Crystallography Open Database

Information card for entry 7111583

Preview

Coordinates	7111583.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H62 Eu N4 O1.5
Calculated formula	C48 H58 Eu N4 O1.5
Title of publication	New reaction of β-diketiminatoeuropium complex: sterically induced oxidation‒coupling of β-diketiminato ligands
Authors of publication	Jiao, Rui; Shen, Xiaodong; Xue, Mingqiang; Zhang, Yong; Yao, Yingming; Shen, Qi
Journal of publication	Chemical Communications
Year of publication	2010
Journal volume	46
Journal issue	23
Pages of publication	4118 - 4120
a	11.2725 ± 0.0013 Å
b	20.602 ± 0.002 Å
c	19.583 ± 0.002 Å
α	90°
β	91.485 ± 0.003°
γ	90°
Cell volume	4546.4 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0784
Residual factor for significantly intense reflections	0.0576
Weighted residual factors for significantly intense reflections	0.094
Weighted residual factors for all reflections included in the refinement	0.1008
Goodness-of-fit parameter for all reflections included in the refinement	1.188
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7111583.cif
96677	2014-01-29	cif/ Adding structures of 7111583, 7111584, 7111585 via cif-deposit CGI script.	7111583.cif