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Information card for entry 7111224
Preview
| Coordinates | 7111224.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H68 P2 |
|---|---|
| Calculated formula | C42 H58 P2 |
| Title of publication | Preparation of 2,4-bis(2,4,6-tri-tert-butylphenyl)-1,3-diphosphacyclobutenes from 2-(2,4,6-tri-tert-butylphenyl)-1-phosphaethyne and alkyllithiums |
| Authors of publication | Ito, Shigekazu; Sugiyama, Hiroki; Yoshifuji, Masaaki |
| Journal of publication | Chemical Communications |
| Year of publication | 2002 |
| Journal issue | 16 |
| Pages of publication | 1744 |
| a | 13.592 ± 0.002 Å |
| b | 14.861 ± 0.002 Å |
| c | 10.916 ± 0.002 Å |
| α | 98.722 ± 0.003° |
| β | 98.76 ± 0.002° |
| γ | 67.629 ± 0.009° |
| Cell volume | 2004.6 ± 0.6 Å3 |
| Cell temperature | 110.2 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 0.1384 |
| Weighted residual factors for all reflections included in the refinement | 0.3198 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.914 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176453 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7. |
7111224.cif |
| 96365 | 2014-01-29 | cif/ Adding structures of 7111224 via cif-deposit CGI script. |
7111224.cif |
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Users of the data should acknowledge the original authors of the
structural data.