Crystallography Open Database

Information card for entry 7110555

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Structure parameters

Formula	C24 H40 P2 Sn
Calculated formula	C24 H40 P2 Sn
Title of publication	2,5-Di-(tert-butyl)phospholyl sandwich complexes containing group 14 elements (Ge, Sn, Pb). Synthesis, molecular structure, and ring transfer chemistry of [M(PC4H2But2)2] (M= Sn, Pb)
Authors of publication	Forissier, Kareen; Ricard, Louis; Carmichael, Duncan; Mathey, François
Journal of publication	Chemical Communications
Year of publication	1999
Journal issue	14
Pages of publication	1273
a	16.046 ± 0.0002 Å
b	20.328 ± 0.0002 Å
c	16.374 ± 0.0002 Å
α	90°
β	101.089 ± 0.0006°
γ	90°
Cell volume	5241.2 ± 0.11 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0305
Residual factor for significantly intense reflections	0.0278
Weighted residual factors for significantly intense reflections	0.0737
Weighted residual factors for all reflections included in the refinement	0.0754
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301857 (current)	2025-08-22	Add cross-references to PubChem compounds in COD range 7/11/ Each referenced PubChem compound corresponds to the full crystal structure.	7110555.cif
180219	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/05.	7110555.cif
95389	2014-01-28	cif/ Adding structures of 7110554, 7110555 via cif-deposit CGI script.	7110555.cif