Crystallography Open Database

Information card for entry 7110248

Preview

Coordinates	7110248.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	tetramethylammonium pentaniobotellurate hydrate
Formula	C20 H94 N5 Nb5 O39.25 Te
Calculated formula	C20 H94 N5 Nb5.046 O39.29 Te0.954
Title of publication	A tellurium-substituted Lindqvist-type polyoxoniobate showing high H2 evolution catalyzed by tellurium nanowires via photodecomposition
Authors of publication	Jung-Ho Son; Jiarui Wang; Frank E. Osterloh; Ping Yu; William H. Casey
Journal of publication	Chem.Commun.
Year of publication	2014
Journal volume	50
Pages of publication	836
a	33.87 ± 0.0015 Å
b	8.4954 ± 0.0004 Å
c	21.9238 ± 0.001 Å
α	90°
β	110.475 ± 0.001°
γ	90°
Cell volume	5909.8 ± 0.5 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.019
Residual factor for significantly intense reflections	0.0163
Weighted residual factors for significantly intense reflections	0.0397
Weighted residual factors for all reflections included in the refinement	0.0407
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180216 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/02.	7110248.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7110248.cif
93830	2014-01-15	cif/ Adding structures of 7110248 via cif-deposit CGI script.	7110248.cif