Crystallography Open Database

Information card for entry 7109446

Preview

Coordinates	7109446.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C154 H126 Cl0 Cu8 F30 N12 O40 P6 S10 Se6
Calculated formula	C154 H126 Cu8 F30 N12 O40 P6 S10 Se6
Title of publication	Syntheses of CuI polymetallic assemblies from reaction of ligands bearing the 2,5-bis(2-pyridyl)phosphole fragment with CuII precursors
Authors of publication	Mehdi El Sayed Moussa; Fabian Friess; Wenting Shen; Muriel Hissler; Regis Reau; Christophe Lescop
Journal of publication	Chem.Commun.
Year of publication	2013
Journal volume	49
Pages of publication	6158
a	16.945 ± 0.001 Å
b	18.478 ± 0.001 Å
c	20.154 ± 0.001 Å
α	107.916 ± 0.002°
β	104.98 ± 0.002°
γ	112.985 ± 0.002°
Cell volume	4984.7 ± 0.5 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	10
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1005
Residual factor for significantly intense reflections	0.0591
Weighted residual factors for significantly intense reflections	0.1535
Weighted residual factors for all reflections included in the refinement	0.171
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180198 (current)	2016-03-26	cif/7/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/10/94.	7109446.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7109446.cif
86340	2013-06-21	cif/ Adding structures of 7109442, 7109443, 7109444, 7109445, 7109446, 7109447 via cif-deposit CGI script.	7109446.cif