Crystallography Open Database

Information card for entry 7113440

Preview

Coordinates	7113440.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H74 Lu N3 Si2
Calculated formula	C48 H65 Lu N3 Si2
Title of publication	Unusual alkyl group activation and cationic complex formation from a novel lutetium dialkyl complex supported by a tridentate monoanionic ligand
Authors of publication	Cameron, Thomas M.; Gordon, John C.; Michalczyk, Ryszard; Scott, Brian L.
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2003
Journal issue	18
Pages of publication	2282 - 2283
a	18.45 ± 0.005 Å
b	14.22 ± 0.004 Å
c	19.167 ± 0.005 Å
α	90°
β	104.742 ± 0.005°
γ	90°
Cell volume	4863 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0604
Residual factor for significantly intense reflections	0.0533
Weighted residual factors for significantly intense reflections	0.0998
Weighted residual factors for all reflections included in the refinement	0.1009
Goodness-of-fit parameter for all reflections included in the refinement	2.115
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7104800
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
210609 (current)	2018-09-09	cif/7/ Updating bibliography in entries 7104800, 7113440. Marking entry 7113440 as a duplicate of entry 7104800.	7113440.cif
180248	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/34.	7113440.cif
115064	2014-06-02	cif/ Adding structures of 7113440 via cif-deposit CGI script.	7113440.cif