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Information card for entry 7101188
Preview
| Coordinates | 7101188.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C36 H43 B Cl4 F6 N9 O P2 Rh S3 |
|---|---|
| Calculated formula | C36 H43 B Cl4 F6 N9 O P2 Rh S3 |
| Title of publication | The oxidative activation of a B-H bond: novel route to metallaboratrane complexes |
| Authors of publication | Adams, C.J.; Blagg, R.J.; Charmant, J.P.H.; Connelly, N.G.; Haddow, M.F.; Orpen, A.G. |
| Journal of publication | Chemical Communications |
| Year of publication | 2006 |
| Journal issue | 22 |
| a | 12.8991 ± 0.0019 Å |
| b | 14.035 ± 0.002 Å |
| c | 14.286 ± 0.002 Å |
| α | 68.377 ± 0.005° |
| β | 88.304 ± 0.006° |
| γ | 87.738 ± 0.005° |
| Cell volume | 2402.1 ± 0.6 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 10 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0997 |
| Residual factor for significantly intense reflections | 0.0552 |
| Weighted residual factors for significantly intense reflections | 0.1188 |
| Weighted residual factors for all reflections included in the refinement | 0.1364 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.021 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 277870 (current) | 2022-09-15 | cif/ Added space group information derived from the space group operation list using the 'cif_filter' program. |
7101188.cif |
| 180113 | 2016-03-26 | cif/7/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/10/11. |
7101188.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7101188.cif |
| 91955 | 2013-12-31 | cod/ (saulius@koala.ibt.lt) Removing '_journal_page_first ?' data items from a bunch of COD CIFs so that the quastion mark does not appear in the COD SQL tables as a page number. |
7101188.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7101188.cif |
| 966 | 2010-01-30 | cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated. |
7101188.cif |
| 271 | 2008-03-15 | Adding CIF files from the Chem-Comm-2006-20_48/ deposion. |
7101188.cif |
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Users of the data should acknowledge the original authors of the
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