Crystallography Open Database

Information card for entry 7113373

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Coordinates	7113373.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H32 Cl F9 N3 P2 Ru Sb
Calculated formula	C48 H32 Cl F9 N3 P2 Ru Sb
Title of publication	A new class of tethered-arene ruthenium(II) complexes with pendant P and C donor atoms: synthesis of eta6:eta1:eta1 phosphonio-azabutadienyl ruthenabicycles via allenylidene intermediates.
Authors of publication	Cadierno, Victorio; Díez, Josefina; García-Alvarez, Joaquín; Gimeno, José
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2004
Journal issue	16
Pages of publication	1820 - 1821
a	39.587 ± 0.007 Å
b	12.43 ± 0.002 Å
c	20.522 ± 0.004 Å
α	90°
β	117.306 ± 0.007°
γ	90°
Cell volume	8973 ± 3 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1175
Residual factor for significantly intense reflections	0.0603
Weighted residual factors for significantly intense reflections	0.1392
Weighted residual factors for all reflections included in the refinement	0.1652
Goodness-of-fit parameter for all reflections included in the refinement	0.968
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180247 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/33.	7113373.cif
114605	2014-05-28	cif/ Adding structures of 7113373, 7113374 via cif-deposit CGI script.	7113373.cif