 -8 2 5.10 4.14 1 0 -8 2 176.37 9.67 1 1 -8 2 51.77 5.48 1 2 -8 2 196.23 9.56 1 3 -8 2 3.53 2.01 1 4 -8 2 3.09 2.09 1 5 -8 2 61.85 4.85 1 6 -8 2 35.18 4.66 1 7 -8 2 108.75 6.91 1 8 -8 2 10.26 3.80 1 9 -8 2 25.00 8.40 1 -5 -7 2 296.44 23.11 1 -4 -7 2 2.21 3.41 1 -3 -7 2 5.09 3.64 1 -2 -7 2 417.55 14.80 1 -1 -7 2 165.41 9.00 1 0 -7 2 222.42 10.28 1 1 -7 3 221.55 9.41 -2 1 -7 2 221.55 9.41 1 2 -7 2 204.57 9.37 1 3 -7 2 4.86 1.63 1 4 -7 2 105.48 5.25 1 5 -7 2 14.64 2.23 1 6 -7 2 22.08 2.85 1 7 -7 2 4.85 5.34 1 8 -7 2 40.47 7.06 1 9 -7 2 1.59 4.76 1 -6 -6 2 111.30 9.46 1 -5 -6 2 41.19 5.63 1 -4 -6 2 6.89 3.33 1 -3 -6 2 251.74 12.08 1 -2 -6 2 154.40 8.60 1 -1 -6 2 1420.42 23.62 1 0 -6 3 374.48 15.72 -2 0 -6 2 374.48 15.72 1 1 -6 2 121.70 5.35 1 2 -6 2 336.56 10.15 1 3 -6 2 325.50 8.27 1 4 -6 2 66.67 2.95 1 5 -6 2 96.32 4.34 1 6 -6 2 124.31 6.13 1 7 -6 2 91.84 11.64 1 8 -6 2 6.05 3.65 1 -9 6 5 -7.25 7.25 -2 9 -6 2 -7.25 7.25 1 -7 -5 2 78.47 11.92 1 -6 -5 2 85.59 7.72 1 -5 -5 2 14.76 4.64 1 -4 -5 2 774.95 19.28 1 -3 -5 2 13.56 3.53 1 -2 -5 4 69.54 5.38 -2 -2 -5 2 69.54 5.38 1 -1 -5 2 190.44 8.22 1 0 -5 2 1134.69 18.08 1 1 -5 2 378.38 8.14 1 2 -5 2 10.41 1.47 1 3 -5 2 1083.98 10.42 1 4 -5 2 79.76 3.63 1 5 -5 2 86.30 4.09 1 6 -5 2 231.71 11.78 1 -7 5 4 103.55 6.87 -2 7 -5 2 103.55 6.87 1 8 -5 2 9.72 5.01 1 9 -5 2 18.27 5.90 1 -8 -4 2 5.52 5.77 1 -7 -4 2 108.26 9.32 1 -6 -4 2 64.18 5.77 1 -5 -4 2 231.67 10.06 1 -4 -4 2 1.25 2.04 1 -3 -4 4 133.23 14.11 -2 -3 -4 2 133.23 14.11 1 -2 -4 2 296.54 9.46 1 -1 -4 2 145.27 6.42 1 0 -4 2 715.22 12.76 1 1 -4 2 33.58 2.36 1 2 -4 2 222.52 3.71 1 3 -4 2 1021.33 8.44 1 4 -4 2 1484.40 16.58 1 5 -4 2 30.39 3.45 1 -6 4 4 186.28 8.39 -2 6 -4 2 186.28 8.39 1 7 -4 2 110.32 8.43 1 8 -4 2 30.26 8.25 1 9 -4 2 41.53 7.35 1 -9 -3 2 4.66 5.92 1 -8 -3 2 5.18 5.69 1 -7 -3 2 160.49 10.55 1 -6 -3 2 580.88 15.76 1 -5 -3 5 417.39 12.48 -2 -5 -3 2 417.39 12.48 1 -4 -3 2 1032.09 17.94 1 -3 -3 2 544.63 12.06 1 -2 -3 2 54.83 3.39 1 -1 -3 2 0.80 2.86 1 0 -3 2 214.81 4.44 1 1 -3 2 4030.00 26.16 1 2 -3 2 194.40 3.15 1 3 -3 2 684.44 6.76 1 -4 3 3 176.67 6.74 -2 4 -3 2 176.67 6.74 1 5 -3 2 74.76 5.09 1 6 -3 2 92.78 6.21 1 7 -3 2 174.18 8.89 1 8 -3 2 281.05 12.29 1 9 -3 2 109.08 13.47 1 -9 -2 2 67.02 11.74 1 -8 -2 2 70.13 10.87 1 -7 -2 2 33.13 14.83 1 -6 -2 5 584.57 14.50 -2 -6 -2 2 584.57 14.50 1 -5 -2 2 183.40 6.72 1 -4 -2 2 117.91 5.73 1 -3 -2 2 496.72 10.30 1 -2 -2 2 74.78 2.17 1 -1 -2 2 429.89 4.40 1 0 -2 2 3850.29 16.94 1 1 -2 2 785.83 5.19 1 2 -2 2 60.72 2.37 1 -3 2 3 127.99 4.03 -2 3 -2 2 127.99 4.03 1 4 -2 2 1.32 2.32 1 5 -2 2 271.97 11.41 1 6 -2 2 14.32 3.87 1 7 -2 2 214.43 17.06 1 8 -2 2 57.59 7.18 1 9 -2 2 24.85 6.26 1 -9 -1 2 22.32 7.19 1 -8 -1 6 14.98 4.24 -2 -8 -1 2 14.98 4.24 1 -7 -1 2 204.32 8.86 1 -6 -1 2 179.96 7.51 1 -5 -1 2 1659.47 23.67 1 -4 -1 2 1.58 1.35 1 -3 -1 2 318.41 5.57 1 -2 -1 2 2244.72 15.75 1 -1 -1 2 1107.72 7.46 1 1 -1 2 1333.23 10.52 1 2 -1 2 581.02 8.15 1 3 -1 2 1010.38 17.80 1 4 -1 2 220.52 9.65 1 5 -1 2 33.74 4.47 1 6 -1 2 153.39 12.23 1 7 -1 2 193.13 16.11 1 8 -1 2 344.32 23.46 1 9 -1 2 5.16 6.07 1 -10 0 2 31.23 8.61 1 -9 0 6 126.80 11.18 -2 -9 0 2 126.80 11.18 1 -8 0 2 87.24 6.63 1 -7 0 2 46.16 3.85 1 -6 0 2 89.80 5.57 1 -5 0 2 1182.28 23.52 1 -4 0 2 1477.29 20.69 1 -3 0 2 4.35 0.88 1 -2 0 2 903.59 7.48 1 -1 0 2 1862.11 14.05 1 0 0 2 224.79 4.00 -2 0 0 2 224.79 4.00 1 1 0 2 3042.78 27.55 1 2 0 2 350.94 6.53 1 3 0 2 702.79 15.37 1 4 0 2 32.45 4.01 1 5 0 2 255.15 16.86 1 6 0 2 5.39 2.83 1 7 0 2 46.01 12.75 1 8 0 2 109.87 15.39 1 -9 0 10 25.29 8.75 -2 9 0 2 25.29 8.75 1 -10 1 2 56.38 11.45 1 -9 1 2 36.97 6.44 1 -8 1 2 3.23 2.87 1 -7 1 2 225.64 8.50 1 -6 1 2 432.31 8.90 1 -5 1 2 495.28 6.12 1 -4 1 2 828.05 8.14 1 -3 1 2 240.83 3.24 1 -2 1 2 37.75 6.50 1 -1 1 2 622.75 16.18 1 0 1 2 5047.13 82.99 1 1 1 2 210.25 4.80 1 2 1 2 87.25 3.18 1 3 1 2 161.11 9.26 1 4 1 2 1177.02 29.84 1 5 1 2 157.29 8.07 1 6 1 2 107.16 7.56 1 7 1 2 165.50 17.82 1 -8 -1 10 17.74 8.02 -2 8 1 2 17.74 8.02 1 -9 2 2 43.22 9.39 1 -8 2 2 153.13 16.03 1 -7 2 2 100.37 3.61 1 -6 2 2 10.27 2.85 1 -5 2 2 78.81 3.25 1 -4 2 2 1887.03 19.89 1 3 -2 1 106.78 7.13 -2 -3 2 2 106.78 7.13 1 -2 2 2 132.62 1.95 1 -1 2 2 44.85 2.00 1 0 2 2 41.78 2.51 1 1 2 2 337.31 6.68 1 2 2 2 710.83 25.34 1 3 2 2 171.94 13.42 1 4 2 2 48.63 4.53 1 5 2 2 300.03 31.84 1 -6 -2 9 20.56 7.30 -2 6 2 2 20.56 7.30 1 7 2 2 57.74 12.16 1 -10 3 2 0.42 5.56 1 -9 3 2 42.19 6.77 1 -8 3 2 184.43 12.22 1 -7 3 2 18.09 2.84 1 -6 3 2 213.59 4.35 1 -5 3 2 1372.67 17.87 1 4 -3 1 331.61 13.27 -2 -4 3 2 331.61 13.27 1 -3 3 2 315.88 11.37 1 -2 3 2 97.69 3.22 1 -1 3 2 104.29 3.56 1 0 3 2 15.57 2.70 1 1 3 2 2207.10 20.58 1 2 3 2 51.62 4.17 1 3 3 2 105.61 11.45 1 4 3 2 34.87 9.71 1 -5 -3 9 475.31 27.61 -2 5 3 2 475.31 27.61 1 6 3 2 17.12 7.58 1 7 3 2 104.33 15.83 1 -10 4 2 499.15 23.37 1 -9 4 2 48.51 7.20 1 -8 4 2 362.88 17.20 1 -7 4 2 789.79 19.23 1 -6 4 0 23.41 3.07 -2 -6 4 2 23.41 3.07 1 -5 4 2 37.17 6.12 1 -4 4 2 24.18 2.18 1 -3 4 2 68.79 2.18 1 -2 4 2 7.42 1.22 1 -1 4 2 705.98 15.04 1 0 4 2 914.56 19.14 1 1 4 2 17.52 2.55 1 2 4 2 11.73 2.34 1 -3 -4 8 88.26 11.33 -2 3 4 2 88.26 11.33 1 4 4 2 27.87 8.04 1 5 4 2 15.32 7.12 1 6 4 2 12.85 7.46 1 -10 5 2 180.93 20.62 1 -9 5 2 55.91 12.03 1 -8 5 2 31.57 4.56 1 -7 5 0 629.52 17.49 -2 -7 5 2 629.52 17.49 1 -6 5 2 77.88 12.42 1 -5 5 2 89.24 3.58 1 -4 5 2 459.42 5.72 1 -3 5 2 5.21 1.15 1 -2 5 2 4.21 1.76 1 -1 5 2 22.09 3.72 1 0 5 2 163.41 9.23 1 1 5 2 540.45 22.99 1 -2 -5 8 127.05 9.69 -2 2 5 2 127.05 9.69 1 3 5 2 23.26 8.09 1 4 5 2 30.29 9.46 1 5 5 2 35.08 10.12 1 -9 6 1 299.21 14.18 -2 -9 6 2 299.21 14.18 1 -8 6 2 143.65 10.00 1 -7 6 2 428.08 15.03 1 -6 6 2 916.40 15.37 1 -5 6 2 76.89 3.82 1 -4 6 2 54.84 2.78 1 -3 6 2 155.68 5.66 1 -2 6 2 12.58 2.65 1 -1 6 2 734.62 20.27 1 0 -6 7 443.97 17.01 -2 0 6 2 443.97 17.01 1 1 6 2 362.95 13.17 1 2 6 2 61.65 6.34 1 3 6 2 20.15 4.40 1 4 6 2 40.32 7.43 1 -9 7 2 44.15 5.95 1 -8 7 2 277.95 14.47 1 -7 7 2 21.14 4.09 1 -6 7 2 170.59 9.10 1 -5 7 2 157.24 5.88 1 -4 7 2 34.41 2.99 1 -3 7 2 166.96 6.45 1 -2 7 2 302.96 9.10 1 1 -7 7 78.26 8.01 -2 -1 7 2 78.26 8.01 1 0 7 2 290.54 35.18 1 1 7 2 7.21 3.36 1 2 7 2 111.64 10.98 1 3 7 2 16.90 5.09 1 -9 8 2 -2.01 5.89 1 -8 8 2 14.05 4.61 1 -7 8 2 84.37 15.64 1 -6 8 2 406.89 18.72 1 -5 8 2 93.68 8.96 1 -4 8 2 409.40 11.58 1 -3 8 2 13.93 4.37 1 -2 8 2 18.03 6.00 1 -1 8 2 11.21 3.71 1 0 8 2 413.51 36.36 1 1 8 2 190.93 24.10 1 2 8 2 3.80 5.11 1 -8 9 2 35.12 9.56 1 -7 9 2 137.68 11.88 1 -6 9 2 46.34 7.24 1 -5 9 2 35.29 6.21 1 4 -9 6 3.99 2.79 -2 -4 9 2 3.99 2.79 1 -3 9 2 15.58 4.53 1 -2 9 2 7.45 4.03 1 -1 9 2 157.97 10.05 1 0 9 2 12.36 3.63 1 -7 10 2 -6.87 6.87 1 -6 10 2 147.18 17.46 1 -3 10 2 57.75 12.74 1 -2 10 2 19.09 7.04 1 -1 10 2 40.23 10.36 1 1 -11 3 28.52 8.60 1 3 -11 3 152.06 18.35 1 4 -11 3 37.51 16.10 1 5 -11 3 405.30 28.66 1 0 -10 3 -1.09 3.86 1 1 -10 3 49.55 6.13 1 2 -10 3 127.12 9.11 1 3 -10 3 -2.85 2.85 1 4 -10 3 37.93 6.28 1 5 -10 1 94.00 7.96 -2 5 -10 3 94.00 7.96 1 6 -10 3 14.57 7.44 1 7 -10 3 38.74 10.08 1 -2 -9 3 149.89 10.67 1 -1 -9 3 251.28 12.81 1 0 -9 3 11.57 3.35 1 1 -9 3 159.94 9.61 1 2 -9 3 32.36 4.47 1 3 -9 3 236.42 9.43 1 4 -9 1 1.88 3.22 -2 4 -9 3 1.88 3.22 1 5 -9 3 39.21 5.58 1 6 -9 3 268.77 16.16 1 7 -9 3 78.55 9.16 1 -4 -8 3 212.06 18.21 1 -3 -8 3 4.41 3.41 1 -2 -8 3 -2.64 3.07 1 -1 -8 3 135.18 9.05 1 0 -8 3 1.22 3.34 1 1 -8 3 126.58 8.14 1 2 -8 3 208.13 8.17 1 3 -8 3 6.72 2.17 1 4 -8 3 75.33 4.94 1 5 -8 3 28.10 3.44 1 6 -8 3 74.54 6.71 1 7 -8 3 19.26 4.44 1 -5 -7 3 3.29 3.34 1 -4 -7 3 158.77 10.33 1 -3 -7 3 11.84 3.75 1 -2 -7 3 50.30 5.93 1 -1 -7 3 441.30 14.59 1 0 -7 3 654.59 20.29 1 1 -7 2 59.51 5.43 -2 1 -7 3 59.51 5.43 1 2 -7 3 308.12 9.03 1 3 -7 3 5.86 2.00 1 4 -7 3 7.36 2.07 1 5 -7 3 202.77 6.27 1 6 -7 3 438.49 10.42 1 7 -7 3 20.40 5.00 1 8 -7 3 71.94 8.46 1 9 -7 3 35.44 9.27 1 -7 -6 3 82.26 13.30 1 -6 -6 3 7.01 3.77 1 -5 -6 3 -0.56 3.08 1 -4 -6 3 304.07 13.01 1 -3 -6 3 239.41 12.07 1 -2 -6 3 -0.75 3.59 1 -1 -6 3 25.39 3.37 1 0 -6 2 313.07 10.77 -2 0 -6 3 313.07 10.77 1 1 -6 3 225.35 6.93 1 2 -6 3 25.32 2.21 1 3 -6 3 54.85 2.68 1 4 -6 3 2.62 1.28 1 5 -6 3 112.78 5.57 1 6 -6 3 80.76 6.40 1 7 -6 3 11.40 2.96 1 8 -6 3 3.35 3.56 1 -9 6 6 33.03 9.48 -2 9 -6 3 33.03 9.48 1 -7 -5 3 -2.33 2.68 1 -6 -5 3 25.47 6.40 1 -5 -5 3 61.98 5.97 1 -4 -5 3 0.58 2.56 1 -3 -5 3 488.94 14.97 1 -2 -5 3 35.91 3.10 -2 -2 -5 3 35.91 3.10 1 -1 -5 3 87.92 4.76 1 0 -5 3 76.97 5.10 1 1 -5 3 228.77 6.20 1 2 -5 3 142.93 3.05 1 3 -5 3 491.04 7.53 1 4 -5 3 1.09 1.30 1 5 -5 3 80.91 5.69 1 6 -5 3 677.90 16.64 1 -7 5 5 230.29 10.43 -2 7 -5 3 230.29 10.43 1 8 -5 3 8.55 6.57 1 9 -5 3 37.20 10.10 1 -8 -4 3 134.77 11.59 1 -7 -4 3 31.16 4.10 1 -6 -4 3 155.69 7.71 1 -5 -4 3 2.65 2.11 1 -4 -4 3 164.39 11.72 1 -3 -4 3 200.70 7.26 -2 -3 -4 3 200.70 7.26 1 -2 -4 3 2.76 1.93 1 -1 -4 3 77.01 3.35 1 0 -4 3 665.23 12.60 1 1 -4 3 1765.13 14.70 1 2 -4 3 583.63 6.85 1 3 -4 3 1.21 0.80 1 4 -4 3 1.61 1.81 1 5 -4 3 19.10 4.24 1 -6 4 5 160.21 8.16 -2 6 -4 3 160.21 8.16 1 7 -4 3 4.83 3.36 1 8 -4 3 29.89 4.64 1 9 -4 3 2.89 4.13 1 -9 -3 3 121.54 11.17 1 -8 -3 3 1.89 5.83 1 -7 -3 3 136.56 8.22 1 -6 -3 3 15.43 3.58 1 -5 -3 4 617.35 13.03 -2 -5 -3 3 617.35 13.03 1 -4 -3 3 361.17 18.02 1 -3 -3 3 75.29 6.51 1 -2 -3 3 5.71 1.34 1 -1 -3 3 13.71 2.29 1 0 -3 3 245.99 6.99 1 1 -3 3 198.78 3.49 1 2 -3 3 279.59 5.48 1 3 -3 3 145.08 5.60 1 -4 3 4 69.83 6.06 -2 4 -3 3 69.83 6.06 1 5 -3 3 111.15 7.69 1 6 -3 3 41.69 5.62 1 7 -3 3 121.07 9.71 1 8 -3 3 23.04 4.94 1 9 -3 3 6.78 5.13 1 -9 -2 3 212.28 13.84 1 -8 -2 3 25.63 5.38 1 -7 -2 3 318.13 11.46 1 -6 -2 4 536.30 11.96 -2 -6 -2 3 536.30 11.96 1 -5 -2 3 4.79 1.73 1 -4 -2 3 13.04 2.00 1 -3 -2 3 260.51 5.79 1 -2 -2 3 369.73 4.92 1 -1 -2 3 194.02 3.07 1 0 -2 3 472.87 12.88 1 1 -2 3 7.75 1.05 1 2 -2 3 68.25 3.09 1 -3 2 4 51.81 5.70 -2 3 -2 3 51.81 5.70 1 4 -2 3 1.11 2.22 1 5 -2 3 65.93 6.38 1 6 -2 3 97.28 8.29 1 7 -2 3 110.66 10.92 1 8 -2 3 53.97 7.04 1 9 -2 3 23.22 7.57 1 -10 -1 3 126.04 16.30 1 -9 -1 3 57.39 6.52 1 -8 -1 5 228.09 12.70 -2 -8 -1 3 228.09 12.70 1 -7 -1 3 318.24 10.42 1 -6 -1 3 302.41 9.29 1 -5 -1 3 79.53 3.92 1 -4 -1 3 2456.38 28.25 1 -3 -1 3 1663.81 8.84 1 -2 -1 3 699.69 6.08 1 -1 -1 3 215.43 2.37 1 0 -1 3 1215.17 12.43 1 1 -1 3 470.56 7.28 1 2 -1 3 22.21 2.74 1 3 -1 3 0.26 3.09 1 4 -1 3 360.88 12.72 1 5 -1 3 50.34 5.73 1 6 -1 3 191.71 11.48 1 7 -1 3 31.93 8.09 1 8 -1 3 2.79 5.62 1 9 -1 3 2.18 5.48 1 -10 0 3 81.44 13.16 1 -9 0 5 102.64 10.02 -2 -9 0 3 102.64 10.02 1 -8 0 3 170.16 8.89 1 -7 0 3 182.54 6.35 1 -6 0 3 43.41 4.33 1 -5 0 3 2.41 0.92 1 -4 0 3 31.27 1.47 1 -3 0 3 7.86 0.83 1 -2 0 3 1864.96 11.33 1 -1 0 3 2529.22 47.60 1 0 0 3 330.58 4.25 -2 0 0 3 330.58 4.25 1 1 0 3 535.34 32.18 1 2 0 3 148.96 8.32 1 3 0 3 18.22 4.74 1 4 0 3 0.44 2.18 1 5 0 3 5.67 2.31 1 6 0 3 121.91 14.97 1 7 0 3 23.02 7.15 1 8 0 3 9.90 7.14 1 -10 1 3 275.49 23.91 1 -9 1 3 7.38 4.35 1 -8 1 3 10.42 3.52 1 -7 1 3 177.81 8.56 1 -6 1 3 599.08 6.78 1 -5 1 3 596.92 7.36 1 -4 1 3 132.61 2.75 1 -3 1 3 5520.07 29.12 1 -2 1 3 80.24 14.57 1 -1 1 3 133.29 5.22 1 0 1 3 16.73 2.91 1 1 1 3 1349.11 16.45 1 2 1 3 151.70 8.92 1 3 1 3 858.27 22.40 1 4 1 3 8.41 2.46 1 5 1 3 -1.20 3.49 1 6 1 3 19.96 7.00 1 7 1 3 125.11 16.23 1 -10 2 3 10.27 7.56 1 -9 2 3 34.96 8.74 1 -8 2 3 33.61 8.08 1 -7 2 3 0.64 1.63 1 -6 2 3 262.51 5.29 1 -5 2 3 11.05 1.10 1 -4 2 3 245.54 7.56 1 3 -2 2 544.71 5.79 -2 -3 2 3 544.71 5.79 1 -2 2 3 25.68 1.32 1 -1 2 3 439.05 9.67 1 0 2 3 748.43 14.50 1 1 2 3 807.99 13.14 1 2 2 3 33.18 3.73 1 3 2 3 95.81 10.73 1 4 2 3 232.84 18.00 1 5 2 3 11.86 5.68 1 -6 -2 10 133.19 15.96 -2 6 2 3 133.19 15.96 1 7 2 3 45.22 11.29 1 -10 3 3 53.88 11.68 1 -9 3 3 27.14 8.52 1 -8 3 3 18.36 5.12 1 -7 3 3 646.50 17.13 1 -6 3 3 247.06 6.34 1 -5 3 3 935.80 14.50 1 4 -3 2 52.79 5.87 -2 -4 3 3 52.79 5.87 1 -3 3 3 19.62 1.15 1 -2 3 3 253.43 4.12 1 -1 3 3 67.73 3.13 1 0 3 3 706.06 15.95 1 1 3 3 80.17 4.38 1 2 3 3 1149.33 35.15 1 3 3 3 512.29 26.05 1 4 3 3 300.37 21.91 1 -5 -3 10 18.39 7.92 -2 5 3 3 18.39 7.92 1 6 3 3 44.36 10.20 1 -10 4 3 39.24 10.15 1 -9 4 3 23.04 5.83 1 -8 4 3 3.85 3.62 1 -7 4 3 7.52 3.60 1 6 -4 1 622.65 9.85 -2 -6 4 3 622.65 9.85 1 -5 4 3 2.08 1.10 1 -4 4 3 40.99 2.95 1 -3 4 3 231.89 4.14 1 -2 4 3 305.35 5.94 1 -1 4 3 7.00 2.63 1 0 4 3 -0.22 2.22 1 1 4 3 457.90 10.69 1 2 4 3 -3.35 3.72 1 -3 -4 9 108.77 13.15 -2 3 4 3 108.77 13.15 1 4 4 3 62.10 11.17 1 5 4 3 89.28 14.16 1 -10 5 3 34.47 10.33 1 -9 5 3 88.68 7.67 1 -8 5 3 20.18 4.88 1 7 -5 1 70.23 5.46 -2 -7 5 3 70.23 5.46 1 -6 5 3 1432.38 22.89 1 -5 5 3 37.83 2.35 1 -4 5 3 49.59 2.36 1 -3 5 3 51.84 2.61 1 -2 5 3 310.32 9.45 1 -1 5 3 67.50 5.87 1 0 5 3 722.63 19.69 1 1 5 3 347.53 48.11 1 -2 -5 9 79.73 11.87 -2 2 5 3 79.73 11.87 1 3 5 3 61.09 11.60 1 4 5 3 141.77 17.04 1 -9 6 0 11.23 4.05 -2 -9 6 3 11.23 4.05 1 -8 6 3 107.57 8.51 1 -7 6 3 85.86 6.73 1 -6 6 3 176.18 13.00 1 -5 6 3 96.28 4.22 1 -4 6 3 78.65 4.06 1 -3 6 3 36.65 3.89 1 -2 6 3 33.39 3.69 1 -1 6 3 327.16 14.74 1 0 -6 8 379.50 13.01 -2 0 6 3 379.50 13.01 1 1 6 3 41.58 11.20 1 2 6 3 57.19 7.79 1 3 6 3 42.05 10.51 1 -9 7 3 13.43 4.55 1 -8 7 3 27.20 10.72 1 -7 7 3 60.31 6.17 1 -6 7 3 12.64 3.59 1 -5 7 3 842.98 19.31 1 -4 7 3 -0.27 1.73 1 -3 7 3 47.16 3.71 1 -2 7 3 187.70 8.90 1 1 -7 8 96.02 8.61 -2 -1 7 3 96.02 8.61 1 0 7 3 155.11 11.56 1 1 7 3 348.94 33.05 1 2 7 3 153.32 12.78 1 -9 8 3 -6.70 6.70 1 -8 8 3 3.55 3.19 1 -7 8 3 197.38 13.60 1 -6 8 3 103.61 9.53 1 -5 8 3 45.87 5.08 1 -4 8 3 26.45 3.51 1 -3 8 3 29.42 4.16 1 -2 8 3 147.47 7.63 1 -1 8 3 25.02 6.01 1 0 8 3 18.58 4.19 1 1 8 3 173.25 13.96 1 -8 9 3 5.27 5.93 1 -7 9 3 109.57 14.38 1 -6 9 3 45.43 7.00 1 -5 9 3 47.57 11.75 1 4 -9 7 32.80 9.01 -2 -4 9 3 32.80 9.01 1 -3 9 3 22.30 8.51 1 -2 9 3 26.85 6.47 1 -1 9 3 26.10 4.81 1 0 9 3 120.57 11.62 1 -3 10 3 1.64 6.19 1 1 -11 4 164.15 18.81 1 2 -11 4 346.73 25.86 1 4 -11 4 32.60 9.13 1 5 -11 4 12.64 6.34 1 -1 -10 4 0.17 4.80 1 0 -10 4 2.61 3.41 1 1 -10 4 -3.49 3.49 1 2 -10 4 77.17 7.10 1 3 -10 4 3.18 3.28 1 4 -10 4 88.72 19.89 1 -5 10 0 15.50 3.90 -2 5 -10 4 15.50 3.90 1 6 -10 4 43.44 10.17 1 7 -10 4 51.99 11.02 1 -2 -9 4 71.37 7.48 1 -1 -9 4 2.61 2.94 1 0 -9 4 229.43 11.77 1 1 -9 4 316.29 13.44 1 2 -9 4 372.52 24.84 1 3 -9 4 230.54 11.16 1 -4 9 0 33.55 4.57 -2 4 -9 4 33.55 4.57 1 5 -9 4 38.42 5.31 1 6 -9 4 2.93 3.47 1 7 -9 4 -4.77 6.05 1 8 -9 4 371.59 27.43 1 -4 -8 4 3.01 4.12 1 -3 -8 4 68.78 7.13 1 -2 -8 4 105.95 8.18 1 -1 -8 4 66.17 6.63 1 0 -8 4 165.22 9.40 1 1 -8 4 33.97 5.40 1 2 -8 4 62.87 4.89 1 3 -8 4 68.40 7.68 1 4 -8 4 2.84 3.35 1 5 -8 4 6.49 2.48 1 6 -8 4 2.11 2.52 1 7 -8 4 33.93 10.60 1 -6 -7 4 109.68 15.91 1 -5 -7 4 11.80 4.47 1 -4 -7 4 155.30 10.22 1 -3 -7 4 51.91 6.05 1 -2 -7 4 254.09 11.56 1 -1 -7 4 549.02 16.02 1 0 -7 4 407.67 15.04 1 1 -7 1 613.41 16.15 -2 1 -7 4 613.41 16.15 1 2 -7 4 445.19 10.59 1 3 -7 4 64.74 4.21 1 4 -7 4 31.15 3.09 1 5 -7 4 84.35 4.55 1 6 -7 4 10.23 3.20 1 7 -7 4 124.75 10.46 1 8 -7 4 60.77 13.19 1 -7 -6 4 32.89 9.19 1 -6 -6 4 40.05 5.80 1 -5 -6 4 136.73 9.22 1 -4 -6 4 74.26 6.73 1 -3 -6 4 2.35 2.75 1 -2 -6 4 187.83 9.14 1 -1 -6 4 215.88 15.51 1 0 -6 1 64.13 8.72 -2 0 -6 4 64.13 8.72 1 1 -6 4 361.04 8.30 1 2 -6 4 78.26 4.20 1 3 -6 4 10.75 2.14 1 4 -6 4 469.96 9.29 1 5 -6 4 66.77 4.62 1 6 -6 4 28.51 5.64 1 7 -6 4 5.56 2.77 1 8 -6 4 77.84 9.34 1 9 -6 4 6.61 4.87 1 -8 -5 4 36.91 8.08 1 -7 -5 4 70.48 5.80 1 -6 -5 4 6.06 3.23 1 -5 -5 4 171.15 8.16 1 -4 -5 4 13.67 4.85 1 -3 -5 4 33.90 5.52 1 -2 -5 2 97.33 4.56 -2 -2 -5 4 97.33 4.56 1 -1 -5 4 955.71 30.53 1 0 -5 4 303.17 6.67 1 1 -5 4 452.03 6.84 1 2 -5 4 600.68 9.46 1 3 -5 4 305.15 6.08 1 4 -5 4 7.49 2.19 1 5 -5 4 510.15 13.90 1 6 -5 4 141.17 8.04 1 -7 5 6 86.26 6.81 -2 7 -5 4 86.26 6.81 1 8 -5 4 134.20 10.36 1 9 -5 4 65.90 12.25 1 -8 -4 4 -2.14 3.09 1 -7 -4 4 -0.34 3.34 1 -6 -4 4 1.52 2.24 1 -5 -4 4 61.61 4.70 1 -4 -4 4 624.59 13.23 1 -3 -4 2 298.19 8.63 -2 -3 -4 4 298.19 8.63 1 -2 -4 4 144.42 5.52 1 -1 -4 4 6.37 1.74 1 0 -4 4 3.33 2.14 1 1 -4 4 48.41 2.58 1 2 -4 4 181.83 4.96 1 3 -4 4 362.04 7.01 1 4 -4 4 422.32 11.53 1 5 -4 4 222.27 12.92 1 -6 4 6 101.09 6.97 -2 6 -4 4 101.09 6.97 1 7 -4 4 9.13 3.34 1 8 -4 4 -1.58 2.83 1 -9 -3 4 4.76 5.72 1 -8 -3 4 2.06 3.19 1 -7 -3 4 67.10 5.41 1 -6 -3 4 99.76 10.47 1 -5 -3 3 609.23 12.75 -2 -5 -3 4 609.23 12.75 1 -4 -3 4 231.81 23.50 1 -3 -3 4 48.69 5.30 1 -2 -3 4 85.63 3.50 1 -1 -3 4 689.77 5.92 1 0 -3 4 1187.12 15.49 1 1 -3 4 15.13 3.11 1 2 -3 4 413.35 8.03 1 3 -3 4 73.08 4.96 1 -4 3 5 86.66 6.98 -2 4 -3 4 86.66 6.98 1 5 -3 4 241.46 12.30 1 6 -3 4 537.33 19.05 1 7 -3 4 197.51 12.73 1 8 -3 4 233.22 14.68 1 9 -3 4 28.83 8.50 1 -9 -2 4 95.44 7.97 1 -8 -2 4 3.60 2.77 1 -7 -2 4 1.34 3.20 1 -6 -2 3 149.06 6.31 -2 -6 -2 4 149.06 6.31 1 -5 -2 4 99.51 4.85 1 -4 -2 4 4.74 1.73 1 -3 -2 4 6.02 1.30 1 -2 -2 4 1077.13 7.18 1 -1 -2 4 43.30 1.67 1 0 -2 4 521.88 22.72 1 1 -2 4 440.77 12.02 1 2 -2 4 86.18 5.74 1 -3 2 5 109.53 7.03 -2 3 -2 4 109.53 7.03 1 4 -2 4 17.21 4.20 1 5 -2 4 204.18 11.03 1 6 -2 4 29.76 4.93 1 7 -2 4 24.34 5.10 1 8 -2 4 45.12 10.07 1 -10 -1 4 50.70 11.63 1 -9 -1 4 26.91 5.36 1 -8 -1 4 40.49 5.23 -2 -8 -1 4 40.49 5.23 1 -7 -1 4 52.63 7.94 1 -6 -1 4 28.28 3.08 1 -5 -1 4 250.26 6.02 1 -4 -1 4 36.86 1.77 1 -3 -1 4 49.04 1.69 1 -2 -1 4 3.29 0.73 1 -1 -1 4 174.28 2.85 1 0 -1 4 4405.17 42.92 1 1 -1 4 1223.15 25.79 1 2 -1 4 69.70 5.16 1 3 -1 4 5.74 2.73 1 4 -1 4 45.79 5.19 1 5 -1 4 122.94 8.83 1 6 -1 4 191.91 16.02 1 7 -1 4 255.42 21.07 1 8 -1 4 8.33 6.71 1 -10 0 4 115.54 16.57 1 -9 0 4 7.15 3.71 -2 -9 0 4 7.15 3.71 1 -8 0 4 6.29 3.86 1 -7 0 4 2.37 1.18 1 -6 0 4 30.99 3.35 1 -5 0 4 64.27 2.45 1 -4 0 4 430.63 4.69 1 -3 0 4 7.89 1.01 1 -2 0 4 5.96 0.94 1 -1 0 4 2610.87 16.82 1 0 0 4 6.20 1.02 -2 0 0 4 6.20 1.02 1 1 0 4 688.34 14.96 1 2 0 4 18.69 3.22 1 3 0 4 15.59 1.51 1 4 0 4 164.04 6.36 1 5 0 4 181.98 16.18 1 6 0 4 52.18 10.05 1 7 0 4 -5.21 5.70 1 -10 1 4 381.37 21.13 1 -9 1 4 82.85 9.02 1 -8 1 4 125.37 14.48 1 -7 1 4 2.46 4.40 1 -6 1 4 182.62 5.99 1 -5 1 4 255.68 4.46 1 -4 1 4 1572.96 9.90 1 -3 1 4 29.82 1.89 1 -2 1 4 121.37 3.12 1 -1 1 4 500.70 11.19 1 0 1 4 66.69 4.77 1 1 1 4 251.32 7.45 1 2 1 4 93.30 5.69 1 3 1 4 13.22 4.96 1 4 1 4 54.93 8.76 1 5 1 4 795.48 35.39 1 6 1 4 16.20 6.50 1 7 1 4 38.28 10.28 1 -10 2 4 226.26 22.30 1 -9 2 4 88.99 13.84 1 -8 2 4 9.89 5.46 1 -7 2 4 1.17 1.90 1 -6 2 4 19.41 1.18 1 -5 2 4 3.42 0.86 1 -4 2 4 117.60 2.67 1 3 -2 3 16.68 1.23 -2 -3 2 4 16.68 1.23 1 -2 2 4 57.17 4.01 1 -1 2 4 21.13 2.34 1 0 2 4 88.50 3.67 1 1 2 4 159.59 6.65 1 2 2 4 138.27 7.33 1 3 2 4 135.87 13.54 1 4 2 4 210.37 17.80 1 5 2 4 63.21 11.40 1 -6 -2 11 119.33 16.28 -2 6 2 4 119.33 16.28 1 -10 3 4 350.01 27.10 1 -9 3 4 9.70 5.80 1 -8 3 4 88.08 11.38 1 -7 3 4 437.18 12.35 1 -6 3 4 79.68 5.43 1 -5 3 4 94.23 5.19 1 4 -3 3 232.59 5.05 -2 -4 3 4 232.59 5.05 1 -3 3 4 892.05 12.31 1 -2 3 4 273.47 6.49 1 -1 3 4 16.68 4.21 1 0 3 4 525.03 21.39 1 1 3 4 31.43 2.11 1 2 3 4 100.18 11.86 1 3 3 4 8.61 5.66 1 4 3 4 12.13 6.93 1 -5 -3 11 21.70 8.80 -2 5 3 4 21.70 8.80 1 -9 4 4 313.55 17.80 1 -8 4 4 -1.49 2.60 1 -7 4 4 68.71 7.85 1 6 -4 2 61.35 4.91 -2 -6 4 4 61.35 4.91 1 -5 4 4 151.32 4.88 1 -4 4 4 583.31 6.55 1 -3 4 4 3.25 0.95 1 -2 4 4 120.59 4.73 1 -1 4 4 117.77 7.01 1 0 4 4 113.76 10.78 1 1 4 4 178.47 15.22 1 2 4 4 51.94 9.54 1 -3 -4 10 38.24 9.44 -2 3 4 4 38.24 9.44 1 4 4 4 70.16 12.97 1 5 4 4 39.61 10.93 1 -10 5 4 97.81 14.43 1 -9 5 4 188.16 11.22 1 -8 5 4 360.55 16.55 1 7 -5 2 103.30 6.57 -2 -7 5 4 103.30 6.57 1 -6 5 4 126.82 7.79 1 -5 5 4 173.26 4.71 1 -4 5 4 5.02 1.41 1 -3 5 4 394.73 8.67 1 -2 5 4 -1.81 1.97 1 -1 5 4 35.31 5.42 1 0 5 4 69.45 8.14 1 1 5 4 46.71 9.00 1 -2 -5 10 16.73 5.80 -2 2 5 4 16.73 5.80 1 3 5 4 77.70 12.71 1 4 5 4 100.89 15.83 1 -10 6 4 7.27 6.52 1 9 -6 1 29.54 5.61 -2 -9 6 4 29.54 5.61 1 -8 6 4 57.72 6.39 1 -7 6 4 198.05 10.24 1 -6 6 4 117.15 7.46 1 -5 6 4 7.05 3.13 1 -4 6 4 236.34 6.79 1 -3 6 4 725.22 16.34 1 -2 6 4 95.16 6.33 1 -1 6 4 3.48 2.96 1 0 -6 9 490.69 18.80 -2 0 6 4 490.69 18.80 1 1 6 4 39.98 8.94 1 2 6 4 14.41 7.17 1 3 6 4 9.53 6.48 1 -9 7 4 58.57 11.15 1 -8 7 4 5.49 3.42 1 -7 7 4 318.53 17.25 1 -6 7 4 398.15 17.73 1 -5 7 4 59.03 5.40 1 -4 7 4 64.24 4.74 1 -3 7 4 343.94 9.83 1 -2 7 4 9.95 3.84 1 1 -7 9 146.17 14.03 -2 -1 7 4 146.17 14.03 1 0 7 4 202.33 10.95 1 1 7 4 5.85 5.84 1 2 7 4 15.28 7.44 1 -9 8 4 14.26 6.38 1 -8 8 4 -4.93 5.38 1 -7 8 4 53.24 7.07 1 -6 8 4 392.90 19.29 1 -5 8 4 92.39 9.11 1 -4 8 4 82.94 6.86 1 -3 8 4 12.68 3.81 1 -2 8 4 198.08 10.27 1 -1 8 4 12.80 4.34 1 0 8 4 7.07 3.47 1 -3 9 4 32.25 9.83 1 -2 9 4 80.16 13.09 1 -1 9 4 13.82 7.07 1 2 -11 5 119.37 15.41 1 0 -10 5 3.69 3.81 1 1 -10 5 2.54 3.28 1 2 -10 5 473.74 17.30 1 3 -10 5 240.56 12.24 1 4 -10 5 12.04 5.65 1 -5 10 1 125.49 12.07 -2 5 -10 5 125.49 12.07 1 6 -10 5 36.72 10.99 1 -2 -9 5 50.72 6.60 1 -1 -9 5 43.13 6.15 1 0 -9 5 52.62 6.26 1 1 -9 5 177.37 10.29 1 2 -9 5 4.27 3.64 1 3 -9 5 12.43 3.78 1 -4 9 1 12.29 3.64 -2 4 -9 5 12.29 3.64 1 5 -9 5 7.73 3.47 1 6 -9 5 47.47 6.71 1 7 -9 5 56.16 11.17 1 -4 -8 5 0.65 3.23 1 -3 -8 5 219.98 12.04 1 -2 -8 5 24.84 4.31 1 -1 -8 5 84.03 7.25 1 0 -8 5 2.92 2.77 1 1 -8 5 204.51 10.49 1 2 -8 5 334.04 12.83 1 3 -8 5 586.83 22.70 1 4 -8 5 67.31 7.08 1 5 -8 5 12.78 3.03 1 6 -8 5 243.86 14.91 1 7 -8 5 66.75 13.41 1 -6 -7 5 5.49 6.41 1 -5 -7 5 355.27 15.39 1 -4 -7 5 122.39 8.78 1 -3 -7 5 100.11 7.73 1 -2 -7 5 5.08 3.02 1 -1 -7 5 44.33 6.59 1 0 -7 5 136.27 11.21 1 -1 7 0 313.83 8.91 -2 1 -7 5 313.83 8.91 1 2 -7 5 229.45 10.85 1 3 -7 5 72.52 5.97 1 4 -7 5 -2.27 3.91 1 5 -7 5 19.31 3.65 1 6 -7 5 163.00 20.10 1 7 -7 5 83.86 9.11 1 -7 -6 5 119.71 15.26 1 -6 -6 5 21.87 4.62 1 -5 -6 5 -1.43 3.51 1 -4 -6 5 5.25 2.93 1 -3 -6 5 143.77 8.47 1 -2 -6 5 187.35 9.28 1 -1 -6 5 362.32 12.19 1 0 6 0 275.00 11.28 -2 0 -6 5 275.00 11.28 1 1 -6 5 -0.92 1.42 1 2 -6 5 215.96 6.41 1 3 -6 5 187.92 5.77 1 4 -6 5 168.29 6.70 1 5 -6 5 19.65 3.06 1 6 -6 5 624.08 17.26 1 7 -6 5 2.73 2.72 1 8 -6 5 35.65 10.00 1 -8 -5 5 118.11 11.54 1 -7 -5 5 16.59 4.36 1 -6 -5 5 13.81 3.00 1 -5 -5 5 161.64 8.00 1 -4 -5 5 345.22 10.79 1 -3 -5 5 43.41 4.54 1 -2 -5 1 152.59 8.54 -2 -2 -5 5 152.59 8.54 1 -1 -5 5 255.04 9.61 1 0 -5 5 219.41 8.82 1 1 -5 5 14.52 1.44 1 2 -5 5 1008.55 15.75 1 3 -5 5 36.51 3.13 1 4 -5 5 1.22 2.65 1 5 -5 5 35.34 4.17 1 6 -5 5 46.49 7.70 1 -7 5 7 186.87 10.26 -2 7 -5 5 186.87 10.26 1 8 -5 5 47.55 6.05 1 -8 -4 5 -3.08 3.08 1 -7 -4 5 21.06 3.20 1 -6 -4 5 530.62 13.71 1 -5 -4 5 33.38 4.64 1 -4 -4 5 4.48 2.21 1 -3 -4 1 29.63 3.34 -2 -3 -4 5 29.63 3.34 1 -2 -4 5 115.88 5.26 1 -1 -4 5 61.71 3.34 1 0 -4 5 796.18 10.14 1 1 -4 5 649.90 16.87 1 2 -4 5 37.44 2.90 1 3 -4 5 454.73 8.61 1 4 -4 5 33.00 5.06 1 5 -4 5 29.82 7.92 1 -6 4 7 85.24 9.23 -2 6 -4 5 85.24 9.23 1 7 -4 5 595.62 18.21 1 8 -4 5 22.66 4.65 1 -9 -3 5 8.04 3.06 1 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-1 5 1458.56 10.44 1 -1 -1 5 933.59 19.80 1 0 -1 5 243.72 13.11 1 1 -1 5 759.95 19.60 1 2 -1 5 51.58 5.85 1 3 -1 5 37.01 4.77 1 4 -1 5 43.05 5.24 1 5 -1 5 90.39 7.69 1 6 -1 5 473.09 28.31 1 7 -1 5 50.94 10.50 1 -10 0 5 87.47 14.20 1 -9 0 3 40.98 6.41 -2 -9 0 5 40.98 6.41 1 -8 0 5 6.25 2.51 1 -7 0 5 35.90 5.08 1 -6 0 5 44.97 2.39 1 -5 0 5 9.62 0.96 1 -4 0 5 958.84 7.32 1 -3 0 5 5.65 0.88 1 -2 0 5 2290.98 18.84 1 -1 0 5 1143.86 17.14 1 0 0 5 544.70 7.21 -2 0 0 5 544.70 7.21 1 1 0 5 239.05 7.72 1 2 0 5 635.42 11.57 1 3 0 5 70.68 6.02 1 4 0 5 116.34 12.66 1 5 0 5 187.30 17.48 1 6 0 5 44.72 10.39 1 7 0 5 13.55 7.93 1 -10 1 5 108.78 11.72 1 -9 1 5 1.49 5.53 1 -8 1 5 19.63 7.00 1 -7 1 5 9.76 4.24 1 -6 1 5 171.51 5.29 1 -5 1 5 793.30 9.52 1 -4 1 5 50.96 2.16 1 -3 1 5 8.82 0.79 1 -2 1 5 150.45 3.52 1 -1 1 5 1634.57 29.26 1 0 1 5 253.22 6.45 1 1 1 5 33.62 6.12 1 2 1 5 1338.50 21.86 1 3 1 5 335.03 21.16 1 4 1 5 54.21 9.59 1 5 1 5 69.12 11.40 1 6 1 5 202.03 20.70 1 -10 2 5 68.36 12.84 1 -9 2 5 -2.10 4.82 1 -8 2 5 33.12 7.67 1 -7 2 5 -2.72 2.72 1 -6 2 5 183.67 9.09 1 -5 2 5 33.79 4.11 1 -4 2 5 22.98 1.73 1 3 -2 4 253.87 4.93 -2 -3 2 5 253.87 4.93 1 -2 2 5 727.54 18.25 1 -1 2 5 324.09 15.09 1 0 2 5 17.68 5.21 1 1 2 5 797.59 14.36 1 2 2 5 198.78 8.91 1 3 2 5 957.01 37.08 1 4 2 5 68.81 11.18 1 5 2 5 96.71 14.36 1 -6 -2 12 90.85 14.86 -2 6 2 5 90.85 14.86 1 -10 3 5 -5.38 6.99 1 -9 3 5 38.35 9.15 1 -8 3 5 36.82 5.85 1 -7 3 5 28.79 3.64 1 -6 3 5 153.18 7.01 1 -5 3 5 14.74 4.10 1 4 -3 4 17.19 1.92 -2 -4 3 5 17.19 1.92 1 -3 3 5 195.87 3.95 1 -2 3 5 11.40 2.12 1 -1 3 5 202.30 12.95 1 0 3 5 585.66 12.64 1 1 3 5 71.41 9.34 1 2 3 5 132.51 13.88 1 3 3 5 122.66 15.38 1 4 3 5 324.28 24.69 1 -5 -3 12 56.38 11.81 -2 5 3 5 56.38 11.81 1 -9 4 5 0.50 4.09 1 -8 4 5 1.94 2.29 1 -7 4 5 295.70 10.53 1 6 -4 3 93.26 6.55 -2 -6 4 5 93.26 6.55 1 -5 4 5 172.91 9.74 1 -4 4 5 40.52 3.59 1 -3 4 5 51.77 3.84 1 -2 4 5 124.88 5.28 1 -1 4 5 633.25 24.30 1 0 4 5 43.43 7.95 1 1 4 5 1.69 4.15 1 2 4 5 271.05 21.13 1 -3 -4 11 0.97 4.76 -2 3 4 5 0.97 4.76 1 4 4 5 360.30 27.97 1 -9 5 5 4.43 3.35 1 -8 5 5 94.62 6.71 1 7 -5 3 223.90 10.82 -2 -7 5 5 223.90 10.82 1 -6 5 5 69.87 6.05 1 -5 5 5 17.61 2.91 1 -4 5 5 92.57 4.84 1 -3 5 5 2.42 3.29 1 -2 5 5 363.02 10.43 1 -1 5 5 239.33 16.26 1 0 5 5 16.12 6.15 1 1 5 5 96.42 13.22 1 -2 -5 11 7.43 6.39 -2 2 5 5 7.43 6.39 1 3 5 5 20.38 9.55 1 -10 6 5 393.11 28.55 1 9 -6 2 4.94 5.24 -2 -9 6 5 4.94 5.24 1 -8 6 5 16.27 3.83 1 -7 6 5 7.38 2.94 1 -6 6 5 372.13 13.21 1 -5 6 5 7.40 2.79 1 -4 6 5 274.06 10.58 1 -3 6 5 166.28 7.92 1 -2 6 5 456.84 16.59 1 -1 6 5 27.98 6.79 1 0 -6 10 66.76 10.76 -2 0 6 5 66.76 10.76 1 1 6 5 18.29 7.59 1 2 6 5 11.98 7.98 1 -9 7 5 12.81 4.92 1 -8 7 5 42.31 5.59 1 -7 7 5 30.01 8.29 1 -6 7 5 111.17 10.34 1 -5 7 5 33.06 6.16 1 -4 7 5 32.10 4.49 1 -3 7 5 52.43 6.50 1 -2 7 5 21.18 5.07 1 1 -7 10 288.61 15.61 -2 -1 7 5 288.61 15.61 1 0 7 5 18.50 4.86 1 1 7 5 -3.52 6.11 1 -8 8 5 -4.78 6.07 1 -7 8 5 34.23 9.37 1 -6 8 5 3.45 8.98 1 -5 8 5 346.18 24.05 1 -4 8 5 66.68 15.07 1 -3 8 5 127.92 15.52 1 -2 8 5 92.09 9.48 1 -1 8 5 222.54 21.62 1 2 -11 6 28.61 8.39 1 0 -10 6 32.94 5.68 1 1 -10 6 161.63 10.78 1 2 -10 6 244.74 12.89 1 3 -10 6 73.71 7.31 1 4 -10 6 6.97 3.17 1 5 -10 6 134.06 16.46 1 -2 -9 6 42.32 6.36 1 -1 -9 6 3.67 3.29 1 0 -9 6 86.83 9.35 1 1 -9 6 20.00 4.28 1 2 -9 6 35.87 5.24 1 3 -9 6 4.66 3.12 1 -4 9 2 11.41 3.54 -2 4 -9 6 11.41 3.54 1 5 -9 6 30.83 5.41 1 6 -9 6 0.12 5.79 1 -4 -8 6 554.04 19.75 1 -3 -8 6 1.15 2.80 1 -2 -8 6 68.64 6.80 1 -1 -8 6 82.70 7.06 1 0 -8 6 220.37 11.13 1 1 -8 6 349.04 13.86 1 2 -8 6 963.04 22.30 1 3 -8 6 154.30 9.02 1 4 -8 6 94.52 6.59 1 5 -8 6 1.82 2.60 1 6 -8 6 107.45 25.84 1 -6 -7 6 54.51 12.21 1 -5 -7 6 27.59 5.49 1 -4 -7 6 12.00 3.77 1 -3 -7 6 135.83 10.03 1 -2 -7 6 3.91 4.38 1 -1 -7 6 603.75 25.17 1 0 -7 6 85.02 7.30 1 -1 7 1 46.84 6.53 -2 1 -7 6 46.84 6.53 1 2 -7 6 36.85 6.83 1 3 -7 6 119.21 7.67 1 4 -7 6 0.40 4.69 1 5 -7 6 117.99 10.40 1 6 -7 6 29.26 6.19 1 7 -7 6 29.23 11.57 1 -7 -6 6 14.92 4.99 1 -6 -6 6 8.07 3.56 1 -5 -6 6 21.17 4.29 1 -4 -6 6 1184.96 24.72 1 -3 -6 6 240.61 11.08 1 -2 -6 6 6.81 3.32 1 -1 -6 6 49.40 5.10 1 0 6 1 467.27 21.41 -2 0 -6 6 467.27 21.41 1 1 -6 6 119.77 8.28 1 2 -6 6 917.94 14.55 1 3 -6 6 2075.45 36.10 1 4 -6 6 22.55 3.66 1 5 -6 6 156.54 11.59 1 6 -6 6 10.14 6.86 1 7 -6 6 72.81 9.06 1 -8 -5 6 3.67 5.11 1 -7 -5 6 0.98 2.52 1 -6 -5 6 57.40 5.24 1 -5 -5 6 51.64 4.70 1 -4 -5 6 39.35 4.24 1 -3 -5 6 43.29 5.64 1 2 5 0 21.15 2.89 -2 -2 -5 6 21.15 2.89 1 -1 -5 6 99.74 8.96 1 0 -5 6 505.35 8.20 1 1 -5 6 29.64 2.57 1 2 -5 6 8.22 1.58 1 3 -5 6 31.58 2.83 1 4 -5 6 817.21 17.16 1 5 -5 6 351.60 12.47 1 6 -5 6 197.25 11.42 1 -7 5 8 70.62 6.61 -2 7 -5 6 70.62 6.61 1 8 -5 6 10.70 6.88 1 -9 -4 6 30.99 8.79 1 -8 -4 6 27.09 4.70 1 -7 -4 6 217.19 8.23 1 -6 -4 6 73.77 4.62 1 -5 -4 6 107.36 5.24 1 -4 -4 6 119.12 5.18 1 3 4 0 371.78 8.01 -2 -3 -4 6 371.78 8.01 1 -2 -4 6 20.24 1.43 1 -1 -4 6 117.55 4.97 1 0 -4 6 258.50 8.49 1 1 -4 6 949.31 35.22 1 2 -4 6 8.17 3.42 1 3 -4 6 1118.84 16.07 1 4 -4 6 728.79 21.73 1 5 -4 6 304.59 15.15 1 -6 4 8 195.37 12.68 -2 6 -4 6 195.37 12.68 1 7 -4 6 4.71 3.59 1 8 -4 6 128.36 9.65 1 -9 -3 6 110.85 14.80 1 -8 -3 6 2.96 3.05 1 -7 -3 6 34.74 3.56 1 -6 -3 6 78.66 9.19 1 -5 -3 1 87.69 4.34 -2 -5 -3 6 87.69 4.34 1 -4 -3 6 50.67 5.97 1 -3 -3 6 62.95 2.88 1 -2 -3 6 47.26 2.49 1 -1 -3 6 6.59 1.70 1 0 -3 6 558.22 16.78 1 1 -3 6 102.66 7.37 1 2 -3 6 118.39 4.37 1 3 -3 6 42.07 3.72 1 -4 3 7 36.57 5.50 -2 4 -3 6 36.57 5.50 1 5 -3 6 432.79 17.60 1 6 -3 6 238.94 14.10 1 7 -3 6 122.50 11.31 1 8 -3 6 72.17 12.68 1 -9 -2 6 2.98 8.74 1 -8 -2 6 34.19 4.50 1 -7 -2 6 267.83 9.33 1 -6 -2 1 513.55 11.54 -2 -6 -2 6 513.55 11.54 1 -5 -2 6 233.50 9.55 1 -4 -2 6 15.49 1.79 1 -3 -2 6 43.00 2.42 1 -2 -2 6 205.52 4.12 1 -1 -2 6 1762.50 11.54 1 0 -2 6 1699.34 20.56 1 1 -2 6 32.66 2.73 1 2 -2 6 150.39 6.69 1 -3 2 7 64.91 6.01 -2 3 -2 6 64.91 6.01 1 4 -2 6 150.70 10.51 1 5 -2 6 140.53 10.12 1 6 -2 6 540.78 21.11 1 7 -2 6 147.45 11.92 1 -9 -1 6 339.19 20.81 1 -8 -1 2 13.44 5.59 -2 -8 -1 6 13.44 5.59 1 -7 -1 6 37.92 4.51 1 -6 -1 6 19.05 2.20 1 -5 -1 6 307.13 5.23 1 -4 -1 6 277.83 5.30 1 -3 -1 6 365.12 7.00 1 -2 -1 6 72.67 3.08 1 -1 -1 6 37.07 2.92 1 0 -1 6 132.79 18.87 1 1 -1 6 315.61 7.32 1 2 -1 6 36.82 11.39 1 3 -1 6 112.97 4.47 1 4 -1 6 65.68 7.21 1 5 -1 6 99.93 8.63 1 6 -1 6 91.51 14.06 1 7 -1 6 55.50 11.42 1 -10 0 6 30.36 9.29 1 -9 0 2 97.77 11.45 -2 -9 0 6 97.77 11.45 1 -8 0 6 40.22 7.84 1 -7 0 6 21.46 5.63 1 -6 0 6 380.25 9.99 1 -5 0 6 994.99 8.84 1 -4 0 6 282.73 4.92 1 -3 0 6 17.34 1.43 1 -2 0 6 18.13 2.10 1 -1 0 6 472.64 11.96 1 0 0 6 3397.11 22.82 -2 0 0 6 3397.11 22.82 1 1 0 6 750.08 14.11 1 2 0 6 20.27 2.98 1 3 0 6 198.08 16.61 1 4 0 6 11.62 6.91 1 5 0 6 22.20 7.02 1 6 0 6 13.09 5.95 1 -10 1 6 15.54 6.13 1 -9 1 6 -3.51 5.29 1 -8 1 6 155.44 16.08 1 -7 1 6 0.47 3.38 1 -6 1 6 124.72 5.44 1 -5 1 6 161.42 4.93 1 -4 1 6 841.15 14.92 1 -3 1 6 46.97 3.51 1 -2 1 6 101.25 4.40 1 -1 1 6 654.89 13.66 1 0 1 6 146.49 5.12 1 1 1 6 52.02 8.07 1 2 1 6 173.33 15.46 1 3 1 6 -0.58 5.29 1 4 1 6 126.69 15.42 1 5 1 6 13.50 7.72 1 -10 2 6 16.68 7.53 1 -9 2 6 117.61 15.30 1 -8 2 6 1.05 3.12 1 -7 2 6 217.24 10.48 1 -6 2 6 -0.25 2.68 1 -5 2 6 727.60 8.54 1 -4 2 6 72.84 2.85 1 3 -2 5 32.95 2.20 -2 -3 2 6 32.95 2.20 1 -2 2 6 224.18 12.81 1 -1 2 6 3.24 3.27 1 0 2 6 1214.55 13.42 1 1 2 6 1279.29 38.88 1 2 2 6 97.16 11.94 1 3 2 6 5.29 4.65 1 4 2 6 147.76 16.73 1 5 2 6 7.52 7.23 1 -9 3 6 0.16 5.15 1 -8 3 6 114.97 8.58 1 -7 3 6 88.87 7.22 1 -6 3 6 406.28 16.95 1 -5 3 6 219.90 13.17 1 4 -3 5 0.69 1.61 -2 -4 3 6 0.69 1.61 1 -3 3 6 142.66 4.85 1 -2 3 6 14.92 4.00 1 -1 3 6 408.37 19.48 1 0 3 6 192.83 15.05 1 1 3 6 549.52 26.99 1 2 3 6 7.62 6.45 1 3 3 6 75.72 12.55 1 4 3 6 1.98 5.66 1 -9 4 6 22.73 5.94 1 -8 4 6 156.94 10.10 1 -7 4 6 229.10 10.64 1 6 -4 4 223.97 9.78 -2 -6 4 6 223.97 9.78 1 -5 4 6 9.78 2.54 1 -4 4 6 469.53 8.94 1 -3 4 6 -0.01 1.55 1 -2 4 6 212.18 13.58 1 -1 4 6 79.73 9.76 1 0 4 6 384.61 22.34 1 1 4 6 137.38 14.86 1 2 4 6 150.05 16.84 1 -3 -4 12 40.57 9.59 -2 3 4 6 40.57 9.59 1 -9 5 6 313.27 15.15 1 -8 5 6 56.84 6.20 1 7 -5 4 82.34 9.44 -2 -7 5 6 82.34 9.44 1 -6 5 6 142.90 8.17 1 -5 5 6 555.23 14.55 1 -4 5 6 13.14 4.00 1 -3 5 6 282.17 14.86 1 -2 5 6 25.09 5.86 1 -1 5 6 139.45 13.46 1 0 5 6 81.85 11.91 1 1 5 6 -0.17 4.58 1 -2 -5 12 254.89 22.65 -2 2 5 6 254.89 22.65 1 9 -6 3 136.60 17.89 -2 -9 6 6 136.60 17.89 1 -8 6 6 228.48 15.77 1 -7 6 6 18.25 5.99 1 -6 6 6 77.17 8.72 1 -5 6 6 439.63 20.51 1 -4 6 6 92.00 6.93 1 -3 6 6 345.52 23.75 1 -2 6 6 134.57 10.94 1 -1 6 6 105.52 12.65 1 0 -6 11 9.14 6.50 -2 0 6 6 9.14 6.50 1 1 6 6 172.30 18.75 1 -8 7 6 163.99 18.85 1 -7 7 6 4.47 5.31 1 -6 7 6 91.76 9.94 1 -5 7 6 66.97 8.33 1 -4 7 6 364.37 24.26 1 -3 7 6 277.32 15.11 1 -2 7 6 121.09 10.68 1 1 -7 11 72.92 9.48 -2 -1 7 6 72.92 9.48 1 0 7 6 126.56 15.94 1 -7 8 6 213.17 21.53 1 -6 8 6 -0.66 5.41 1 -5 8 6 17.75 7.10 1 -4 8 6 291.68 23.36 1 -3 8 6 75.11 8.49 1 -2 8 6 78.45 9.32 1 0 -10 7 13.77 8.06 1 1 -10 7 3.90 4.54 1 2 -10 7 86.09 8.23 1 3 -10 7 13.52 5.06 1 4 -10 7 74.47 9.22 1 -2 -9 7 7.22 6.95 1 -1 -9 7 113.37 9.38 1 0 -9 7 43.91 6.06 1 1 -9 7 202.75 11.57 1 2 -9 7 15.34 4.14 1 3 -9 7 14.36 4.25 1 -4 9 3 2.21 2.96 -2 4 -9 7 2.21 2.96 1 5 -9 7 17.58 4.66 1 6 -9 7 44.58 10.88 1 -4 -8 7 54.73 6.90 1 -3 -8 7 97.19 11.32 1 -2 -8 7 311.55 14.08 1 -1 -8 7 99.63 7.91 1 0 -8 7 30.97 4.63 1 1 -8 7 34.84 5.53 1 2 -8 7 -1.64 3.56 1 3 -8 7 29.73 6.11 1 4 -8 7 14.73 4.21 1 5 -8 7 265.87 23.87 1 6 -8 7 35.20 10.52 1 -6 -7 7 3.87 6.81 1 -5 -7 7 23.75 4.84 1 -4 -7 7 103.71 8.32 1 -3 -7 7 272.59 12.65 1 -2 -7 7 1.80 2.70 1 -1 -7 7 25.88 4.27 1 0 -7 7 342.32 16.34 1 -1 7 2 285.42 11.99 -2 1 -7 7 285.42 11.99 1 2 -7 7 98.30 12.82 1 3 -7 7 36.71 11.05 1 4 -7 7 7.38 3.35 1 5 -7 7 7.55 4.35 1 6 -7 7 85.81 9.29 1 7 -7 7 3.96 4.33 1 -7 -6 7 125.47 16.81 1 -6 -6 7 88.17 7.74 1 -5 -6 7 924.87 22.97 1 -4 -6 7 367.57 23.73 1 -3 -6 7 192.19 9.94 1 -2 -6 7 2.32 3.08 1 -1 -6 7 443.63 26.85 1 0 6 2 208.22 13.27 -2 0 -6 7 208.22 13.27 1 1 -6 7 851.56 19.62 1 2 -6 7 618.12 20.59 1 3 -6 7 38.22 4.95 1 4 -6 7 5.23 7.21 1 5 -6 7 114.28 10.45 1 6 -6 7 83.75 9.19 1 7 -6 7 3.67 3.85 1 -7 -5 7 3.75 3.51 1 -6 -5 7 57.53 5.22 1 -5 -5 7 225.85 7.78 1 -4 -5 7 203.02 6.88 1 -3 -5 7 54.26 3.78 1 2 5 1 356.58 12.09 -2 -2 -5 7 356.58 12.09 1 -1 -5 7 92.69 14.26 1 0 -5 7 2.95 1.78 1 1 -5 7 1111.74 16.75 1 2 -5 7 1029.58 25.64 1 3 -5 7 4.43 6.38 1 4 -5 7 56.50 7.14 1 5 -5 7 79.65 8.71 1 6 -5 7 34.01 6.32 1 -7 5 9 133.19 11.90 -2 7 -5 7 133.19 11.90 1 -8 -4 7 2.39 2.89 1 -7 -4 7 99.50 6.55 1 -6 -4 7 96.61 5.21 1 -5 -4 7 909.39 14.68 1 -4 -4 7 1521.71 26.11 1 3 4 1 219.38 5.46 -2 -3 -4 7 219.38 5.46 1 -2 -4 7 41.67 2.59 1 -1 -4 7 4.97 2.06 1 0 -4 7 591.30 12.74 1 1 -4 7 1.54 1.29 1 2 -4 7 3392.84 43.06 1 3 -4 7 485.64 17.49 1 4 -4 7 23.86 5.09 1 5 -4 7 21.81 4.58 1 -6 4 9 124.82 10.94 -2 6 -4 7 124.82 10.94 1 7 -4 7 37.41 6.60 1 -9 -3 7 57.69 11.39 1 -8 -3 7 5.44 3.97 1 -7 -3 7 86.97 6.74 1 -6 -3 7 227.22 7.46 1 5 3 0 34.35 2.97 -2 -5 -3 7 34.35 2.97 1 -4 -3 7 334.14 7.20 1 -3 -3 7 348.06 7.51 1 -2 -3 7 4.37 1.13 1 -1 -3 7 1004.93 16.75 1 0 -3 7 5.57 4.21 1 1 -3 7 39.72 7.62 1 2 -3 7 137.14 5.38 1 3 -3 7 475.12 16.71 1 -4 3 8 47.40 6.28 -2 4 -3 7 47.40 6.28 1 5 -3 7 59.10 7.26 1 6 -3 7 413.65 19.01 1 7 -3 7 148.93 20.09 1 -9 -2 7 15.05 4.99 1 -8 -2 7 334.56 15.82 1 -7 -2 7 23.35 4.35 1 6 2 0 197.56 6.38 -2 -6 -2 7 197.56 6.38 1 -5 -2 7 128.71 6.19 1 -4 -2 7 1731.17 15.47 1 -3 -2 7 752.05 11.23 1 -2 -2 7 286.50 5.20 1 -1 -2 7 2.51 1.08 1 0 -2 7 139.70 5.69 1 1 -2 7 410.39 9.84 1 2 -2 7 230.11 15.44 1 -3 2 8 2154.62 34.03 -2 3 -2 7 2154.62 34.03 1 4 -2 7 231.39 18.15 1 5 -2 7 156.54 11.16 1 6 -2 7 54.42 12.20 1 -9 -1 7 -3.61 3.61 1 -8 -1 1 4.72 5.21 -2 -8 -1 7 4.72 5.21 1 -7 -1 7 198.52 11.74 1 -6 -1 7 17.08 2.52 1 -5 -1 7 98.14 3.74 1 -4 -1 7 98.71 3.38 1 -3 -1 7 472.93 8.38 1 -2 -1 7 457.37 9.15 1 -1 -1 7 1329.81 16.83 1 0 -1 7 143.19 12.19 1 1 -1 7 8.21 2.37 1 2 -1 7 12.71 3.96 1 3 -1 7 5.16 5.33 1 4 -1 7 492.74 23.62 1 5 -1 7 7.77 5.40 1 6 -1 7 177.16 19.75 1 -10 0 7 111.69 15.52 1 -9 0 1 8.66 4.48 -2 -9 0 7 8.66 4.48 1 -8 0 7 7.39 5.25 1 -7 0 7 628.69 13.93 1 -6 0 7 1.42 1.76 1 -5 0 7 248.32 5.53 1 -4 0 7 167.49 4.80 1 -3 0 7 1935.76 14.41 1 -2 0 7 371.69 8.63 1 -1 0 7 718.25 28.37 1 0 0 7 375.67 8.20 -2 0 0 7 375.67 8.20 1 1 0 7 214.83 7.67 1 2 0 7 312.26 20.91 1 3 0 7 476.31 27.40 1 4 0 7 238.08 20.77 1 5 0 7 12.80 7.24 1 -10 1 7 48.49 10.83 1 -9 1 7 15.83 5.21 1 -8 1 7 19.25 3.70 1 -7 1 7 32.82 3.75 1 -6 1 7 387.88 9.80 1 -5 1 7 7.89 2.31 1 -4 1 7 18.46 1.08 1 -3 1 7 233.97 5.42 1 -2 1 7 182.26 6.29 1 -1 1 7 24.41 3.09 1 0 1 7 522.45 23.99 1 1 1 7 182.05 15.61 1 2 1 7 66.16 10.21 1 3 1 7 6.90 4.56 1 4 1 7 106.45 14.46 1 5 1 7 169.36 19.37 1 -9 2 7 0.40 4.50 1 -8 2 7 26.09 4.95 1 -7 2 7 125.21 8.48 1 -6 2 7 614.89 33.22 1 -5 2 7 58.37 5.06 1 -4 2 7 11.64 3.80 1 3 -2 6 240.85 8.57 -2 -3 2 7 240.85 8.57 1 -2 2 7 592.17 22.01 1 -1 2 7 377.29 15.90 1 0 2 7 997.47 34.23 1 1 2 7 317.39 20.88 1 2 2 7 473.35 27.11 1 3 2 7 4.64 5.49 1 4 2 7 46.76 10.31 1 -9 3 7 239.73 13.12 1 -8 3 7 4.04 4.89 1 -7 3 7 12.50 4.49 1 -6 3 7 108.07 9.97 1 -5 3 7 38.04 6.46 1 4 -3 6 93.30 6.81 -2 -4 3 7 93.30 6.81 1 -3 3 7 38.38 6.63 1 -2 3 7 315.42 16.74 1 -1 3 7 158.25 13.20 1 0 3 7 9.27 5.64 1 1 3 7 138.03 14.64 1 2 3 7 25.27 8.39 1 3 3 7 27.85 7.73 1 -9 4 7 48.26 6.62 1 -8 4 7 49.29 7.95 1 -7 4 7 48.98 7.15 1 6 -4 5 356.97 17.21 -2 -6 4 7 356.97 17.21 1 -5 4 7 182.94 12.62 1 -4 4 7 3.77 3.76 1 -3 4 7 61.27 5.25 1 -2 4 7 0.99 4.20 1 -1 4 7 225.28 16.73 1 0 4 7 262.90 19.78 1 1 4 7 186.96 18.03 1 2 4 7 95.57 13.94 1 -3 -4 13 240.79 23.61 -2 3 4 7 240.79 23.61 1 -8 5 7 280.24 17.34 1 7 -5 5 114.64 11.03 -2 -7 5 7 114.64 11.03 1 -6 5 7 121.84 11.02 1 -5 5 7 4.06 3.67 1 -4 5 7 151.81 11.44 1 -3 5 7 2.05 3.00 1 -2 5 7 161.64 13.58 1 -1 5 7 -1.46 4.25 1 0 5 7 5.06 6.01 1 1 5 7 17.66 7.27 1 2 5 7 17.86 8.19 1 -8 6 7 67.93 13.13 1 -7 6 7 320.76 19.20 1 -6 6 7 43.94 7.02 1 -5 6 7 463.84 28.82 1 -4 6 7 11.48 3.71 1 -3 6 7 25.81 7.46 1 -2 6 7 20.76 7.65 1 -1 6 7 9.56 5.58 1 0 -6 12 118.13 15.60 -2 0 6 7 118.13 15.60 1 1 6 7 47.31 11.05 1 -7 7 7 301.52 25.14 1 -6 7 7 198.73 20.32 1 -5 7 7 92.29 10.32 1 -4 7 7 12.33 4.98 1 -3 7 7 162.54 12.45 1 -2 7 7 47.03 8.38 1 0 7 7 54.58 11.33 1 -5 8 7 9.16 6.38 1 -4 8 7 52.04 11.09 1 2 -10 8 35.32 10.76 1 3 -10 8 171.75 19.32 1 4 -10 8 69.53 11.93 1 -2 -9 8 19.55 6.49 1 -1 -9 8 256.30 21.27 1 0 -9 8 20.67 4.66 1 1 -9 8 32.58 5.81 1 2 -9 8 119.28 9.25 1 3 -9 8 10.58 3.66 1 4 -9 8 455.78 17.96 1 5 -9 8 50.92 10.64 1 -4 -8 8 9.99 11.78 1 -3 -8 8 284.23 14.20 1 -2 -8 8 7.69 3.49 1 -1 -8 8 4.79 3.35 1 0 -8 8 190.79 10.81 1 1 -8 8 77.37 7.15 1 2 -8 8 59.21 6.78 1 3 -8 8 24.75 5.03 1 4 -8 8 199.78 10.04 1 5 -8 8 112.89 11.35 1 -6 -7 8 118.30 15.82 1 -5 -7 8 47.63 6.13 1 -4 -7 8 200.26 11.32 1 -3 -7 8 -1.68 3.25 1 -2 -7 8 472.20 16.44 1 -1 -7 8 50.32 7.65 1 0 -7 8 422.23 15.38 1 -1 7 3 39.42 7.20 -2 1 -7 8 39.42 7.20 1 2 -7 8 88.26 7.42 1 3 -7 8 161.24 11.83 1 4 -7 8 239.86 14.79 1 5 -7 8 13.76 5.08 1 6 -7 8 108.07 11.18 1 -6 -6 8 20.69 6.79 1 -5 -6 8 33.50 4.73 1 -4 -6 8 33.83 4.70 1 -3 -6 8 4.76 2.53 1 -2 -6 8 531.15 16.81 1 -1 -6 8 86.16 7.22 1 0 6 3 89.50 7.11 -2 0 -6 8 89.50 7.11 1 1 -6 8 103.40 7.35 1 2 -6 8 67.32 9.92 1 3 -6 8 52.75 7.06 1 4 -6 8 133.82 13.97 1 5 -6 8 12.16 4.70 1 6 -6 8 13.62 6.04 1 -7 -5 8 8.93 9.00 1 -6 -5 8 1.62 2.26 1 -5 -5 8 219.74 9.36 1 -4 -5 8 429.77 12.61 1 -3 -5 8 25.83 4.20 1 2 5 2 116.23 5.69 -2 -2 -5 8 116.23 5.69 1 -1 -5 8 696.52 13.01 1 0 -5 8 93.91 4.91 1 1 -5 8 621.05 20.86 1 2 -5 8 3.72 4.64 1 3 -5 8 336.61 15.98 1 4 -5 8 -0.99 6.98 1 5 -5 8 130.19 11.01 1 6 -5 8 7.21 15.00 1 7 -5 8 101.63 14.76 1 -8 -4 8 326.96 24.69 1 -7 -4 8 3.45 3.51 1 -6 -4 8 250.40 9.59 1 -5 -4 8 203.24 7.01 1 -4 -4 8 104.26 4.34 1 3 4 2 109.43 5.16 -2 -3 -4 8 109.43 5.16 1 -2 -4 8 7.85 2.17 1 -1 -4 8 719.81 13.35 1 0 -4 8 245.47 9.04 1 1 -4 8 22.74 7.10 1 2 -4 8 43.73 6.58 1 3 -4 8 29.83 5.27 1 4 -4 8 66.88 14.81 1 5 -4 8 125.14 10.67 1 -6 4 10 2.53 5.23 -2 6 -4 8 2.53 5.23 1 -8 -3 8 34.22 8.61 1 -7 -3 8 104.49 7.40 1 -6 -3 8 17.84 2.91 1 5 3 1 504.59 9.59 -2 -5 -3 8 504.59 9.59 1 -4 -3 8 172.81 5.32 1 -3 -3 8 320.77 8.20 1 -2 -3 8 88.08 5.00 1 -1 -3 8 54.02 4.66 1 0 -3 8 778.36 30.85 1 1 -3 8 285.62 8.12 1 2 -3 8 73.05 6.79 1 3 -3 8 2.86 2.83 1 -4 3 9 355.06 16.07 -2 4 -3 8 355.06 16.07 1 5 -3 8 20.65 6.28 1 6 -3 8 120.09 16.51 1 -9 -2 8 39.33 9.54 1 -8 -2 8 69.22 13.94 1 -7 -2 8 367.65 14.35 1 6 2 1 151.18 6.05 -2 -6 -2 8 151.18 6.05 1 -5 -2 8 1527.40 15.83 1 -4 -2 8 779.48 12.23 1 -3 -2 8 39.07 2.73 1 -2 -2 8 4.23 1.55 1 -1 -2 8 188.12 4.94 1 0 -2 8 3.73 1.85 1 1 -2 8 137.31 8.11 1 2 -2 8 827.66 20.42 1 -3 2 9 346.20 14.39 -2 3 -2 8 346.20 14.39 1 4 -2 8 63.58 11.74 1 5 -2 8 104.23 15.13 1 -9 -1 8 5.93 5.89 1 8 1 0 42.36 10.92 -2 -8 -1 8 42.36 10.92 1 -7 -1 8 51.64 5.33 1 -6 -1 8 430.36 11.55 1 -5 -1 8 80.51 6.85 1 -4 -1 8 1657.74 20.57 1 -3 -1 8 36.27 2.71 1 -2 -1 8 402.18 9.23 1 -1 -1 8 64.19 4.21 1 0 -1 8 11.28 2.56 1 1 -1 8 410.73 12.07 1 2 -1 8 244.14 19.75 1 3 -1 8 21.07 8.40 1 4 -1 8 34.37 9.47 1 5 -1 8 171.53 19.19 1 9 0 0 193.65 14.23 -2 -9 0 8 193.65 14.23 1 -8 0 8 8.52 3.79 1 -7 0 8 -0.06 3.21 1 -6 0 8 663.47 12.66 1 -5 0 8 562.63 12.46 1 -4 0 8 1897.58 30.16 1 -3 0 8 98.39 4.45 1 -2 0 8 1.47 1.47 1 -1 0 8 12.26 3.71 1 0 0 8 376.77 21.71 -2 0 0 8 376.77 21.71 1 1 0 8 -1.75 5.08 1 2 0 8 495.81 28.07 1 3 0 8 640.14 33.63 1 4 0 8 31.30 9.22 1 -9 1 8 78.03 9.06 1 -8 1 8 33.61 4.83 1 -7 1 8 88.97 6.20 1 -6 1 8 43.52 3.85 1 -5 1 8 727.32 13.53 1 -4 1 8 344.63 9.33 1 -3 1 8 509.75 15.74 1 -2 1 8 68.35 4.28 1 -1 1 8 629.61 14.75 1 0 1 8 80.86 10.58 1 1 1 8 271.01 20.32 1 2 1 8 3.77 4.36 1 3 1 8 341.53 25.38 1 4 1 8 3.35 5.81 1 -9 2 8 37.96 5.98 1 -8 2 8 419.19 16.27 1 -7 2 8 1.99 3.87 1 -6 2 8 9.18 4.44 1 -5 2 8 490.65 24.39 1 -4 2 8 663.95 20.37 1 3 -2 7 946.09 21.73 -2 -3 2 8 946.09 21.73 1 -2 2 8 154.82 16.50 1 -1 2 8 465.64 23.34 1 0 2 8 54.98 9.57 1 1 2 8 145.49 15.06 1 2 2 8 40.81 8.90 1 3 2 8 338.25 26.75 1 -9 3 8 86.37 8.44 1 -8 3 8 30.08 6.09 1 -7 3 8 306.30 16.61 1 -6 3 8 31.66 5.53 1 -5 3 8 166.89 11.86 1 4 -3 7 183.41 8.15 -2 -4 3 8 183.41 8.15 1 -3 3 8 44.57 4.58 1 -2 3 8 239.58 16.15 1 -1 3 8 4.27 3.67 1 0 3 8 467.03 26.17 1 1 3 8 43.32 9.19 1 2 3 8 31.49 9.10 1 3 3 8 24.93 9.55 1 -8 4 8 99.15 12.29 1 -7 4 8 196.17 18.64 1 6 -4 6 87.51 17.97 -2 -6 4 8 87.51 17.97 1 -5 4 8 24.28 5.34 1 -4 4 8 122.61 10.30 1 -3 4 8 478.48 18.53 1 -2 4 8 54.27 8.24 1 -1 4 8 136.85 14.00 1 0 4 8 261.93 20.71 1 1 4 8 1.41 4.68 1 2 4 8 117.02 16.11 1 -8 5 8 60.39 8.58 1 7 -5 6 102.54 10.83 -2 -7 5 8 102.54 10.83 1 -6 5 8 193.14 13.87 1 -5 5 8 45.54 6.99 1 -4 5 8 168.47 12.54 1 -3 5 8 4.45 12.11 1 -2 5 8 21.67 5.20 1 -1 5 8 5.69 4.76 1 0 5 8 60.21 11.03 1 1 5 8 95.96 14.70 1 -7 6 8 56.13 12.52 1 -6 6 8 222.50 23.19 1 -5 6 8 5.73 4.59 1 -4 6 8 79.72 9.58 1 -3 6 8 42.26 14.01 1 -2 6 8 43.41 10.94 1 -1 6 8 39.78 8.79 1 0 6 8 122.85 16.33 1 -1 -9 9 5.13 6.99 1 0 -9 9 39.30 6.02 1 1 -9 9 27.32 5.74 1 2 -9 9 176.57 14.20 1 3 -9 9 62.66 12.23 1 4 -9 9 -2.51 4.86 1 -4 -8 9 7.63 5.16 1 -3 -8 9 142.23 10.39 1 -2 -8 9 0.58 3.20 1 -1 -8 9 75.45 7.51 1 0 -8 9 40.38 5.82 1 1 -8 9 6.70 3.79 1 2 -8 9 235.41 12.65 1 3 -8 9 37.23 5.41 1 4 -8 9 -1.53 3.57 1 -6 -7 9 -0.07 4.43 1 -5 -7 9 97.05 8.30 1 -4 -7 9 152.64 10.16 1 -3 -7 9 461.82 17.05 1 -2 -7 9 204.54 12.58 1 -1 -7 9 94.52 7.81 1 0 -7 9 24.27 5.39 1 -1 7 4 212.94 11.44 -2 1 -7 9 212.94 11.44 1 2 -7 9 0.96 5.09 1 3 -7 9 277.47 16.21 1 4 -7 9 48.92 7.60 1 5 -7 9 3.35 4.29 1 -6 -6 9 100.34 8.16 1 -5 -6 9 2.11 3.32 1 -4 -6 9 423.71 15.53 1 -3 -6 9 6.79 3.03 1 -2 -6 9 2.88 3.17 1 -1 -6 9 5.56 3.18 1 0 6 4 485.99 17.29 -2 0 -6 9 485.99 17.29 1 1 -6 9 40.11 5.31 1 2 -6 9 298.14 22.90 1 3 -6 9 10.38 3.91 1 4 -6 9 19.50 8.14 1 5 -6 9 11.03 6.12 1 6 -6 9 11.39 6.73 1 -7 -5 9 197.94 19.91 1 -6 -5 9 34.42 4.27 1 -5 -5 9 40.19 4.43 1 -4 -5 9 197.29 8.87 1 -3 -5 9 455.32 15.72 1 2 5 3 226.46 8.24 -2 -2 -5 9 226.46 8.24 1 -1 -5 9 320.71 9.59 1 0 -5 9 294.43 9.20 1 1 -5 9 54.77 10.51 1 2 -5 9 413.57 18.92 1 3 -5 9 80.34 8.57 1 4 -5 9 122.87 10.79 1 5 -5 9 3.98 4.25 1 -8 -4 9 11.87 6.34 1 -7 -4 9 21.35 5.37 1 -6 -4 9 214.08 10.84 1 -5 -4 9 2.77 2.43 1 -4 -4 9 11.33 3.00 1 3 4 3 393.02 9.78 -2 -3 -4 9 393.02 9.78 1 -2 -4 9 19.71 3.00 1 -1 -4 9 30.75 3.46 1 0 -4 9 54.26 6.37 1 1 -4 9 603.19 30.35 1 2 -4 9 86.65 8.00 1 3 -4 9 118.71 9.69 1 4 -4 9 43.13 6.60 1 5 -4 9 11.80 7.33 1 -7 -3 9 17.30 7.11 1 -6 -3 9 65.20 5.71 1 5 3 2 214.76 6.51 -2 -5 -3 9 214.76 6.51 1 -4 -3 9 341.25 9.05 1 -3 -3 9 184.02 6.60 1 -2 -3 9 647.86 12.09 1 -1 -3 9 27.79 4.46 1 0 -3 9 220.55 17.91 1 1 -3 9 188.11 10.36 1 2 -3 9 62.17 6.80 1 3 -3 9 384.38 26.49 1 -4 3 10 115.30 15.97 -2 4 -3 9 115.30 15.97 1 5 -3 9 92.00 15.73 1 -8 -2 9 198.20 13.49 1 -7 -2 9 79.42 6.53 1 6 2 2 16.49 2.54 -2 -6 -2 9 16.49 2.54 1 -5 -2 9 11.85 2.50 1 -4 -2 9 4.46 2.05 1 -3 -2 9 71.79 3.87 1 -2 -2 9 50.43 3.56 1 -1 -2 9 -1.43 1.69 1 0 -2 9 103.20 4.86 1 1 -2 9 22.90 7.51 1 2 -2 9 76.99 12.17 1 -3 2 10 203.16 20.32 -2 3 -2 9 203.16 20.32 1 4 -2 9 114.27 16.61 1 -9 -1 9 219.60 20.47 1 8 1 1 32.15 6.15 -2 -8 -1 9 32.15 6.15 1 -7 -1 9 44.03 5.35 1 -6 -1 9 111.11 6.25 1 -5 -1 9 428.29 11.46 1 -4 -1 9 299.09 7.66 1 -3 -1 9 507.01 9.80 1 -2 -1 9 2.68 1.60 1 -1 -1 9 42.36 3.69 1 0 -1 9 15.32 6.05 1 1 -1 9 114.97 13.82 1 2 -1 9 60.03 11.94 1 3 -1 9 214.12 20.46 1 4 -1 9 41.87 10.47 1 9 0 1 28.51 7.99 -2 -9 0 9 28.51 7.99 1 -8 0 9 324.12 21.45 1 -7 0 9 65.35 6.40 1 -6 0 9 380.28 11.13 1 -5 0 9 88.38 5.39 1 -4 0 9 437.40 9.80 1 -3 0 9 16.29 3.77 1 -2 0 9 150.46 6.31 1 -1 0 9 3.56 6.55 1 0 0 9 51.28 9.50 -2 0 0 9 51.28 9.50 1 1 0 9 20.66 7.69 1 2 0 9 4.30 5.85 1 3 0 9 144.06 17.45 1 4 0 9 33.13 10.45 1 -9 1 9 6.43 3.60 1 -8 1 9 185.66 12.37 1 -7 1 9 165.12 10.04 1 -6 1 9 4.33 3.18 1 -5 1 9 320.57 9.62 1 -4 1 9 577.88 12.74 1 -3 1 9 135.50 6.24 1 -2 1 9 278.25 8.62 1 -1 1 9 29.85 7.35 1 0 1 9 128.57 14.61 1 1 1 9 120.61 14.62 1 2 1 9 83.79 12.61 1 3 1 9 82.57 13.81 1 -9 2 9 8.92 13.34 1 -8 2 9 23.30 4.68 1 -7 2 9 262.77 12.69 1 -6 2 9 52.77 5.83 1 -5 2 9 143.80 8.57 1 -4 2 9 726.21 14.58 1 3 -2 8 253.56 8.56 -2 -3 2 9 253.56 8.56 1 -2 2 9 20.28 5.14 1 -1 2 9 334.70 21.49 1 0 2 9 40.10 8.72 1 1 2 9 121.32 14.82 1 2 2 9 39.57 10.15 1 -8 3 9 35.02 7.24 1 -7 3 9 7.20 5.94 1 -6 3 9 288.33 16.21 1 -5 3 9 4.30 3.56 1 4 -3 8 336.08 16.78 -2 -4 3 9 336.08 16.78 1 -3 3 9 406.62 15.17 1 -2 3 9 165.47 11.20 1 -1 3 9 18.38 6.09 1 0 3 9 7.83 5.74 1 1 3 9 87.68 13.41 1 2 3 9 136.92 17.56 1 -8 4 9 47.22 11.24 1 -7 4 9 0.24 3.31 1 6 -4 7 96.18 10.14 -2 -6 4 9 96.18 10.14 1 -5 4 9 84.34 18.38 1 -4 4 9 176.12 12.80 1 -3 4 9 126.52 12.62 1 -2 4 9 6.92 4.10 1 -1 4 9 -5.37 5.37 1 0 4 9 17.37 7.49 1 1 4 9 0.58 5.19 1 7 -5 7 269.57 24.67 -2 -7 5 9 269.57 24.67 1 -6 5 9 63.62 12.95 1 -5 5 9 303.25 17.79 1 -4 5 9 51.13 7.90 1 -3 5 9 135.55 12.03 1 -2 5 9 28.33 9.30 1 -1 5 9 10.97 5.53 1 0 5 9 27.28 7.98 1 -3 -8 10 18.41 5.48 1 -2 -8 10 52.81 6.45 1 -1 -8 10 12.10 3.91 1 0 -8 10 4.58 3.36 1 1 -8 10 4.36 3.35 1 2 -8 10 45.06 6.48 1 3 -8 10 17.45 9.06 1 -6 -7 10 2.25 7.95 1 -5 -7 10 212.01 14.97 1 -4 -7 10 2.35 2.91 1 -3 -7 10 6.83 3.32 1 -2 -7 10 48.22 6.00 1 -1 -7 10 35.06 5.51 1 0 -7 10 47.52 9.10 1 -1 7 5 238.01 12.69 -2 1 -7 10 238.01 12.69 1 2 -7 10 11.83 5.45 1 3 -7 10 2.95 7.82 1 4 -7 10 12.08 5.94 1 5 -7 10 6.99 5.64 1 -6 -6 10 99.42 10.17 1 -5 -6 10 22.61 4.82 1 -4 -6 10 53.10 6.08 1 -3 -6 10 77.10 6.91 1 -2 -6 10 14.19 3.96 1 -1 -6 10 101.57 8.36 1 0 6 5 21.71 4.63 -2 0 -6 10 21.71 4.63 1 1 -6 10 18.56 5.51 1 2 -6 10 13.22 8.59 1 3 -6 10 7.69 4.38 1 4 -6 10 70.78 9.19 1 -7 -5 10 30.86 8.76 1 -6 -5 10 57.99 6.70 1 -5 -5 10 57.57 5.42 1 -4 -5 10 168.49 8.35 1 -3 -5 10 82.08 6.94 1 2 5 4 88.19 6.98 -2 -2 -5 10 88.19 6.98 1 -1 -5 10 163.57 9.81 1 0 -5 10 270.27 22.14 1 1 -5 10 21.30 7.88 1 2 -5 10 117.39 10.12 1 3 -5 10 9.98 6.22 1 4 -5 10 21.79 7.93 1 -7 -4 10 30.52 8.43 1 -6 -4 10 135.79 11.35 1 -5 -4 10 292.05 10.58 1 -4 -4 10 13.30 2.65 1 3 4 4 11.13 2.44 -2 -3 -4 10 11.13 2.44 1 -2 -4 10 91.18 5.83 1 -1 -4 10 158.08 10.04 1 0 -4 10 58.48 6.62 1 1 -4 10 28.53 5.09 1 2 -4 10 59.60 11.45 1 3 -4 10 37.75 10.09 1 4 -4 10 6.63 6.80 1 -7 -3 10 45.69 6.85 1 -6 -3 10 6.94 3.05 1 5 3 3 69.86 5.46 -2 -5 -3 10 69.86 5.46 1 -4 -3 10 85.81 4.89 1 -3 -3 10 328.59 10.18 1 -2 -3 10 3.39 2.63 1 -1 -3 10 162.89 10.51 1 0 -3 10 32.85 7.88 1 1 -3 10 63.60 11.27 1 2 -3 10 1.56 4.69 1 3 -3 10 137.15 18.05 1 -4 3 11 49.05 12.68 -2 4 -3 10 49.05 12.68 1 -7 -2 10 145.97 9.23 1 6 2 3 282.27 12.30 -2 -6 -2 10 282.27 12.30 1 -5 -2 10 2.21 2.65 1 -4 -2 10 487.33 15.00 1 -3 -2 10 76.65 4.18 1 -2 -2 10 105.42 6.89 1 -1 -2 10 44.91 6.35 1 0 -2 10 158.50 16.22 1 1 -2 10 56.05 11.04 1 2 -2 10 66.43 12.23 1 -3 2 11 142.88 17.67 -2 3 -2 10 142.88 17.67 1 8 1 2 13.68 5.14 -2 -8 -1 10 13.68 5.14 1 -7 -1 10 116.36 11.19 1 -6 -1 10 0.37 3.24 1 -5 -1 10 424.69 11.90 1 -4 -1 10 74.34 5.21 1 -3 -1 10 97.38 4.29 1 -2 -1 10 112.40 5.60 1 -1 -1 10 86.85 6.87 1 0 -1 10 64.80 11.21 1 1 -1 10 34.22 8.37 1 2 -1 10 109.94 14.95 1 3 -1 10 7.02 6.89 1 9 0 2 54.10 9.73 -2 -9 0 10 54.10 9.73 1 -8 0 10 4.14 5.37 1 -7 0 10 34.26 5.26 1 -6 0 10 79.42 6.69 1 -5 0 10 99.94 5.15 1 -4 0 10 449.27 11.75 1 -3 0 10 37.66 3.68 1 -2 0 10 23.08 3.78 1 -1 0 10 26.04 4.64 1 0 0 10 244.35 20.36 -2 0 0 10 244.35 20.36 1 1 0 10 209.79 20.02 1 2 0 10 36.84 10.39 1 3 0 10 109.68 16.78 1 -8 1 10 7.56 3.96 1 -7 1 10 33.69 5.05 1 -6 1 10 86.52 7.40 1 -5 1 10 9.31 3.15 1 -4 1 10 490.02 12.46 1 -3 1 10 193.78 9.40 1 -2 1 10 137.30 8.18 1 -1 1 10 1.20 3.86 1 0 1 10 351.45 24.47 1 1 1 10 46.75 10.41 1 2 1 10 0.80 5.25 1 -8 2 10 20.07 4.45 1 -7 2 10 0.35 3.01 1 -6 2 10 4.78 2.95 1 -5 2 10 24.29 4.65 1 -4 2 10 42.01 6.48 1 3 -2 9 425.75 14.21 -2 -3 2 10 425.75 14.21 1 -2 2 10 26.74 4.42 1 -1 2 10 93.36 12.17 1 0 2 10 -1.13 4.95 1 1 2 10 231.05 21.68 1 -8 3 10 63.22 8.55 1 -7 3 10 61.40 6.84 1 -6 3 10 11.27 3.66 1 -5 3 10 234.73 27.78 1 4 -3 9 21.14 5.49 -2 -4 3 10 21.14 5.49 1 -3 3 10 326.51 17.13 1 -2 3 10 25.25 4.50 1 -1 3 10 53.87 10.11 1 0 3 10 70.06 12.35 1 1 3 10 61.62 12.00 1 -7 4 10 10.00 6.79 1 6 -4 8 22.49 5.80 -2 -6 4 10 22.49 5.80 1 -5 4 10 12.19 5.31 1 -4 4 10 130.79 11.60 1 -3 4 10 267.65 16.52 1 -2 4 10 126.02 17.26 1 -1 4 10 -4.13 4.13 1 0 4 10 47.68 10.38 1 -5 5 10 74.22 12.93 1 -4 5 10 109.70 15.79 1 -3 5 10 26.43 9.35 1 -1 -8 11 10.22 7.62 1 -5 -7 11 91.01 14.49 1 -4 -7 11 92.96 10.19 1 -3 -7 11 31.56 5.32 1 -2 -7 11 26.35 5.17 1 -1 -7 11 55.09 6.61 1 0 -7 11 4.81 3.58 1 -1 7 6 81.49 7.93 -2 1 -7 11 81.49 7.93 1 2 -7 11 339.99 29.86 1 -5 -6 11 3.24 7.93 1 -4 -6 11 4.86 3.90 1 -3 -6 11 178.37 10.55 1 -2 -6 11 -0.90 2.73 1 -1 -6 11 62.49 6.80 1 0 6 6 28.20 6.40 -2 0 -6 11 28.20 6.40 1 1 -6 11 117.24 17.13 1 2 -6 11 169.23 19.99 1 -6 -5 11 35.87 9.83 1 -5 -5 11 6.27 3.30 1 -4 -5 11 14.93 3.48 1 -3 -5 11 36.21 5.22 1 2 5 5 45.04 5.61 -2 -2 -5 11 45.04 5.61 1 -1 -5 11 17.78 5.12 1 0 -5 11 134.48 16.32 1 1 -5 11 5.54 6.17 1 2 -5 11 208.92 21.88 1 -7 -4 11 84.01 12.88 1 -6 -4 11 49.54 7.56 1 -5 -4 11 2.07 3.38 1 -4 -4 11 54.08 5.10 1 3 4 5 6.41 2.57 -2 -3 -4 11 6.41 2.57 1 -2 -4 11 192.06 12.64 1 -1 -4 11 73.63 7.76 1 0 -4 11 0.37 3.38 1 1 -4 11 71.43 13.14 1 2 -4 11 50.97 12.26 1 3 -4 11 125.26 17.40 1 -7 -3 11 7.14 5.39 1 -6 -3 11 24.37 4.61 1 5 3 4 50.56 5.66 -2 -5 -3 11 50.56 5.66 1 -4 -3 11 67.54 11.22 1 -3 -3 11 1.91 2.15 1 -2 -3 11 2.44 2.37 1 -1 -3 11 2.26 2.64 1 0 -3 11 2.51 4.78 1 1 -3 11 144.50 17.76 1 2 -3 11 6.45 5.58 1 -7 -2 11 99.81 10.62 1 6 2 4 104.92 8.14 -2 -6 -2 11 104.92 8.14 1 -5 -2 11 21.54 4.26 1 -4 -2 11 8.80 4.39 1 -3 -2 11 24.64 3.90 1 -2 -2 11 45.54 6.63 1 -1 -2 11 3.22 4.73 1 0 -2 11 -4.47 4.47 1 1 -2 11 7.17 6.28 1 2 -2 11 72.42 13.30 1 -8 -1 11 268.21 24.73 1 -7 -1 11 10.58 6.71 1 -6 -1 11 0.20 2.65 1 -5 -1 11 134.29 7.00 1 -4 -1 11 70.18 5.31 1 -3 -1 11 10.03 3.10 1 -2 -1 11 53.15 7.03 1 -1 -1 11 81.20 8.70 1 0 -1 11 11.72 7.64 1 1 -1 11 28.90 10.41 1 2 -1 11 105.75 15.21 1 -7 0 11 399.82 16.20 1 -6 0 11 20.73 4.26 1 -5 0 11 107.03 7.73 1 -4 0 11 -0.95 2.76 1 -3 0 11 43.36 4.72 1 -2 0 11 44.61 4.98 1 -1 0 11 210.55 19.19 1 0 0 11 13.38 6.75 -2 0 0 11 13.38 6.75 1 1 0 11 63.74 12.12 1 -8 1 11 -5.62 5.62 1 -7 1 11 126.32 9.30 1 -6 1 11 111.57 8.36 1 -5 1 11 5.98 2.90 1 -4 1 11 0.88 6.95 1 -3 1 11 162.97 12.66 1 -2 1 11 79.35 6.80 1 -1 1 11 8.32 3.83 1 0 1 11 17.64 8.51 1 1 1 11 20.69 9.22 1 -8 2 11 19.82 8.32 1 -7 2 11 71.70 9.93 1 -6 2 11 134.33 9.37 1 -5 2 11 2.92 2.91 1 -4 2 11 315.27 16.99 1 3 -2 10 51.50 9.03 -2 -3 2 11 51.50 9.03 1 -2 2 11 104.59 7.98 1 -1 2 11 269.82 21.84 1 0 2 11 108.15 15.13 1 -7 3 11 42.56 7.04 1 -6 3 11 8.32 6.86 1 -5 3 11 153.66 13.19 1 4 -3 10 98.23 10.20 -2 -4 3 11 98.23 10.20 1 -3 3 11 2.95 3.49 1 -2 3 11 20.73 6.98 1 -1 3 11 96.68 13.95 1 0 3 11 5.84 6.78 1 -6 4 11 67.71 12.70 1 -5 4 11 28.90 9.62 1 -4 4 11 256.43 23.34 1 -3 4 11 120.04 17.02 1 -2 4 11 85.37 14.37 1 -3 -7 12 0.18 4.92 1 -2 -7 12 29.04 8.30 1 -1 -7 12 3.09 4.81 1 0 -7 12 65.46 13.33 1 -5 -6 12 300.01 24.48 1 -4 -6 12 6.68 6.16 1 -3 -6 12 92.57 11.69 1 -2 -6 12 115.23 9.22 1 -1 -6 12 115.70 21.40 1 0 6 7 42.33 7.43 -2 0 -6 12 42.33 7.43 1 -5 -5 12 126.87 11.53 1 -4 -5 12 20.01 4.99 1 -3 -5 12 107.35 8.25 1 2 5 6 88.52 9.40 -2 -2 -5 12 88.52 9.40 1 -1 -5 12 108.21 12.44 1 0 -5 12 193.35 21.10 1 1 -5 12 71.27 13.70 1 -6 -4 12 2.47 4.87 1 -5 -4 12 6.34 4.72 1 -4 -4 12 353.30 26.77 1 3 4 6 10.30 3.93 -2 -3 -4 12 10.30 3.93 1 -2 -4 12 46.45 5.50 1 -1 -4 12 57.53 7.47 1 0 -4 12 286.92 15.75 1 1 -4 12 15.82 8.10 1 -7 -3 12 3.44 6.37 1 -6 -3 12 25.04 5.56 1 5 3 5 84.74 7.36 -2 -5 -3 12 84.74 7.36 1 -4 -3 12 28.17 5.60 1 -3 -3 12 73.74 8.13 1 -2 -3 12 36.03 5.16 1 -1 -3 12 100.68 9.81 1 0 -3 12 18.53 5.52 1 1 -3 12 57.94 11.98 1 -7 -2 12 3.41 4.53 1 6 2 5 142.15 9.76 -2 -6 -2 12 142.15 9.76 1 -5 -2 12 19.57 4.21 1 -4 -2 12 77.80 7.05 1 -3 -2 12 57.01 10.43 1 -2 -2 12 13.21 4.75 1 -1 -2 12 19.58 5.14 1 0 -2 12 2.72 5.42 1 1 -2 12 241.87 23.41 1 -7 -1 12 75.22 9.78 1 -6 -1 12 80.83 9.31 1 -5 -1 12 57.42 7.21 1 -4 -1 12 80.35 6.88 1 -3 -1 12 47.20 7.07 1 -2 -1 12 48.86 7.12 1 -1 -1 12 -0.30 3.80 1 0 -1 12 205.45 20.89 1 1 -1 12 25.71 9.69 1 -7 0 12 82.73 14.13 1 -6 0 12 6.36 4.24 1 -5 0 12 204.70 14.78 1 -4 0 12 5.09 5.96 1 -3 0 12 19.22 5.21 1 -2 0 12 97.18 10.22 1 -1 0 12 106.95 10.80 1 0 0 12 42.06 10.75 -2 0 0 12 42.06 10.75 1 -8 1 12 -2.05 4.90 1 -7 1 12 146.46 12.12 1 -6 1 12 31.47 4.89 1 -5 1 12 240.26 14.86 1 -4 1 12 80.86 13.80 1 -3 1 12 15.63 7.86 1 -2 1 12 35.97 6.96 1 -1 1 12 56.19 11.28 1 0 1 12 174.37 19.38 1 -7 2 12 55.38 10.95 1 -6 2 12 8.27 4.87 1 -5 2 12 1.96 4.37 1 -4 2 12 105.51 13.98 1 -1 2 12 107.64 14.98 1 -6 3 12 11.28 5.77 1 -5 3 12 38.56 9.73 1 -4 3 12 107.41 14.90 1 -3 3 12 135.06 16.38 1 -2 -6 13 92.59 14.25 1 -1 -6 13 22.07 8.47 1 -1 -5 13 19.95 7.84 1 -6 -4 13 64.36 12.55 1 -5 -4 13 9.90 7.18 1 -4 -4 13 104.40 15.33 1 3 4 7 411.45 29.01 -2 -3 -4 13 411.45 29.01 1 -2 -4 13 103.95 16.36 1 -1 -4 13 8.29 6.77 1 -6 -3 13 40.93 10.05 1 -5 -3 13 36.75 6.09 1 -4 -3 13 3.71 4.36 1 -3 -3 13 22.85 4.63 1 -2 -3 13 75.96 8.78 1 -1 -3 13 15.96 4.50 1 0 -3 13 30.06 9.21 1 -6 -2 13 7.83 4.55 1 -5 -2 13 295.42 13.81 1 -4 -2 13 -0.64 3.38 1 -3 -2 13 74.58 8.75 1 -2 -2 13 19.86 5.15 1 -1 -2 13 13.78 4.83 1 0 -2 13 37.22 10.77 1 -6 -1 13 167.02 19.00 1 -5 -1 13 5.66 6.24 1 -4 -1 13 2.46 4.98 1 -3 -1 13 64.34 8.80 1 -2 -1 13 68.46 10.64 1 -1 -1 13 43.92 7.34 1 -4 0 13 340.92 27.86 1 -3 0 13 7.55 6.16 1 -2 0 13 35.55 9.76 1 -1 0 13 22.93 8.75 1 -4 -3 14 435.29 30.21 1 -3 -3 14 31.86 6.79 1 -2 -3 14 -3.06 5.09 1 -4 -2 14 182.61 19.92 1 -3 -2 14 12.58 4.38 1 -2 -2 14 13.81 5.18 1 -2 -1 14 4.35 5.33 1 0 0 0 0.00 0.00 0 TITL Olex2 generated HKLF5 file CELL 0.71073 8.0335 8.3743 10.4076 104.2960 104.6700 105.4190 ZERR 2.00000 0.0007 0.0008 0.0010 0.0090 0.0080 0.0080 BASF 0.1283 REM Matrix: -1.000 0 0 0 -1 0 0.8890.841 1 HKLF 5 ; _shelx_hkl_checksum 25536 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.9249(3) 0.2157(3) 0.5864(2) 0.0141(4) Uani 1 1 d . . . . . H1O H 1.005(5) 0.192(5) 0.610(4) 0.017 Uiso 1 1 d . U . . . O2 O 1.2052(3) 0.2268(3) 0.4807(2) 0.0157(4) Uani 1 1 d . . . . . O3 O 0.7734(3) 0.3452(2) 0.2861(2) 0.0122(4) Uani 1 1 d . . . . . N1 N 0.4576(3) 0.1368(3) 0.3818(2) 0.0102(5) Uani 1 1 d . . . . . H1N H 0.376(5) 0.165(4) 0.417(3) 0.012 Uiso 1 1 d . U . . . C1 C 0.9085(4) 0.3477(3) 0.2314(3) 0.0134(6) Uani 1 1 d . . . . . C2 C 1.0560(4) 0.3103(4) 0.2932(3) 0.0129(5) Uani 1 1 d . . . . . H2 H 1.143(5) 0.317(4) 0.258(4) 0.015 Uiso 1 1 d . U . . . C3 C 1.0733(4) 0.2637(3) 0.4164(3) 0.0119(5) Uani 1 1 d . . . . . C4 C 0.9222(4) 0.2588(3) 0.4700(3) 0.0108(5) Uani 1 1 d . . . . . C5 C 0.7805(4) 0.2998(3) 0.4040(3) 0.0101(5) Uani 1 1 d . . . . . C6 C 0.6201(4) 0.3060(3) 0.4495(3) 0.0110(5) Uani 1 1 d . . . . . H6A H 0.653(4) 0.338(4) 0.547(4) 0.013 Uiso 1 1 d . U . . . H6B H 0.577(4) 0.392(4) 0.424(3) 0.013 Uiso 1 1 d . U . . . C7 C 0.4898(4) -0.0141(4) 0.4232(3) 0.0118(5) Uani 1 1 d . . . . . H7A H 0.382(5) -0.114(4) 0.366(4) 0.014 Uiso 1 1 d . U . . . H7B H 0.596(5) -0.025(4) 0.407(3) 0.014 Uiso 1 1 d . U . . . C15 C 0.3892(4) 0.0863(4) 0.2241(3) 0.0150(6) Uani 1 1 d . . . . . H15A H 0.382(5) 0.191(5) 0.204(4) 0.022 Uiso 1 1 d . U . . . H15B H 0.474(5) 0.041(5) 0.194(4) 0.022 Uiso 1 1 d . U . . . H15C H 0.274(5) 0.004(5) 0.202(4) 0.022 Uiso 1 1 d . U . . . C16 C 0.8730(5) 0.3927(5) 0.1006(4) 0.0203(6) Uani 1 1 d . . . . . H16A H 0.950(5) 0.365(5) 0.043(4) 0.030 Uiso 1 1 d . U . . . H16B H 0.750(6) 0.321(5) 0.034(4) 0.030 Uiso 1 1 d . U . . . H16C H 0.890(5) 0.502(6) 0.118(4) 0.030 Uiso 1 1 d . U . . . O1W O 1.5450(3) 0.4433(3) 0.7414(3) 0.0224(5) Uani 1 1 d . . . . . H1WA H 1.577(6) 0.496(5) 0.835(5) 0.034 Uiso 1 1 d . U . . . H1WB H 1.452(6) 0.378(6) 0.720(5) 0.034 Uiso 1 1 d . U . . . Cl1 Cl 1.23754(9) 0.15992(8) 0.88243(7) 0.01202(18) Uani 1 1 d . . . . . O11 O 1.2163(3) 0.1424(3) 0.7358(2) 0.0187(5) Uani 1 1 d . . . . . O12 O 1.3679(4) 0.3317(3) 0.9691(3) 0.0306(6) Uani 1 1 d . . . . . O13 O 1.3052(3) 0.0285(3) 0.9158(2) 0.0213(5) Uani 1 1 d . . . . . O14 O 1.0649(3) 0.1400(4) 0.9012(3) 0.0321(6) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0127(10) 0.0218(10) 0.0136(10) 0.0102(9) 0.0057(8) 0.0099(9) O2 0.0112(10) 0.0246(11) 0.0159(10) 0.0078(9) 0.0071(8) 0.0100(8) O3 0.0128(10) 0.0145(9) 0.0139(10) 0.0075(8) 0.0077(8) 0.0065(8) N1 0.0075(10) 0.0135(11) 0.0119(12) 0.0050(9) 0.0052(9) 0.0048(9) C1 0.0169(14) 0.0113(12) 0.0162(14) 0.0053(11) 0.0113(12) 0.0056(11) C2 0.0134(13) 0.0125(12) 0.0150(14) 0.0039(11) 0.0094(12) 0.0041(11) C3 0.0095(12) 0.0094(12) 0.0149(14) 0.0016(10) 0.0051(11) 0.0021(10) C4 0.0112(13) 0.0099(12) 0.0118(13) 0.0041(10) 0.0052(11) 0.0029(10) C5 0.0116(13) 0.0066(11) 0.0124(13) 0.0033(10) 0.0059(11) 0.0017(10) C6 0.0109(13) 0.0114(12) 0.0133(14) 0.0053(11) 0.0060(11) 0.0049(10) C7 0.0120(13) 0.0104(12) 0.0148(14) 0.0047(11) 0.0062(11) 0.0046(11) C15 0.0130(14) 0.0213(15) 0.0101(14) 0.0061(12) 0.0023(11) 0.0061(12) C16 0.0280(17) 0.0243(16) 0.0215(16) 0.0154(14) 0.0158(15) 0.0152(14) O1W 0.0227(12) 0.0226(12) 0.0213(12) 0.0060(10) 0.0126(11) 0.0039(10) Cl1 0.0136(3) 0.0113(3) 0.0110(3) 0.0029(2) 0.0047(3) 0.0044(2) O11 0.0206(11) 0.0285(12) 0.0121(10) 0.0098(9) 0.0065(9) 0.0128(9) O12 0.0357(14) 0.0146(11) 0.0269(13) -0.0004(10) 0.0043(11) -0.0006(10) O13 0.0309(12) 0.0197(11) 0.0181(11) 0.0085(9) 0.0075(10) 0.0154(10) O14 0.0241(13) 0.0456(15) 0.0412(15) 0.0204(13) 0.0235(12) 0.0180(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 O1 H1O 110(3) . . ? C1 O3 C5 120.3(2) . . ? C7 N1 C15 110.1(2) . . ? C7 N1 C6 114.3(2) . . ? C15 N1 C6 111.6(2) . . ? C7 N1 H1N 108(2) . . ? C15 N1 H1N 110(2) . . ? C6 N1 H1N 102(2) . . ? O3 C1 C2 121.3(2) . . ? O3 C1 C16 112.4(2) . . ? C2 C1 C16 126.3(3) . . ? C1 C2 C3 121.5(2) . . ? C1 C2 H2 119(2) . . ? C3 C2 H2 119(2) . . ? O2 C3 C2 125.9(2) . . ? O2 C3 C4 118.9(2) . . ? C2 C3 C4 115.3(2) . . ? O1 C4 C5 119.9(2) . . ? O1 C4 C3 120.1(2) . . ? C5 C4 C3 120.0(2) . . ? C4 C5 O3 121.6(2) . . ? C4 C5 C6 125.8(2) . . ? O3 C5 C6 112.5(2) . . ? C5 C6 N1 113.9(2) . . ? C5 C6 H6A 111(2) . . ? N1 C6 H6A 109(2) . . ? C5 C6 H6B 110.1(19) . . ? N1 C6 H6B 105(2) . . ? H6A C6 H6B 107(3) . . ? N1 C7 C7 111.3(3) . 2_656 ? N1 C7 H7A 105(2) . . ? C7 C7 H7A 108(2) 2_656 . ? N1 C7 H7B 108(2) . . ? C7 C7 H7B 110(2) 2_656 . ? H7A C7 H7B 113(3) . . ? N1 C15 H15A 106(2) . . ? N1 C15 H15B 105(2) . . ? H15A C15 H15B 116(3) . . ? N1 C15 H15C 101(2) . . ? H15A C15 H15C 112(3) . . ? H15B C15 H15C 115(3) . . ? C1 C16 H16A 115(2) . . ? C1 C16 H16B 112(2) . . ? H16A C16 H16B 101(3) . . ? C1 C16 H16C 112(3) . . ? H16A C16 H16C 107(3) . . ? H16B C16 H16C 110(3) . . ? H1WA O1W H1WB 105(4) . . ? O14 Cl1 O13 110.80(14) . . ? O14 Cl1 O12 110.28(16) . . ? O13 Cl1 O12 109.85(15) . . ? O14 Cl1 O11 109.24(14) . . ? O13 Cl1 O11 108.72(12) . . ? O12 Cl1 O11 107.87(14) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C4 1.344(3) . ? O1 H1O 0.72(4) . ? O2 C3 1.258(3) . ? O3 C1 1.345(3) . ? O3 C5 1.364(3) . ? N1 C7 1.495(3) . ? N1 C15 1.501(4) . ? N1 C6 1.505(3) . ? N1 H1N 0.88(3) . ? C1 C2 1.351(4) . ? C1 C16 1.480(4) . ? C2 C3 1.415(4) . ? C2 H2 0.87(3) . ? C3 C4 1.454(4) . ? C4 C5 1.347(4) . ? C5 C6 1.490(4) . ? C6 H6A 0.93(3) . ? C6 H6B 0.94(3) . ? C7 C7 1.517(5) 2_656 ? C7 H7A 0.95(3) . ? C7 H7B 0.94(3) . ? C15 H15A 0.96(4) . ? C15 H15B 0.94(4) . ? C15 H15C 0.92(4) . ? C16 H16A 1.00(4) . ? C16 H16B 0.97(4) . ? C16 H16C 0.85(4) . ? O1W H1WA 0.90(5) . ? O1W H1WB 0.74(5) . ? Cl1 O14 1.421(2) . ? Cl1 O13 1.428(2) . ? Cl1 O12 1.435(2) . ? Cl1 O11 1.457(2) . ?