Crystallography Open Database

Information card for entry 7112009

7112008 << 7112009 >> 7112010

Preview

Coordinates	7112009.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C280 H436 Ag70 B10 F40 N4 O73 P2 W18
Calculated formula	C280 H426 Ag70 B10 F40 N4 O73 P2 W18
Title of publication	Ag70(PW9O34)2(tBuC[triple bond, length as m-dash]C)44(H2O)2]8+: ionothermal synthesis of a silver cluster encapsulating lacunary polyoxometalate ions
Authors of publication	Zhan-Guo Jiang; Kang Shi; Yu-Mei Lin; Quan-Ming Wang
Journal of publication	Chem.Commun.
Year of publication	2014
Journal volume	50
Pages of publication	2353
a	24.1791 ± 0.0005 Å
b	22.448 ± 0.0005 Å
c	39.8847 ± 0.0012 Å
α	90°
β	106.426 ± 0.003°
γ	90°
Cell volume	20764.8 ± 0.9 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0915
Residual factor for significantly intense reflections	0.0532
Weighted residual factors for significantly intense reflections	0.0864
Weighted residual factors for all reflections included in the refinement	0.0971
Goodness-of-fit parameter for all reflections included in the refinement	0.978
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180234 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/20.	7112009.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7112009.cif
103338	2014-02-28	cif/ Adding structures of 7112009 via cif-deposit CGI script.	7112009.cif