Crystallography Open Database

Information card for entry 7110260

Preview

Coordinates	7110260.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H72 F N10 Zn2
Calculated formula	C64 H72 F N10 Zn2
Title of publication	Reactions of a Zn(I) complex with group 14 azides ‒ formation of zinc azide and zinc hexazene complexes
Authors of publication	S. Gondzik; S. Schulz; D. Blaser; C. Wolper; R. Haack; G. Jansena
Journal of publication	Chem.Commun.
Year of publication	2014
Journal volume	50
Pages of publication	927
a	12.8569 ± 0.0009 Å
b	17.7885 ± 0.0013 Å
c	13.5948 ± 0.001 Å
α	90°
β	104.691 ± 0.004°
γ	90°
Cell volume	3007.6 ± 0.4 Å³
Cell temperature	180 ± 1 K
Ambient diffraction temperature	180 ± 1 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0618
Residual factor for significantly intense reflections	0.0395
Weighted residual factors for significantly intense reflections	0.1043
Weighted residual factors for all reflections included in the refinement	0.1178
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180216 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/02.	7110260.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7110260.cif
93863	2014-01-20	cif/ Adding structures of 7110260 via cif-deposit CGI script.	7110260.cif