Crystallography Open Database

Information card for entry 7113504

Preview

Coordinates	7113504.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H27 I3 N9 O0 U
Calculated formula	C18 I2.99 N9 U
Title of publication	Preparation and structures of homoleptic Pu(III) and U(III) acetonitrile salts
Authors of publication	Enriquez, Alejandro E.; Matonic, John H.; Scott, Brian L.; Neu, Mary P.
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2003
Journal issue	15
Pages of publication	1892 - 1893
a	10.974 ± 0.004 Å
b	10.974 ± 0.004 Å
c	24.475 ± 0.011 Å
α	90°
β	90°
γ	120°
Cell volume	2552.6 ± 1.7 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	6
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0863
Residual factor for significantly intense reflections	0.0737
Weighted residual factors for significantly intense reflections	0.1273
Weighted residual factors for all reflections included in the refinement	0.1296
Goodness-of-fit parameter for all reflections included in the refinement	2.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	7103807
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
210459 (current)	2018-09-05	cif/7/ Updating bibliography in entries 7103806-7103807, 7113503-7113504. Marking entries 7113503-7113504 as duplicates of entries 7103806-7103807.	7113504.cif
180249	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/35.	7113504.cif
115096	2014-06-02	cif/ Adding structures of 7113503, 7113504 via cif-deposit CGI script.	7113504.cif