Crystallography Open Database

Information card for entry 7110308

Preview

Coordinates	7110308.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H18 Cl2 Cu F24 N2 Sb
Calculated formula	C37 H18 Cl2 Cu F24 N2 Sb
Title of publication	Oxidation-resistant, sterically demanding phenanthrolines as supporting ligands for copper(i) nitrene transfer catalystsElectronic Supplementary Information (ESI) available: Synthesis of 1?4?, with spectroscopic and analytical details; crystallographic data plus additional structures. See http://www.rsc.org/suppdata/cc/b4/b404515g/
Authors of publication	Hamilton, Charles W.; Laitar, David S.; Sadighi, Joseph P.
Journal of publication	Chemical Communications
Year of publication	2004
Journal issue	14
Pages of publication	1628 - 1629
a	12.8498 ± 0.0011 Å
b	17.2274 ± 0.0014 Å
c	19.3942 ± 0.0016 Å
α	88.865 ± 0.002°
β	85.991 ± 0.002°
γ	72.624 ± 0.002°
Cell volume	4087.3 ± 0.6 Å³
Cell temperature	194 ± 2 K
Ambient diffraction temperature	194 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0893
Residual factor for significantly intense reflections	0.0687
Weighted residual factors for significantly intense reflections	0.1748
Weighted residual factors for all reflections included in the refinement	0.2015
Goodness-of-fit parameter for all reflections included in the refinement	1.124
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180217 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/03.	7110308.cif
94355	2014-01-23	cif/ Adding structures of 7110307, 7110308 via cif-deposit CGI script.	7110308.cif