Crystallography Open Database

Information card for entry 7110569

Preview

Coordinates	7110569.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H29 Li N2 O P
Calculated formula	C21 H29 Li N2 O P
Title of publication	Lithiated organophosphorus enamines: a new synthetic approach and the first crystal structures
Authors of publication	Clegg, William; Liddle, Stephen T.; Davies, Robert P.; Dunbar, Lorraine; Feeder, Neil; Snaith, Ronald; Wheatley, Andrew E. H.; Mulvey, Robert E.
Journal of publication	Chemical Communications
Year of publication	1999
Journal issue	15
Pages of publication	1401
a	27.74 ± 0.006 Å
b	9.803 ± 0.002 Å
c	20.206 ± 0.004 Å
α	90°
β	130.69 ± 0.03°
γ	90°
Cell volume	4166 ± 2 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1363
Residual factor for significantly intense reflections	0.0634
Weighted residual factors for significantly intense reflections	0.1201
Weighted residual factors for all reflections included in the refinement	0.1464
Goodness-of-fit parameter for all reflections included in the refinement	0.96
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180219 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/05.	7110569.cif
95414	2014-01-28	cif/ Adding structures of 7110567, 7110568, 7110569 via cif-deposit CGI script.	7110569.cif