Crystallography Open Database

Information card for entry 7113036

Preview

Coordinates	7113036.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	trans-dichloridotetraphosphaneosmium
Formula	Cl2 H12 Os P4
Calculated formula	Cl2 H12 Os P4
Title of publication	Syntheses and structures of the tetra-phosphine complexes trans-MCl2(PH3)4 (M = Ru, Os).
Authors of publication	Hall, Justin W.; Yang, Xiaoping; Jones, Richard A.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2010
Journal volume	46
Journal issue	33
Pages of publication	6168 - 6170
a	6.5759 ± 0.0009 Å
b	6.5759 ± 0.0009 Å
c	11.744 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	507.84 ± 0.13 Å³
Cell temperature	153 ± 1 K
Ambient diffraction temperature	153 ± 1 K
Number of distinct elements	4
Space group number	136
Hermann-Mauguin space group symbol	P 42/m n m
Hall space group symbol	-P 4n 2n
Residual factor for all reflections	0.0245
Residual factor for significantly intense reflections	0.0189
Weighted residual factors for significantly intense reflections	0.0375
Weighted residual factors for all reflections included in the refinement	0.0393
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180244 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/30.	7113036.cif
112217	2014-04-30	cif/ Adding structures of 7113036, 7113037 via cif-deposit CGI script.	7113036.cif