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Information card for entry 7105136
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| Coordinates | 7105136.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | 2,6-Bis(dimethoxyphosphoryl)-1,2,3,4-tetrahydroquinoline |
|---|---|
| Chemical name | 2,6-Bis(dimethoxyphosphoryl)-1,2,3,4-tetrahydroquinoline |
| Formula | C13 H20 N2 O8 P2 |
| Calculated formula | C12.999 H19.997 N2 O8 P2 |
| Title of publication | One-pot tandem 1,4-1,2-addition of phosphites to quinolines. |
| Authors of publication | De Blieck, Ann; Masschelein, Kurt G R; Dhaene, Fréderic; Rozycka-Sokolowska, Ewa; Marciniak, Bernard; Drabowicz, Jozef; Stevens, Christian V |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2009 |
| Journal volume | 46 |
| Journal issue | 2 |
| Pages of publication | 258 - 260 |
| a | 10.0124 ± 0.0004 Å |
| b | 10.3614 ± 0.0005 Å |
| c | 10.4335 ± 0.0004 Å |
| α | 63.537 ± 0.004° |
| β | 80.792 ± 0.003° |
| γ | 67.351 ± 0.004° |
| Cell volume | 894.17 ± 0.07 Å3 |
| Cell temperature | 292 ± 2 K |
| Ambient diffraction temperature | 292 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0996 |
| Residual factor for significantly intense reflections | 0.0572 |
| Weighted residual factors for significantly intense reflections | 0.1309 |
| Weighted residual factors for all reflections included in the refinement | 0.1463 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 201210 (current) | 2017-09-25 | cif/ Moving the _symmetry_cell_setting data item out of the loop in entries 1513161, 2100005, 2100006, 2202914, 4100109, 4100110, 4100111, 4100242, 4100265, 4100289, 4100287, 4100288, 4100590, 4334471, 7105136. |
7105136.cif |
| 180155 | 2016-03-26 | cif/7/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/10/51. |
7105136.cif |
| 106664 | 2014-03-15 | cif/ (saulius@koala.ibt.lt) Adding DOIs to the rest of the Chem. Comm. files. Some of these files have author names differing from PubMed in diacritics (either diacritics are omitted or we have encoding problems); or they have a year difference of 1. However, since first pages always match and author names are variants of each other, I assume that DOIs are assigned correctly. |
7105136.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7105136.cif |
| 969 | 2010-02-01 | cod/cif/ Depositing CIFs from Chem-Comm-2010_1-5 processing directory. |
7105136.cif |
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