Crystallography Open Database

Information card for entry 7112862

Preview

Coordinates	7112862.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27.5 H23 Cr N O4
Calculated formula	C27.5 H17 Cr N O4
Title of publication	Induction of axially chiral N-C bonds in N-aryl acridane and related complexes by chromium tricarbonyl migration reactions.
Authors of publication	Mori, Akiyoshi; Kinoshita, Shunsuke; Furusyo, Masaru; Kamikawa, Ken
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2010
Journal volume	46
Journal issue	36
Pages of publication	6846 - 6848
a	10.867 ± 0.004 Å
b	14.49 ± 0.007 Å
c	14.911 ± 0.004 Å
α	86.888 ± 0.015°
β	78.146 ± 0.014°
γ	87.429 ± 0.017°
Cell volume	2293.1 ± 1.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0672
Residual factor for significantly intense reflections	0.047
Weighted residual factors for significantly intense reflections	0.1303
Weighted residual factors for all reflections included in the refinement	0.1448
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7112862.cif
112128	2014-04-29	cif/ Adding structures of 7112862 via cif-deposit CGI script.	7112862.cif