Crystallography Open Database

Information card for entry 7110810

Preview

Coordinates	7110810.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C80 H60 Ag2 B2 Cl1.5 F8 N1.5 O3 P6
Calculated formula	C79.99 H60 Ag2 B1.998 Cl1.5 F8 N1.49 O2.98 P6
Title of publication	Triply-bridged diphos disilver helical complexes [Ag2(μ2-dppa-P,P′)3(anion)2] [dppa = bis(diphenylphosphino)acetylene]
Authors of publication	James, Stuart L.; Lozano, Elvira; Nieuwenhuyzen, Mark
Journal of publication	Chemical Communications
Year of publication	2000
Journal issue	7
Pages of publication	617
a	22.1929 ± 0.0016 Å
b	14.8355 ± 0.0018 Å
c	23.8561 ± 0.0013 Å
α	90°
β	99.46 ± 0.006°
γ	90°
Cell volume	7747.6 ± 1.2 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0674
Residual factor for significantly intense reflections	0.0448
Weighted residual factors for significantly intense reflections	0.0963
Weighted residual factors for all reflections included in the refinement	0.1067
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7110810.cif
95926	2014-01-28	cif/ Adding structures of 7110810 via cif-deposit CGI script.	7110810.cif