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Information card for entry 7103957
Preview
| Coordinates | 7103957.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C146 H172 B9 Cu12 F36 N80 Na O39 |
|---|---|
| Calculated formula | C144 H80 B8 Cu12 F32 N80 Na O35 |
| Title of publication | Synthesis, structure and magnetism of a unique dodecanuclearcopper(ii) 'picture frame' held in a 4 × 4 grid-like assembly |
| Authors of publication | Matthews, Craig J.; Onions, Stuart T.; Morata, Gérald; Salvia, Margarita Bosch; Elsegood, Mark R. J.; Price, Daniel J. |
| Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
| Year of publication | 2003 |
| Journal issue | 3 |
| Pages of publication | 320 - 321 |
| a | 21.3049 ± 0.0011 Å |
| b | 21.3272 ± 0.0011 Å |
| c | 24.7637 ± 0.0013 Å |
| α | 75.286 ± 0.002° |
| β | 77.638 ± 0.002° |
| γ | 65.984 ± 0.002° |
| Cell volume | 9862.5 ± 0.9 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1395 |
| Residual factor for significantly intense reflections | 0.0839 |
| Weighted residual factors for significantly intense reflections | 0.2251 |
| Weighted residual factors for all reflections included in the refinement | 0.2543 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.993 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288008 (current) | 2023-12-04 | cif/7/10/39/ Updated bibliographic information in entry 7103957. |
7103957.cif |
| 213973 | 2019-03-05 | cod/ Removed potentially copyrighted or irrelevant data items from 1289 entries. |
7103957.cif |
| 180142 | 2016-03-26 | cif/7/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/10/39. |
7103957.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7103957.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7103957.cif |
| 966 | 2010-01-30 | cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated. |
7103957.cif |
| 823 | 2009-09-25 | cif/ Depositing information from the Chem-Comm-2003_01-17 and J-Org-Chem-2007_13-20 publications. |
7103957.cif |
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