Crystallography Open Database

Information card for entry 7062093

7062092 << 7062093 >> 7062094

Preview

Coordinates	7062093.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H14 Cl2 N2 O5
Calculated formula	C19 H14 Cl2 N2 O5
Title of publication	A solvent controlled three-component reaction of diazo compounds for the synthesis of hydrazone compounds under Brønsted acid catalysis
Authors of publication	He, Hangli; Yan, Zhewei; Wang, Junyong; Yan, Qiongjiao; Wang, Wei; Wang, Haifeng; Chen, Fener
Journal of publication	New Journal of Chemistry
Year of publication	2022
Journal volume	46
Journal issue	47
Pages of publication	22513 - 22517
a	13.1812 ± 0.0018 Å
b	14.144 ± 0.002 Å
c	20.391 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	3801.6 ± 0.9 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.2151
Residual factor for significantly intense reflections	0.069
Weighted residual factors for significantly intense reflections	0.1484
Weighted residual factors for all reflections included in the refinement	0.1926
Goodness-of-fit parameter for all reflections included in the refinement	0.97
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
280198 (current)	2023-01-06	cif/ Updating files of 7062093, 7062094 Original log message: Adding full bibliography for 7062093--7062094.cif.	7062093.cif
279521	2022-11-24	cif/ Adding structures of 7062093, 7062094 via cif-deposit CGI script.	7062093.cif