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Information card for entry 7113438
Preview
| Coordinates | 7113438.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Sym-anti perchlorato |
|---|---|
| Chemical name | Sym-anti perchlorato |
| Formula | C14 H29 Cl2 Co N4 O8 |
| Calculated formula | C14 H29 Cl2 Co N4 O8 |
| Title of publication | The first structurally characterised perchlorato-cobalt(III) complexes, involving the C-bonded macrobicyclic ligand 1,4,8,11-tetraazabicyclo[9.5.2]octadecane |
| Authors of publication | Zhou, Xiangting; Day, Anthony I.; Willis, Anthony C.; Jackson, W. Gregory |
| Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
| Year of publication | 2003 |
| Journal issue | 18 |
| Pages of publication | 2386 - 2387 |
| a | 8.1097 ± 0.0001 Å |
| b | 14.6807 ± 0.0003 Å |
| c | 8.7957 ± 0.0002 Å |
| α | 90° |
| β | 108.442 ± 0.001° |
| γ | 90° |
| Cell volume | 993.4 ± 0.03 Å3 |
| Cell temperature | 200 K |
| Ambient diffraction temperature | 200 K |
| Number of distinct elements | 6 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for significantly intense reflections | 0.0368 |
| Weighted residual factors for all reflections included in the refinement | 0.0416 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.0641 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Duplicate of | 7104781 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 210541 (current) | 2018-09-07 | cif/7/ Updating bibliography in entries 7104780-7104781, 7113437-7113438. Marking entries 7113437-7113438 as duplicates of entries 7104780-7104781. |
7113438.cif |
| 176453 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7. |
7113438.cif |
| 130086 | 2015-01-23 | cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ | xargs -i sh -c 'cif_fix_values {} \ | cif_filter --add-cif-header {} \ | sponge {}' |
7113438.cif |
| 115062 | 2014-06-02 | cif/ Adding structures of 7113437, 7113438 via cif-deposit CGI script. |
7113438.cif |
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Users of the data should acknowledge the original authors of the
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