Crystallography Open Database

Information card for entry 7111617

Preview

Coordinates	7111617.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H42 Li2 O4 Si2
Calculated formula	C16 H42 Li2 O4 Si2
Title of publication	The first asymmetric organolithium tetramers with simple ether donor bases
Authors of publication	Tatic, Tanja; Meindl, Kathrin; Henn, Julian; Pandey, Sushil Kumar; Stalke, Dietmar
Journal of publication	Chemical Communications
Year of publication	2010
Journal volume	46
Journal issue	25
Pages of publication	4562 - 4564
a	10.4667 ± 0.0008 Å
b	18.3838 ± 0.0013 Å
c	19.267 ± 0.0014 Å
α	90°
β	92.89 ± 0.001°
γ	90°
Cell volume	3702.6 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0324
Residual factor for significantly intense reflections	0.0287
Weighted residual factors for significantly intense reflections	0.0755
Weighted residual factors for all reflections included in the refinement	0.0778
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180230 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/16.	7111617.cif
96702	2014-01-29	cif/ Adding structures of 7111616, 7111617, 7111618 via cif-deposit CGI script.	7111617.cif